CN207204067U - A kind of catalyzed by solid base reactor - Google Patents

A kind of catalyzed by solid base reactor Download PDF

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Publication number
CN207204067U
CN207204067U CN201721090651.XU CN201721090651U CN207204067U CN 207204067 U CN207204067 U CN 207204067U CN 201721090651 U CN201721090651 U CN 201721090651U CN 207204067 U CN207204067 U CN 207204067U
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CN
China
Prior art keywords
reactor
board
catalyzed
ultrasonic wave
magnetic field
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Expired - Fee Related
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CN201721090651.XU
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Chinese (zh)
Inventor
方利国
李钰
苏国城
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South China University of Technology SCUT
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South China University of Technology SCUT
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Priority to CN201721090651.XU priority Critical patent/CN207204067U/en
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Abstract

The utility model discloses a kind of catalyzed by solid base reactor, including reactor, ultrasonic transmitter, controller and temperature sensor, the upper end of the reactor is provided with feeding mouth, the lower end of reactor is provided with discharging opening, and the top and bottom of the side wall of reactor are respectively equipped with steam (vapor) outlet and steam inlet;The top and bottom of reactor are equipped with ultrasonic wave joint, this ultrasonic wave joint is connected with ultrasonic transmitter, temperature sensor is installed on reactor, and temperature sensor and ultrasonic transmitter are connected with controller, and the outer surface of reactor is wound with longitudinal magnetic field coiling and transverse magnetic field coiling;Board is provided with reactor, this board is between steam (vapor) outlet and steam inlet.The utility model is made solid catalyst do periodic motion, promotes heterogeneous reactant system to be well mixed, increase the interparticle contact-impact probability of reactant, improve catalytic efficiency, shortened the reaction time using the effect of magnetic field and ultrasonic wave-coupled.

Description

A kind of catalyzed by solid base reactor
Technical field
It the utility model is related to biodiesel Preparation equipment, and in particular to a kind of catalyzed by solid base reactor.
Background technology
With the development of World Economics, the whole world is increasing to the demand of the energy, along with the environment of getting worse Problem, fossil fuel can not meet the needs of development of world economy, find a kind of new, environment-friendly alternative energy Source causes the extensive concern of people.Fuel is transported as green, biodiesel is with its preferable combustibility, environmental protection and is recycled The advantages that regeneration, turn into one of most promising alternative energy source.Catalyst is needed to use in the preparation of biodiesel, and it is current The catalyst used is homogeneous solid catalyst, but homogeneous catalysis of solid catalyst is influenceed greatly by aliphatic acid and water, and catalyst is not Easily recovery, environmental pollution is serious, and product separation is also relatively difficult.
Utility model content
The purpose of this utility model is to overcome above the shortcomings of the prior art, there is provided it is a kind of it is simple in construction, Rationally, convenient recovery catalyst and the catalyzed by solid base reactor to reduce environmental pollution.
The purpose of this utility model is realized by following technical scheme:This catalyzed by solid base reactor, including reactor, Ultrasonic transmitter, controller and temperature sensor, the upper end of the reactor are provided with feeding mouth, and the lower end of the reactor is set There is discharging opening, the top and bottom of the side wall of the reactor are respectively equipped with steam (vapor) outlet and steam inlet;The reactor Top and bottom are equipped with ultrasonic wave joint, and this ultrasonic wave joint is connected with ultrasonic transmitter, the temperature sensor installation In reactor, the temperature sensor and ultrasonic transmitter are connected with controller, and the outer surface of the reactor is wound with Longitudinal magnetic field coiling and transverse magnetic field coiling;Board is provided with the reactor, this board is located at steam (vapor) outlet and steam inlet Between.
Preferably, the reactor includes the rounded kettle and kettle cover in section, and the kettle cover is covered in the upper end of kettle, The feeding mouth is located at the centre of kettle cover, and the discharging openings are among the lower end of kettle.
Preferably, the ultrasonic wave joint positioned at reactor top and bottom is 2, and positioned at 2 of reactor upper end Ultrasonic wave joint is oppositely arranged, and 2 ultrasonic wave joints positioned at reactor lower end are oppositely arranged, and 4 ultrasonic wave joints are located at Same vertical plane.
Preferably, the board is circular ring type board, and this circular ring type board includes the board film of inner ring, outer shroud and ring-type, The outer shroud is fixed on the inwall of reactor, and the outer rim of the board film and the inner side of outer shroud connect, the inner edge of the board film It is connected with the outside of inner ring.
Preferably, the upper end of the reactor is provided with condensation interface tube.
The utility model has the following advantages relative to prior art:
1st, this catalyzed by solid base reactor is mainly made up of reactor, ultrasonic transmitter, controller and temperature sensor, Longitudinal magnetic field coiling and transverse magnetic field coiling are wound with outside reactor, in the presence of magnetic field and ultrasonic wave-coupled, is made solid Body catalyst does periodic motion, promotes heterogeneous reactant system to be well mixed, and the interparticle contact of increase reactant is touched Probability is hit, improves catalytic efficiency, shortens the reaction time.
2nd, this catalyzed by solid base reactor is using caused by field wound (i.e. longitudinal magnetic field coiling and transverse magnetic field coiling) Magnetic field is acted on solid catalyst, so that solid catalyst carries out recovery and rinsing, that is, is simplified recovery and rinsing program, is reduced pair The pollution of environment, meanwhile, it is also convenient for the separation of product.
3rd, this catalyzed by solid base reactor is by the collective effect of ultrasonic transmitter, controller and temperature sensor etc., The reaction temperature and speed in reactor are automatically controlled, this functional reliability is high, and automaticity is high.
Brief description of the drawings
Fig. 1 is the structural representation of catalyzed by solid base reactor of the present utility model.
Fig. 2 is the sectional view of the utility model reactor.
Fig. 3 is the sectional view of the utility model board.
Wherein, 1 is reactor, and 1-1 is kettle, and 1-2 is kettle cover, and 2 be ultrasonic transmitter, and 3 be controller, and 4 be temperature Sensor, 5 be feeding mouth, and 6 be discharging opening, and 7 be steam (vapor) outlet, 8 steam inlets, and 9 be ultrasonic wave joint, 10 be longitudinal magnetic field around Line, 11 be transverse magnetic field coiling, and 12 be condensation interface tube, and 13 be board, and 13-1 is inner ring, and 13-2 is outer shroud, and 13-3 is board Film.
Embodiment
The utility model is described in further detail with reference to the accompanying drawings and examples.
Catalyzed by solid base reactor as depicted in figs. 1 and 2, including reactor, ultrasonic transmitter, controller and temperature Sensor, the upper end of the reactor are provided with feeding mouth, and the lower end of the reactor is provided with discharging opening, the side wall of the reactor Top and bottom be respectively equipped with steam (vapor) outlet and steam inlet;The top and bottom of the reactor are equipped with ultrasonic wave and connect Head, this ultrasonic wave joint are connected with ultrasonic transmitter, and the temperature sensor is installed on reactor, the temperature sensor and Ultrasonic transmitter is connected with controller, the outer surface of the reactor be wound with longitudinal magnetic field coiling and transverse magnetic field around Line;Board is provided with the reactor, this board is between steam (vapor) outlet and steam inlet.
As shown in figure 1, above-below direction winding of the longitudinal magnetic field coiling along reactor, and transverse magnetic field coiling is along reactor Circumferencial direction is wound, and longitudinal magnetic field coiling and transverse magnetic field coiling intersect at the outer surface of reactor, and longitudinal magnetic field coiling and Transverse magnetic intersects to form multiple grids to coiling.This is simple in construction, it is ensured that magnetic field's regularity and stability in reactor. And the controller in the present embodiment is computer.
The reactor includes the rounded kettle and kettle cover in section, and the kettle cover is covered in the upper end of kettle, it is described enter Material mouth is located at the centre of kettle cover, and the discharging openings are among the lower end of kettle.This is simple in construction, and convenient installation is safeguarded.
Ultrasonic wave joint positioned at reactor top and bottom is 2, and 2 ultrasonic waves positioned at reactor upper end connect Head is oppositely arranged, and 2 ultrasonic wave joints positioned at reactor lower end are oppositely arranged, and 4 ultrasonic wave joints are positioned at same vertical Face.As schemed, in one end intercalation reaction kettle of ultrasonic wave joint, and the other end is connected by wire with supersonic generator.This knot Structure is simple, convenient installation, and caused ultrasonic wave is uniformly distributed in reactor.
As shown in figure 3, the board is circular ring type board, this circular ring type board includes the board of inner ring, outer shroud and ring-type Film, the outer shroud are fixed on the inwall of reactor, and the outer rim of the board film and the inner side of outer shroud connect, the board film it is interior The outside of edge and inner ring connects.This is simple in construction, the load bearing solid catalyst that can stablize, ensures effective preparation of biodiesel.
The upper end of the reactor is provided with condensation interface tube.
The course of work of this catalyzed by solid base reactor is as follows,
Raw material enters in reactor from feeding mouth first, by adjusting the size of electric current, direction, cycle so as to controlling longitudinal direction Alternating magnetic field caused by field wound and transverse magnetic field coiling, and then control magnetic retention to urge during biodiesel is prepared The motion of agent improves the yield of biodiesel;
Then, ultrasonic wave caused by supersonic generator is opposite positioned at reactant center in reactor by ultrasonic wave joint It is radial, and the temperature signal detected in reactor is transferred to controller by temperature sensor, controller is according to this temperature The tranmitting frequency of signal control supersonic generator and the speed and temperature of size of current control reaction;
After reactant fully reacts, the solid of magnetic is urged in magnetic field caused by longitudinal magnetic field coiling and transverse magnetic field coiling Agent absorption is reclaimed on the board film of board, and product discharges reactor by discharging opening, and this product is urged with solid Convenient separation between agent.
Finally, steam is slowly discharged into rinse magnetic solid catalyst from steam inlet, steam is arranged by steam (vapor) outlet again Remove, charging reaction next time is waited after rinse, the catalyzed by solid base completed under a kind of magnetic field and ultrasonic wave-coupled effect is anti- Answer the implementation of device.
Above-mentioned embodiment is preferred embodiment of the present utility model, and the utility model can not be defined, Other any changes made without departing from the technical solution of the utility model or other equivalent substitute modes, are included in Within the scope of protection of the utility model.

Claims (5)

  1. A kind of 1. catalyzed by solid base reactor, it is characterised in that:Passed including reactor, ultrasonic transmitter, controller and temperature Sensor, the upper end of the reactor are provided with feeding mouth, and the lower end of the reactor is provided with discharging opening, the side wall of the reactor Top and bottom are respectively equipped with steam (vapor) outlet and steam inlet;The top and bottom of the reactor are equipped with ultrasonic wave joint, This ultrasonic wave joint is connected with ultrasonic transmitter, and the temperature sensor is installed on reactor, the temperature sensor and super Pinger is connected with controller, and the outer surface of the reactor is wound with longitudinal magnetic field coiling and transverse magnetic field coiling; Board is provided with the reactor, this board is between steam (vapor) outlet and steam inlet.
  2. 2. catalyzed by solid base reactor according to claim 1, it is characterised in that:It is rounded that the reactor includes section Kettle and kettle cover, the kettle cover is covered in the upper end of kettle, and the feeding mouth is located at the centre of kettle cover, the discharging openings in Among the lower end of kettle.
  3. 3. catalyzed by solid base reactor according to claim 1, it is characterised in that:Positioned at the super of reactor top and bottom Sonic connector is 2, and 2 ultrasonic wave joints positioned at reactor upper end are oppositely arranged, and 2 positioned at reactor lower end are super Sonic connector is oppositely arranged, and 4 ultrasonic wave joints are located at same vertical plane.
  4. 4. catalyzed by solid base reactor according to claim 1, it is characterised in that:The board is circular ring type board, this Circular ring type board includes the board film of inner ring, outer shroud and ring-type, and the outer shroud is fixed on the inwall of reactor, the board film The inner side of outer rim and outer shroud connects, and the inner edge of the board film and the outside of inner ring connect.
  5. 5. catalyzed by solid base reactor according to claim 1, it is characterised in that:The upper end of the reactor is provided with condensation Interface tube.
CN201721090651.XU 2017-08-28 2017-08-28 A kind of catalyzed by solid base reactor Expired - Fee Related CN207204067U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721090651.XU CN207204067U (en) 2017-08-28 2017-08-28 A kind of catalyzed by solid base reactor

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Application Number Priority Date Filing Date Title
CN201721090651.XU CN207204067U (en) 2017-08-28 2017-08-28 A kind of catalyzed by solid base reactor

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Publication Number Publication Date
CN207204067U true CN207204067U (en) 2018-04-10

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107349885A (en) * 2017-08-28 2017-11-17 华南理工大学 A kind of catalyzed by solid base reactor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107349885A (en) * 2017-08-28 2017-11-17 华南理工大学 A kind of catalyzed by solid base reactor

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180410

Termination date: 20200828

CF01 Termination of patent right due to non-payment of annual fee