CN207187721U - A kind of organic chemistry apparatus for photoreaction - Google Patents
A kind of organic chemistry apparatus for photoreaction Download PDFInfo
- Publication number
- CN207187721U CN207187721U CN201721190774.0U CN201721190774U CN207187721U CN 207187721 U CN207187721 U CN 207187721U CN 201721190774 U CN201721190774 U CN 201721190774U CN 207187721 U CN207187721 U CN 207187721U
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- China
- Prior art keywords
- quartz glass
- glass reaction
- reaction room
- nut
- fixedly connected
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Abstract
The utility model discloses a kind of organic chemistry apparatus for photoreaction, including quartz glass reaction room, ultraviolet radiator, material inlet, upper agitator, discharging opening, heating element heater and cooling tube, the left and right ends of the quartz glass reaction outdoor are provided with ultraviolet radiator, the outside of the quartz glass reaction room is provided with housing, the ultraviolet radiator is fixedly connected with housing by nut, the ultraviolet radiator and external power source are electrically connected with, and the left end of quartz glass reaction room upper surface is provided with material inlet；Novel organic apparatus for photoreaction is provided with agitator, when raw material carries out chemical light reaction, raw material is set to stir, make reaction more abundant, be provided with cooling tube, the temperature in quartz glass reaction room can be reduced, the utility model is provided with heating element heater, heat can be provided for raw material reaction, make reaction more abundant, improve the reaction efficiency of raw material.
Description
Technical field
The utility model belongs to photochemical reaction technical field, and in particular to a kind of organic chemistry apparatus for photoreaction.
Background technology
At present, photochemical reaction common in organic synthesis has photooxidation reaction, photoreduction, photopolymerization reaction and light
Substitution reaction etc., photooxidation reaction are the addition reaction that organic molecule grows prosperity with oxygen under light irradiation, sensitising agent effect, light
Oxidation reaction condition is gentle, it is not necessary to chemical agent and heavy metal catalyst, is become more meticulous in medicine, essence, detergent and dyestuff etc.
Appeared in the newspapers repeatly in terms of the synthesis of product, photoreduction is under photocatalysis, and organic molecule extracts hydrogen point from oxygen donator
Sub and generation reduction reaction.Study at present it is more be hydroxy compounds photoreduction, such as double benzophenones are in hexichol first
Photoreduction occurs in alcohol and can obtain tetraphenyl ethanol, the light filter generation chlorohydrocarbon processed of light substitution reaction commonly aliphatic hydrocarbon,
Monochloro methane, dichloromethane, chloroform and carbon tetrachloride, a variety of cleaning agents, insecticide, antioxygen can be prepared by light substitution reaction
Agent and intermediate, these reactions have the characteristics that gentle compared with other approach, the rate of recovery is high and selectivity is good, and some products are even
Non- optical chlorinating reaction can not be caused thus potential in industrial production.
Original organic chemistry apparatus for photoreaction, reacted in reaction unit not enough fully, reaction efficiency is low, to chemistry
Light reaction can not be controlled.
Utility model content
The purpose of this utility model is to provide a kind of organic chemistry apparatus for photoreaction, to solve to carry in above-mentioned background technology
Go out original organic chemistry apparatus for photoreaction, reacted in reaction unit not enough fully, reaction efficiency is low, to chemically reacting not
The problem of being controlled.
To achieve the above object, the utility model provides following technical scheme：A kind of organic chemistry apparatus for photoreaction, including
Quartz glass reaction room, ultraviolet radiator, material inlet, upper agitator, discharging opening, heating element heater and cooling tube, the stone
The left and right ends of English glass reaction outdoor are provided with ultraviolet radiator, and the outside of the quartz glass reaction room is provided with shell
Body, the ultraviolet radiator are fixedly connected with housing by nut, and the ultraviolet radiator and external power source are electrically connected with,
The left end of quartz glass reaction room upper surface is provided with material inlet, and material inlet and the quartz glass reaction room passes through
Nut is fixedly connected, and the quartz glass reaction room is internally provided with agitator, the outside of the quartz glass reaction room
Lower surface is provided with discharging opening, and the discharging opening is fixedly connected with quartz glass reaction room by nut, and the quartz glass is anti-
Answer the inner bottom of room to be provided with heating element heater, cooling tube, the left and right of the cooling tube are provided with the right side of the heating element heater
Both ends are fixedly connected with quartz glass reaction room by nut.
Preferably, the quartz glass reaction room is fixedly connected with housing by nut, bottom of the housing or so two
End is provided with base leg, and the base leg and housing are fixedly connected by welding.
Preferably, the middle position of quartz glass reaction room upper surface is provided with stirring motor, the stirring electricity
Machine is fixedly connected with quartz glass reaction room by base nut, and the quartz glass reaction chamber interior middle position is provided with
Stirring shaft, the top of the stirring shaft and the rotating shaft of stirring motor are fixedly connected by welding, the stirring motor and outer
Portion's power supply is electrically connected with.
Preferably, the upper agitator is arranged on the upper end of stirring shaft, and the upper agitator and stirring shaft pass through spiral shell
Mother is fixedly connected, and the lower end of the stirring shaft is provided with lower agitator, and the lower agitator and stirring shaft are consolidated by nut
Fixed connection, stirring shaft and the quartz glass reaction room is rotatablely connected by bearing.
Preferably, water inlet pipe is provided with the left of the discharging opening, the left end of the water inlet pipe and cooling tube passes through nut
It is fixedly connected, outlet pipe is provided with the right side of the discharging opening, the right-hand member of the outlet pipe and cooling tube is fixed by nut is connected
Connect.
Preferably, the heating element heater is provided with two, and the heating element heater passes through with quartz glass reaction room respectively
Base nut is fixedly connected, and the heating element heater is separately mounted to the left and right sides of lower agitator, the heating element heater and outside
Power supply is electrically connected with.
Preferably, discharge valve is provided with the discharging opening, is provided with control main frame on the right surface of the housing, institute
State control main frame to be fixedly connected by nut with housing, the control main frame and external power source are electrically connected with.
Preferably, exhaust port, the bottom of the exhaust port and quartz glass are provided with the right side of the stirring motor
Reative cell is fixedly connected by nut.
Compared with prior art, the beneficial effects of the utility model are：The utility model is scientific and reasonable for structure, safe to use
Convenient, novel organic apparatus for photoreaction is provided with agitator, when raw material carries out chemical light reaction, makes raw material stirring equal
It is even, make reaction more abundant, be provided with cooling tube, the temperature in quartz glass reaction room can be reduced, the utility model is provided with
Heating element heater, it can be reacted for raw material and heat is provided, made reaction more abundant, improve the reaction efficiency of raw material.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Fig. 2 is overlooking the structure diagram of the present utility model；
In figure：1- quartz glass reactions room, 2- ultraviolet radiators, 3- material inlets, the upper agitators of 4-, 5- discharging openings,
6- heating element heaters, 7- cooling tubes, 8- discharge valves, 9- housings, 10- bases leg, 11- stirring motors, 12- stirring shafts, 13-
Lower agitator, 14- water inlet pipes, 15- outlet pipes, 16- control main frames, 17- exhaust ports.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belong to the scope of the utility model protection.
Fig. 1 and Fig. 2 are referred to, the utility model provides a kind of organic chemistry apparatus for photoreaction technical scheme：It is a kind of organic
Chemical apparatus for photoreaction, including quartz glass reaction room 1, ultraviolet radiator 2, material inlet 3, upper agitator 4, discharging opening 5,
Heating element heater 6 and cooling tube 7, the left and right ends outside quartz glass reaction room 1 are provided with ultraviolet radiator 2, quartz glass
The outside of reative cell 1 is provided with housing 9, and ultraviolet radiator 2 is fixedly connected with housing 9 by nut, the He of ultraviolet radiator 2
External power source is electrically connected with, and the left end of the upper surface of quartz glass reaction room 1 is provided with material inlet 3, material inlet 3 and quartzy glass
Glass reative cell 1 is fixedly connected by nut, and quartz glass reaction room 1 is internally provided with agitator 4, quartz glass reaction room
1 outer lower face is provided with discharging opening 5, and discharging opening 5 is fixedly connected with quartz glass reaction room 1 by nut, quartz glass
The inner bottom of reative cell 1 is provided with heating element heater 6, and the right side of heating element heater 6 is provided with cooling tube 7, the left and right two of cooling tube 7
End is fixedly connected with quartz glass reaction room 1 by nut.
In the present embodiment, it is preferred that quartz glass reaction room 1 is fixedly connected with housing 9 by nut, the bottom of housing 9
Left and right ends are provided with base leg 10, and base leg 10 and housing 9 are fixedly connected by welding, and support is provided to reaction unit
Effect.
In the present embodiment, it is preferred that the middle position of the upper surface of quartz glass reaction room 1 is provided with stirring motor 11,
Stirring motor 11 is fixedly connected with quartz glass reaction room 1 by base nut, the bosom opening position of quartz glass reaction room 1
Stirring shaft 12 is provided with, the rotating shaft on the top and stirring motor 11 of stirring shaft 12 is fixedly connected by welding, stirring motor
11 and external power source be electrically connected with, in order that raw material stirs, make reaction more abundant.
In the present embodiment, it is preferred that upper agitator 4 is arranged on the upper end of stirring shaft 12, upper agitator 4 and stirring shaft
12 are fixedly connected by nut, and the lower end of stirring shaft 12 is provided with lower agitator 13, and lower agitator 13 and stirring shaft 12 are logical
Cross nut to be fixedly connected, stirring shaft 12 and quartz glass reaction room 1 are rotatablely connected by bearing, in order that raw material stirring is equal
It is even, make reaction more abundant.
In the present embodiment, it is preferred that the left side of discharging opening 5 is provided with the left end of water inlet pipe 14, water inlet pipe 14 and cooling tube 7
It is fixedly connected by nut, the right side of discharging opening 5 is provided with outlet pipe 15, and the right-hand member of outlet pipe 15 and cooling tube 7 passes through nut
It is fixedly connected, in order to cooling in quartz glass reaction room 1.
In the present embodiment, it is preferred that heating element heater 6 is provided with two, and heating element heater 6 respectively with quartz glass reaction room
1 is fixedly connected by base nut, and heating element heater 6 is separately mounted to the left and right sides of lower agitator 13, heating element heater 6 and outside
Power supply is electrically connected with, and heat is provided for some chemical light reactions.
In the present embodiment, it is preferred that discharge valve 8 is provided with discharging opening 5, control is provided with the right surface of housing 9
Main frame 16, control main frame 16 are fixedly connected with housing 9 by nut, and control main frame 16 and external power source are electrically connected with, in order to right
Device is controlled, convenient that chemical light reaction is controlled.
In the present embodiment, it is preferred that the right side of stirring motor 11 is provided with exhaust port 17, the bottom of exhaust port 17 and
Quartz glass reaction room 1 is fixedly connected by nut, in order to be collected to caused gas in reaction.
Operation principle and process for using of the present utility model：After the utility model installs, by quartz glass reaction room 1
The base leg 10 of bottom is placed on a horizontal ground, connects external power source, is added raw material from material inlet 3 is interior, is passed through control
Main frame 16 processed controls ultraviolet radiator 2 to start working, and chemical light reaction is carried out to raw material in quartz glass reaction room 1, in original
When material needs to stir to improve reaction speed, control stirring motor 11 to work by control main frame 16, drive on stirring shaft 12
Upper agitator 4 and lower agitator 13 rotate, raw material is stirred, in raw material course of reaction in quartz glass reaction room 1
When temperature is too high, it can be connected respectively with outlet pipe 15 and water inlet pipe 14 by connecting outer water tube, by cooling tube 7 to quartz
Cool in glass reaction room 1, when needing heat in raw material reaction, raw material can be heated by heating element heater 6, made anti-
Should more fully, exhaust port 17 can collect caused gas in reaction, and reaction can be by opening discharge valve after terminating
8, material residue is discharged from discharging opening 5, complete a kind of process for using of organic chemistry apparatus for photoreaction.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art,
It is appreciated that these embodiments can be carried out with a variety of changes in the case where not departing from principle of the present utility model and spirit, repaiied
Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.
Claims (8)
1. a kind of organic chemistry apparatus for photoreaction, including quartz glass reaction room（1）, ultraviolet radiator（2）, material inlet
（3）, upper agitator（4）, discharging opening（5）, heating element heater（6）And cooling tube（7）, it is characterised in that：The quartz glass reaction
Room（1）Outside left and right ends are provided with ultraviolet radiator（2）, the quartz glass reaction room（1）Outside be provided with shell
Body（9）, the ultraviolet radiator（2）And housing（9）It is fixedly connected by nut, the ultraviolet radiator（2）And outside
Power supply is electrically connected with, the quartz glass reaction room（1）The left end of upper surface is provided with material inlet（3）, the material inlet
（3）With quartz glass reaction room（1）It is fixedly connected by nut, the quartz glass reaction room（1）Be internally provided with and stir
Mix device（4）, the quartz glass reaction room（1）Outer lower face be provided with discharging opening（5）, the discharging opening（5）And quartz
Glass reaction room（1）It is fixedly connected by nut, the quartz glass reaction room（1）Inner bottom be provided with heating element heater
（6）, the heating element heater（6）Right side be provided with cooling tube（7）, the cooling tube（7）Left and right ends and quartz glass it is anti-
Answer room（1）It is fixedly connected by nut.
A kind of 2. organic chemistry apparatus for photoreaction according to claim 1, it is characterised in that：The quartz glass reaction room
（1）And housing（9）It is fixedly connected by nut, the housing（9）Bottom left and right ends be provided with base leg（10）, it is described
Base leg（10）And housing（9）It is fixedly connected by welding.
A kind of 3. organic chemistry apparatus for photoreaction according to claim 1, it is characterised in that：The quartz glass reaction room
（1）The middle position of upper surface is provided with stirring motor（11）, the stirring motor（11）With quartz glass reaction room（1）It is logical
Cross base nut to be fixedly connected, the quartz glass reaction room（1）Bosom opening position is provided with stirring shaft（12）, it is described
Stirring shaft（12）Top and stirring motor（11）Rotating shaft be fixedly connected by welding, the stirring motor（11）And outside
Power supply is electrically connected with.
A kind of 4. organic chemistry apparatus for photoreaction according to claim 1, it is characterised in that：The upper agitator（4）Peace
Mounted in stirring shaft（12）Upper end, the upper agitator（4）And stirring shaft（12）It is fixedly connected by nut, the stirring
Rotating shaft（12）Lower end be provided with lower agitator（13）, the lower agitator（13）And stirring shaft（12）Fixed and connected by nut
Connect, the stirring shaft（12）With quartz glass reaction room（1）It is rotatablely connected by bearing.
A kind of 5. organic chemistry apparatus for photoreaction according to claim 1, it is characterised in that：The discharging opening（5）A left side
Side is provided with water inlet pipe（14）, the water inlet pipe（14）And cooling tube（7）Left end be fixedly connected by nut, the discharging opening
（5）Right side be provided with outlet pipe（15）, the outlet pipe（15）And cooling tube（7）Right-hand member be fixedly connected by nut.
A kind of 6. organic chemistry apparatus for photoreaction according to claim 1, it is characterised in that：The heating element heater（6）If
It is equipped with two, and the heating element heater（6）Respectively with quartz glass reaction room（1）It is fixedly connected by base nut, it is described to add
Thermal element（6）It is separately mounted to lower agitator（13）The left and right sides, the heating element heater（6）It is electrically connected with external power source.
A kind of 7. organic chemistry apparatus for photoreaction according to claim 1, it is characterised in that：The discharging opening（5）On set
It is equipped with discharge valve（8）, the housing（9）Right surface on be provided with control main frame（16）, the control main frame（16）And shell
Body（9）It is fixedly connected by nut, the control main frame（16）It is electrically connected with external power source.
A kind of 8. organic chemistry apparatus for photoreaction according to claim 3, it is characterised in that：The stirring motor（11）'s
Right side is provided with exhaust port（17）, the exhaust port（17）Bottom and quartz glass reaction room（1）Fixed by nut
Connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721190774.0U CN207187721U (en) | 2017-09-18 | 2017-09-18 | A kind of organic chemistry apparatus for photoreaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721190774.0U CN207187721U (en) | 2017-09-18 | 2017-09-18 | A kind of organic chemistry apparatus for photoreaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207187721U true CN207187721U (en) | 2018-04-06 |
Family
ID=61788287
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721190774.0U Expired - Fee Related CN207187721U (en) | 2017-09-18 | 2017-09-18 | A kind of organic chemistry apparatus for photoreaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207187721U (en) |
-
2017
- 2017-09-18 CN CN201721190774.0U patent/CN207187721U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180406 Termination date: 20200918 |