CN207187707U - A kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone - Google Patents
A kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone Download PDFInfo
- Publication number
- CN207187707U CN207187707U CN201721156995.6U CN201721156995U CN207187707U CN 207187707 U CN207187707 U CN 207187707U CN 201721156995 U CN201721156995 U CN 201721156995U CN 207187707 U CN207187707 U CN 207187707U
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- CN
- China
- Prior art keywords
- tank body
- guard
- epoxyprogesterone
- 16alpha
- 17alpha
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
It the utility model is related to technical field of chemical,Especially a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone,Including tank body,The bottom of tank body sets discharge nozzle,The side wall of tank body sets feed pipe,The top of tank body sets top cover,The bottom of tank body sets multiple heating rods,The multiple guards of grafting on top cover,The lumen loading catalyst of guard,Adpting flange is set at the upper end open of guard,Guard is connected by adpting flange with connecting-rod bolt,Guard is located at the inner chamber of tank body,Connecting rod extends to the outside of tank body and is connected with fixed plate,The side wall of fixed plate is fixedly connected with a pair of collars,The side wall of tank body is provided with electric cylinder,The inner chamber of the power rail insertion collar of electric cylinder and locking,The oxidation reaction apparatus of the production 16ALPHA,17ALPHA-epoxyprogesterone can accurately adjust temperature and reaction speed in tank body at work,It is and simple in construction,It is easy to operate,It ensure that the quality of 16ALPHA,17ALPHA-epoxyprogesterone made from reaction.
Description
Technical field
Technical field of chemical is the utility model is related to, more particularly to a kind of oxidation reaction dress for producing 16ALPHA,17ALPHA-epoxyprogesterone
Put.
Background technology
Walsh thing is a kind of chemical intermediate, and it needs to use oxidation reaction apparatus when carrying out oxidation reaction, existing
Oxidation reaction apparatus is usually retort, and walsh raw material is heated in launching into retort, stirred, but existing reaction
Device still suffers from the shortcomings that reaction speed is slow, and reaction speed is not easy to regulation when carrying out walsh thing oxidation reaction.
Utility model content
The purpose of this utility model is, reaction speed slow in order to solve to exist in the prior art oxidation reaction apparatus reaction speed
The shortcomings that degree is not easy to adjust, and a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone proposed.
To achieve these goals, the utility model employs following technical scheme：
A kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone, including tank body are designed, the bottom of the tank body sets discharging
Pipe, the side wall of the tank body set feed pipe, and the top of the tank body sets top cover, and the bottom of the tank body sets multiple heating
Rod, the multiple guards of grafting on the top cover, the lumen loading catalyst of the guard, the company of setting at the upper end open of the guard
Acting flange, the guard are connected by adpting flange with connecting-rod bolt, and the guard is located at the inner chamber of tank body, the connecting rod
Extend to the outside of tank body and be connected with fixed plate, the side wall of the fixed plate is fixedly connected with a pair of collars, the side of the tank body
Wall is provided with electric cylinder, the inner chamber of the power rail insertion collar of the electric cylinder and locking, is installed in the middle part of the outer wall of the top cover
Have motor, the power rail of the motor extends to the inner chamber of tank body and is fixedly connected with rotating shaft, the rotating shaft away from motor one
End is fixedly connected with stirring vane.
Preferably, the outer wall socket rubber sleeve of the adpting flange.
Preferably, the inner cavity top of the guard is fixedly connected with fixed support, and the intracavity bottom of the guard is provided with net
Pocket, the inwall of the string bag and guard are slidably connected, and pull bar are fixedly connected with the string bag, the pull bar is away from the string bag
Fixed support is run through in one end.
Preferably, the bottom of the guard is fixedly connected with cover body.
Preferably, it is provided with location-plate in the middle part of the inner chamber of the tank body.
The utility model proposes a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone, beneficial effect is：By
The bottom of tank body sets multiple heating rods, and heating rod is connected by wire with external power source, and the power of regulation power supply is i.e. adjustable
Reaction temperature in tank body, electric cylinder and guard are set, catalyst is placed in guard, by controlling the flexible of electric cylinder, to control
Depth in guard insertion walsh raw material processed, so as to reach the contact area of regulation catalyst and walsh raw material, is realized
The function of accurate control reaction speed, the oxidation reaction apparatus of the production 16ALPHA,17ALPHA-epoxyprogesterone can accurately adjust tank at work
Temperature and reaction speed in body, and it is simple in construction, it is easy to operate, it ensure that the quality of 16ALPHA,17ALPHA-epoxyprogesterone made from reaction.
Brief description of the drawings
Fig. 1 be the utility model proposes a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone structural representation；
Fig. 2 be the utility model proposes a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone net cover structure signal
Figure.
In figure：1 tank body, 2 heating rods, 3 discharge nozzles, 4 motors, 5 top covers, 6 electric cylinders, 7 feed pipes, 8 fixed plates, 9 connections
Bar, 10 collars, 11 catalyst, 12 guards, 13 rotating shafts, 14 stirring vanes, 15 location-plates, 16 adpting flanges, 17 rubber sleeves, 18 are consolidated
Fixed rack, 19 string bags, 20 cover bodies, 21 pull bars.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.
Reference picture 1-2, a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone, including tank body 1, the bottom of tank body 1 are set
Discharge nozzle 3, the side wall of tank body 1 set feed pipe 7, and the top of tank body 1 sets top cover 5, and the bottom of tank body 1 sets multiple heating rods
2, the multiple guards 12 of grafting on top cover 5, the lumen loading catalyst 11 of guard 12, connection method is set at the upper end open of guard 12
Orchid 16, guard 12 is located at the inner chamber of tank body 1 by adpting flange 16 and the bolt connection of connecting rod 9, guard 12, and connecting rod 9 extends
It is connected to the outside of tank body 1 and with fixed plate 8, the side wall of fixed plate 8 is fixedly connected with a pair of collars 10, the side wall installation of tank body 1
There are electric cylinder 6, the inner chamber of the power rail insertion collar 10 of electric cylinder 6 and locking, motor 4 is installed in the middle part of the outer wall of top cover 5, electricity
The power rail of machine 4 extends to the inner chamber of tank body 1 and is fixedly connected with rotating shaft 13, and the one end of rotating shaft 13 away from motor 4 is fixedly connected
Stirring vane 14.
The outer wall socket rubber sleeve 17 of adpting flange 16, sets rubber sleeve 17 to play a part of sealing, prevents foreign matter
Gap between top cover 5 and connecting rod 9, which enters, pollutes walsh raw material in tank body 1, the inner cavity top of guard 12 is fixedly connected
Fixed support 18, the intracavity bottom of guard 12 are provided with the string bag 19, and the inwall of the string bag 19 and guard 12 is slidably connected, on the string bag 19
Pull bar 21 is fixedly connected with, fixed support 18 is run through in the one end of pull bar 21 away from the string bag 19, sets the string bag 19 and pull bar 21,
Catalyst 11 in guard 12 is taken out and changed by person easy to operation, simply pulls pull bar 21 to connect when taking out catalyst 11
Mouthful, the bottom of guard 12 is fixedly connected with cover body 20, sets cover body 20 to be used to collect the particle of catalyst 11 being scattered, prevents what is be scattered
Catalyst granules 11 enters in walsh raw material, and location-plate 15 is provided with the middle part of the inner chamber of tank body 1, sets location-plate 15 to play limit
The effect of position, prevent the too deep normal rotation for hindering stirring vane 14 of the insertion depth of guard 12.
Operation principle：Heating rod 2 is connected by wire with external power source, in the i.e. adjustable tank body 1 of power of regulation power supply
Reaction temperature, electric cylinder 6 and guard 12 are set, catalyst 11 is placed in guard 12, it is the 6 of electric cylinder flexible by controlling, come
The depth for controlling guard 12 to insert in walsh raw material, so as to reach the contact area of regulation catalyst 11 and walsh raw material,
Realize the function of accurate control reaction speed.
It is described above, the only preferable embodiment of the utility model, but the scope of protection of the utility model is not
This is confined to, any one skilled in the art is in the technical scope that the utility model discloses, according to this practicality
New technical scheme and its utility model design are subject to equivalent substitution or change, should all cover in protection model of the present utility model
Within enclosing.
Claims (5)
1. a kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone, including tank body (1), the bottom of the tank body (1) sets discharging
Manage (3), the side wall of the tank body (1) sets feed pipe (7), and the top of the tank body (1) sets top cover (5), it is characterised in that
The bottom of the tank body (1) sets multiple heating rods (2), the multiple guards of grafting (12) on the top cover (5), the guard (12)
Lumen loading catalyst (11), adpting flange (16) is set at the upper end open of the guard (12), and the guard (12) is logical
Adpting flange (16) and connecting rod (9) bolt connection are crossed, the guard (12) is located at the inner chamber of tank body (1), the connecting rod (9)
Extending to the outside of tank body (1) and be connected with fixed plate (8), the side wall of the fixed plate (8) is fixedly connected with a pair of collars (10),
The side wall of the tank body (1) is provided with electric cylinder (6), the inner chamber of the power rail insertion collar (10) of the electric cylinder (6) and lock
Tightly, motor (4) is installed in the middle part of the outer wall of the top cover (5), the power rail of the motor (4) extends to the inner chamber of tank body (1)
And be fixedly connected with rotating shaft (13), the one end of the rotating shaft (13) away from motor (4) is fixedly connected with stirring vane (14).
A kind of 2. oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone according to claim 1, it is characterised in that the connection
The outer wall socket rubber sleeve (17) of flange (16).
A kind of 3. oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone according to claim 1, it is characterised in that the guard
(12) inner cavity top is fixedly connected with fixed support (18), and the intracavity bottom of the guard (12) is provided with the string bag (19), described
The inwall of the string bag (19) and guard (12) is slidably connected, and pull bar (21), the pull bar are fixedly connected with the string bag (19)
(21) fixed support (18) is run through in one end away from the string bag (19).
A kind of 4. oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone according to claim 1, it is characterised in that the guard
(12) bottom is fixedly connected with cover body (20).
A kind of 5. oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone according to claim 1, it is characterised in that the tank body
(1) location-plate (15) is provided with the middle part of inner chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721156995.6U CN207187707U (en) | 2017-09-11 | 2017-09-11 | A kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721156995.6U CN207187707U (en) | 2017-09-11 | 2017-09-11 | A kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207187707U true CN207187707U (en) | 2018-04-06 |
Family
ID=61790348
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721156995.6U Expired - Fee Related CN207187707U (en) | 2017-09-11 | 2017-09-11 | A kind of oxidation reaction apparatus for producing 16ALPHA,17ALPHA-epoxyprogesterone |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207187707U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115253931A (en) * | 2022-07-06 | 2022-11-01 | 安徽昊源化工集团有限公司 | Coupling reactor for synthesizing ethylene glycol by dimethyl oxalate hydrogenation |
-
2017
- 2017-09-11 CN CN201721156995.6U patent/CN207187707U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115253931A (en) * | 2022-07-06 | 2022-11-01 | 安徽昊源化工集团有限公司 | Coupling reactor for synthesizing ethylene glycol by dimethyl oxalate hydrogenation |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180406 Termination date: 20180911 |