CN207169729U - A kind of Raney's nickel dead catalyst recycling device - Google Patents
A kind of Raney's nickel dead catalyst recycling device Download PDFInfo
- Publication number
- CN207169729U CN207169729U CN201721088389.5U CN201721088389U CN207169729U CN 207169729 U CN207169729 U CN 207169729U CN 201721088389 U CN201721088389 U CN 201721088389U CN 207169729 U CN207169729 U CN 207169729U
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- China
- Prior art keywords
- tank body
- raney
- taper tank
- alkali
- recycling device
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Abstract
The utility model provides a kind of Raney's nickel dead catalyst recycling device, including taper tank body, installation organic frame at the top of the taper tank body, reductor and motor are installed in the frame, the reductor connects agitator, agitator extend into taper tank interior, the paddle of the agitator is frame type stirring leaf, the top side of taper tank body is connected with inlet channel and alkali inlet tube road, top opposite side is provided with manhole, tapered shaped can body side surface is provided with discharge outlet, bottom is provided with regenerated catalyst outlet, liquid level gauge is also equipped with the taper tank body, temperature transmitter and pH measurement mouths, under certain activation condition, the dead catalyst activated recycles from regenerated catalyst outlet.The utility model is simple in construction, easy to operate, reduces labor intensity, pollution-free, improves waste catalyst recovery rate, and production cost is saved in regeneration, and factory is practical.
Description
Technical field
A kind of recycling device is the utility model is related to, specifically a kind of Raney's nickel dead catalyst recycling device.
Background technology
It is mostly tank body to react retracting device, is equipment common in industrial production, and an agitator is installed wherein in tank body,
Subsidiary two sets of paddles up and down on agitator.During work, drive paddle to be stirred to certain orientation by the rotation of agitating shaft, lean on
Vortex one-way flow, particulate matter rotation mixing in material is driven, such paddle contact area is small, and rotation dynamics is little, mixes
Conjunction is not comprehensive, uneven.In some middle-size and small-size producers of production sugar alcohol, produce dead catalyst and also compare more, most of activating and regenerating
Device is all simpler and cruder, and extensive style operation, activation effect is bad, and institute's band small catalyst particles are more in waste discharge, cause dirt
Dye, the wasting of resources.
The content of the invention
For above-mentioned the deficiencies in the prior art, the utility model provides a kind of Raney's nickel dead catalyst recycling device,
The device uses frame type stirring leaf, and stirring contact area is big, and mixing effect is obvious, equipped with a variety of measuring instrumentss, discharge of wastewater peace
Magnetic sheet filter is filled, can accurately control water consumption and alkali charge, effective monitoring activation index is easy to operate, reduces work
Intensity, pollution-free, resource reutilization.
Technical scheme provided by the invention：A kind of Raney's nickel dead catalyst recycling device, including taper tank body, it is described
Organic frame is installed at the top of taper tank body, reductor and motor are installed in the frame, the reductor connects agitator, stirring
Device extend into taper tank interior, and the paddle of the agitator is frame type stirring leaf, and the top side of taper tank body is connected with
Inlet channel and alkali inlet tube road, top opposite side are provided with manhole, and tapered shaped can body side surface is provided with discharge outlet, and bottom is provided with regeneration catalyzing
Agent is exported, and liquid level gauge, temperature transmitter and pH measurement mouths are also equipped with the taper tank body.
Further, inlet valve and alkali-feeding valve door, the water inlet are respectively equipped with inlet channel and the alkali inlet tube road
Valve and alkali-feeding valve door use automatic switch valve, are interlocked with the liquid level gauge, accurate to control water consumption and alkali charge.
Further, draining valve is provided with the discharge outlet, then is connected by pipeline with magnetic sheet filter.
Further, it is also associated with bottom valve on the regenerated catalyst outlet.
Further, the bottom of the taper tank body is arranged with four along tank body side and is used for fixed journal stirrup.
The beneficial effects of the utility model：(1) the utility model uses frame type stirring leaf, and stirring contact area is big, can
Stable agitation catalyst comprehensively, mixing effect is obvious, is well mixed, and is advantageous to improve efficiency so that catalyst wash activation
It is more thorough；
(2) the utility model is equipped with the liquid level gauge with inlet valve and alkali-feeding valve gate interlock, automatic accurate control water consumption
And alkali charge, temperature transmitter and pH measurement mouths are additionally provided with, it is accurate to control activation temperature and pH, effective monitoring activation index；
(3) magnetic sheet filter is installed in discharge outlet, is suspended in the catalyst inactivated in waste water and passes through the magnetic sheet filter
It is trapped collection to get off, for other, can effectively reduces pollution, resource reutilization；
(4) the utility model makes simple, easy to operate, reduces labor intensity, pollution-free, improves dead catalyst activation
Effect, waste catalyst recovery rate is improved, save production cost, factory is practical.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
In figure：1-taper tank body, 2-motor, 3-reductor, 4-frame, 5-agitator, 6-inlet valve, 7-
Alkali-feeding valve door, 8-manhole, 9-discharge outlet, 10-draining valve, 11-magnetic sheet filter, 12-bottom valve, 13-regenerated catalyst
Outlet, 14-journal stirrup, 15-liquid level gauge, 16-temperature transmitter, 17-pH measurement mouths, 18-inlet channel, 19-alkali inlet tube
Road.
Embodiment
The utility model is described further with reference to specific embodiment.
Raney's nickel dead catalyst recycling device as shown in Figure 1, including taper tank body 1, the top of taper tank body 1
Organic frame 4 is installed, reductor 3 and motor 2 are installed in the frame 4, the reductor 3 connects agitator 5, and agitator 5 is stretched
Enter to inside taper tank body 1, the paddle of the agitator 5 is frame type stirring leaf, the top side of taper tank body 1 be connected with into
Waterpipe 18 and alkali inlet tube road 19, top opposite side are provided with manhole 8, and the side of taper tank body 1 is provided with discharge outlet 9, and bottom is provided with
Regenerated catalyst outlet 13, liquid level gauge 15, temperature transmitter 16 and pH measurement mouths 17 are also equipped with the taper tank body 1.
Inlet valve 6 and alkali-feeding valve door 7, the He of inlet valve 6 are respectively equipped with inlet channel 18 and alkali inlet tube road 19
Alkali-feeding valve door 7 uses automatic switch valve, is interlocked with the liquid level gauge 15, accurate to control water consumption and alkali charge；The draining
Draining valve 10 is provided with mouth 9, then is connected by pipeline with magnetic sheet filter 11；It is also associated with the regenerated catalyst outlet 13
Bottom valve 12；The bottom of the taper tank body 1 is arranged with four along tank body side and is used for fixed journal stirrup 14.
The water with water and configuration alkali all uses desalted water, ensures activation of catalyst, not by other ionic soils.
When the utility model is specifically used, first step cleaning dead catalyst, Raney's nickel dead catalyst is by a certain amount of from taper
The manhole 8 of tank body 1 pours into, and dead catalyst liquid level is less than draining open height 20-40cm in tank, opens inlet valve 6 and enters desalted water,
Chain with liquid level gauge 15, arrival requires liquid level, automatic to close water intaking valve 6, starts motor 2 and drives reductor 3 to rotate, so as to stir
Device 5 starts running, and dead catalyst in water arrange comprehensively by cleaning more than 30min, stopping agitator 5, quiescent settling 1 hour, opening
Water valve 10 discharges wash water, if wash water color and luster is opaque, can repeat to operate above, be cleaned multiple times；
Second step activating and regenerating dead catalyst, start, into a certain amount of desalted water, then to open alkali-feeding valve door 7 and enter quality point
Number is 6-10% soda bath, and chain with liquid level gauge 15, after arrival requires liquid level, closing alkali-feeding valve door 7, starts motor automatically
2 drive reductors 3 rotate, so as to which agitator 5 starts running, at 45-55 DEG C of 16 monitor water temperature of pot temperature transmitter, and catalysis of giving up
Agent activates in tank body, operates 1 hour, stops immersion 2 hours, is repeated 3 times, and then opens the discharge immersion alkali lye of draining valve 10,
The metal that inactivation is suspended in buck will be collected by the magnetic absorption of magnetic sheet filter 11, be arranged outside buck；
3rd step clean and reuse dead catalyst, the desalted water that water intaking valve 6 enters 45-55 DEG C is opened, by the operation of the first step
Dead catalyst is cleaned, pH value measurement mouth 17 monitors wash water pH value on tank body, repeatedly cleans, cleans to wash water pH value always and exist
7-8 scopes, wash water of draining, open bottom valve 12 and the catalyst activated is collected from regenerated catalyst outlet 13, with production, magnetic sheet
The gleanings that filter 11 gets off are applied to other.
The detailed description of specific embodiment of the present utility model is the foregoing is only, it is new not limit this practicality with this
Type, all any modification, equivalent and improvement made in mentality of designing of the present utility model etc., should be included in this practicality
Within new protection domain.
Claims (5)
1. a kind of Raney's nickel dead catalyst recycling device, including taper tank body (1), it is characterised in that：The taper tank body
(1) organic frame (4) is installed at top, and reductor (3) and motor (2), reductor (3) connection are provided with the frame (4)
Agitator (5), agitator (5) extend into taper tank body (1) inside, and the paddle of the agitator (5) is frame type stirring leaf, cone
The top side of shape tank body (1) is connected with inlet channel (18) and alkali inlet tube road (19), and top opposite side is provided with manhole (8), cone
The side of shape tank body (1) is provided with discharge outlet (9), and bottom is provided with regenerated catalyst outlet (13), also pacified on the taper tank body (1)
Equipped with liquid level gauge (15), temperature transmitter (16) and pH measurement mouth (17).
2. Raney's nickel dead catalyst recycling device according to claim 1, it is characterised in that：The inlet channel
(18) inlet valve (6) and alkali-feeding valve door (7), the inlet valve (6) and alkali-feeding valve and on alkali inlet tube road (19) are respectively equipped with
Door (7) uses automatic switch valve, is interlocked with the liquid level gauge (15), accurate to control water consumption and alkali charge.
3. Raney's nickel dead catalyst recycling device according to claim 1 or 2, it is characterised in that：The discharge outlet
(9) place is provided with draining valve (10), then is connected by pipeline with magnetic sheet filter (11).
4. Raney's nickel dead catalyst recycling device according to claim 3, it is characterised in that：The regenerated catalyst
Bottom valve (12) is also associated with outlet (13).
5. Raney's nickel dead catalyst recycling device according to claim 3, it is characterised in that：The taper tank body
(1) bottom is arranged with four along tank body side and is used for fixed journal stirrup (14).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721088389.5U CN207169729U (en) | 2017-08-29 | 2017-08-29 | A kind of Raney's nickel dead catalyst recycling device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721088389.5U CN207169729U (en) | 2017-08-29 | 2017-08-29 | A kind of Raney's nickel dead catalyst recycling device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207169729U true CN207169729U (en) | 2018-04-03 |
Family
ID=61739308
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721088389.5U Expired - Fee Related CN207169729U (en) | 2017-08-29 | 2017-08-29 | A kind of Raney's nickel dead catalyst recycling device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207169729U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108704651A (en) * | 2018-05-30 | 2018-10-26 | 嘉兴星创科技有限公司 | A kind of dead catalyst containing nickel recycling and processing device |
| CN109351218A (en) * | 2018-10-12 | 2019-02-19 | 丽水遂智科技咨询有限公司 | A kind of dead catalyst containing nickel recycling and processing device |
| CN110813975A (en) * | 2018-08-09 | 2020-02-21 | 上海立得催化剂有限公司 | Magnesium-titanium polyolefin dry powder catalyst disposal system |
| CN114082452A (en) * | 2020-08-24 | 2022-02-25 | 万华化学集团股份有限公司 | Metal framework catalyst activation system and method |
-
2017
- 2017-08-29 CN CN201721088389.5U patent/CN207169729U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108704651A (en) * | 2018-05-30 | 2018-10-26 | 嘉兴星创科技有限公司 | A kind of dead catalyst containing nickel recycling and processing device |
| CN110813975A (en) * | 2018-08-09 | 2020-02-21 | 上海立得催化剂有限公司 | Magnesium-titanium polyolefin dry powder catalyst disposal system |
| CN109351218A (en) * | 2018-10-12 | 2019-02-19 | 丽水遂智科技咨询有限公司 | A kind of dead catalyst containing nickel recycling and processing device |
| CN114082452A (en) * | 2020-08-24 | 2022-02-25 | 万华化学集团股份有限公司 | Metal framework catalyst activation system and method |
| CN114082452B (en) * | 2020-08-24 | 2023-12-19 | 万华化学集团股份有限公司 | Metal framework catalyst activation system and method |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180403 |
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| CF01 | Termination of patent right due to non-payment of annual fee |