CN207159416U - A kind of variable crucible of internal capacity - Google Patents

A kind of variable crucible of internal capacity Download PDF

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Publication number
CN207159416U
CN207159416U CN201720263741.8U CN201720263741U CN207159416U CN 207159416 U CN207159416 U CN 207159416U CN 201720263741 U CN201720263741 U CN 201720263741U CN 207159416 U CN207159416 U CN 207159416U
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layer
crucible
purity
increase
basal layer
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邹亚静
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Abstract

The utility model discloses a kind of variable crucible of internal capacity, the crucible includes crucible basal layer, increase layer at least provided with one layer on the basal layer, the basal layer and increase layer and increase layer and increase and be mutually linked by ladder buckle structure between layer, it is located at upper interface position in basal layer and the outer surface for increasing layer and is provided with bulge loop or projection uniform in a ring, it is provided with fit sealing annular element on the bulge loop or projection, fit sealing annular element is used for basal layer and increases layer and increase layer and increase and fix between layer and seal.The crucible has the characteristics that simple in construction, easy to use, volume size is variable, inexpensive, high-purity, high density, quartz ceramic crucible inner surface is smooth, be not easy sizing, knot easy to clean, structure are uniform.

Description

A kind of variable crucible of internal capacity
Technical field
It the utility model is related to and did technical field of structures, and in particular to a kind of variable crucible of internal capacity.
Background technology
Quartz-ceramics is also known as fused quartz ceramic, ceramics quartz glass, quartz glass sintered article, vitreous silica sintering system Product, it is to use vitreous silica or quartz glass as raw material, through crushing, shaping, the system prepared by series of ceramic technique such as burning till Product, succeeded in developing at first by the U.S. in early 1960s and put into batch production.
Quartz-ceramics has cost low and high temperature refractoriness under load height, thermal coefficient of expansion is small, heat endurance is good, chemically-resistant The good characteristics such as aggressivity is good, dielectricity is high and resistance is big.Quartz-ceramics is because having extremely low thermal coefficient of expansion, its heat shock resistance Excellent performance, while have excellent chemical stability and extremely strong acid-resistant corrosion (insoluble in addition to hydrofluoric acid and hot sulfuric acid In other acid), therefore silica crucible is widely used in the smeltings such as various rare metals, noble metal, special glass and photovoltaic row In terms of the polycrystalline silicon ingot casting of industry.Especially in the silica crucible used in polycrystalline silicon ingot casting, because its size is big (1200*1200mm), wall Thin (about 20mm), manufacture difficulty is larger.Glass horizontal annealing furnace can be made with Quartz Ceramic Roller, float glass furnace flashboard Brick, Float Glass Annealing stove hollow roll, cast steel water nozzle, sheet metal strip heat-treatment furnace hollow roll, non-ferrous metal metallurgy are used The mouth of a river, stopper, chute, crucible, coke oven door, and tedge liner, glass industry orifice ring, revolving sleeve, stirring rod, material Basin, rotation pipe, radome etc., are widely used in spaceship, rocket, guided missile, radar, atomic energy, electronics, steel, refining The industrial circle such as burnt, non-ferrous metal and glass.
In existing crucible design, the bottom of most crucible internal walls is essentially all the small portion on same horizontal plane The bottom of the crucible internal walls divided is arranged to rough structure, and existing crucible has following ask when carrying out material control Topic:1st, in polycrystalline cast ingot, ingot furnace is most of to set top heater and side heater respectively at the top of it with sidepiece, makes The centre position temperature of the bottom for the crucible internal walls that must be placed in ingot furnace is relatively low, and the marginal position temperature of the bottom of crucible internal walls Degree is higher, i.e., the isothermal level of centre position dimpling is presented in its thermal field, the material of crucible of the bottom all on same horizontal plane Remaining degree is determined that this is allowed for when the silicon material in the centre position of crucible bottom also has remaining, crucible bottom by the thermal field of crucible The silicon material of the marginal position in portion has been changed, and then can not accurately control crucible bottom to have one layer of simple silicon material covering, to ensure Follow-up ingot quality;2nd, bottom is although being not easy of silicon material that the crucible of recess not flat structure enables to the region of depression Fall, beneficial to the follow-up long crystalline substance of silicon material, but it has situations below when carrying out material control:A generally speaking crucible bottom also It is that the remaining degree of its material is determined by the thermal field of crucible with a horizontal plane, this is allowed for when the centre of crucible bottom When the silicon material of position also has remaining, the silicon material of the marginal position of crucible bottom has been changed, and then can not accurately control crucible bottom There is one layer of simple silicon material covering, to ensure follow-up ingot quality;Because crucible is typically using made of mould, bottom is b Rough structure so that need corresponding formulation mould, cost is higher and process is more troublesome;3rd, it is once made in crucible Internal volume has just been fixed up, if the excessive waste that heating energy source is will result in when processing small article of its volume, And it is not easy to operate.If its volume is too small cannot to be used for Large Parts Machining article.
Mostly use two kinds of techniques at present:Grouting process and gel-casting.Grouting process belongs to traditional handicraft, and it has as follows Feature:Technical maturity;Structure is uneven;Green strength is low;Density is higher;Yield rate low cost is high.Day can not increasingly be met Become the casting ingot process requirement of development.Gel-casting is technique emerging in recent years, and its feature is:Green strength is high;Structure is equal It is even;It is adapted to make large scale crucible;But its density is low, complex process, cost are higher.As the raising of casting ingot process is to crucible purity It is required that the increasingly harsh, reduction of crucible cost also constantly proposes new requirement, grouting process and gel-casting all can not once into The high-purity composite crucible of type, cost pressure also increasingly increase.Therefore, it is badly in need of a kind of brand-new technique to meet that crucible technique is simple, low Cost, high-purity, high density, even structure crucible come meet ingot casting market continuous development the needs of.
Utility model content
The purpose of this utility model is, overcomes defect present in prior art, there is provided it is a kind of it is simple in construction, using just It is prompt, volume size is variable, inexpensive, high-purity, high density, quartz ceramic crucible inner surface is smooth, is not easy sizing, is easy to clean Knot, the crucible of structure uniform inner variable volume.
To achieve the above object, the technical solution of the utility model is a kind of variable crucible of internal capacity of design, described Crucible includes crucible basal layer, increases layer at least provided with one layer on the basal layer, the basal layer is with increasing layer and increasing Layer and increasing is mutually linked by ladder buckle structure between layer, is located at upper interface position in basal layer and the outer surface for increasing layer Uniform projection provided with bulge loop or in a ring, fit sealing annular element, fit sealing annular are provided with the bulge loop or projection Part is used for basal layer and increases layer and increase layer and increase and fix between layer and seal.
It is sleeved on securely for the ease of fit sealing annular element and basal layer and increases layer, or is increased layer and increase between layer Interface, and will not rotate, preferable technical scheme is, the basal layer and increase layer outer surface be provided with it is vertical Fin and/or groove, be provided with the inside of the fit sealing annular element groove that is adapted with fin and/or groove and/or Fin.
For the ease of the processing and fabricating of crucible, preferable technical scheme also has, and the basal layer is in the section for increasing layer Trapezoidal barrel-like structure.
For the ease of the use of crucible, suitable for the different types of article of skilled worker, further preferred technical scheme also has, The basal layer, increase layer and the rounded barrel-like structure of fit sealing annular element, or oval barrel-like structure, or rectangular-shape barrel Shape structure.
For the ease of the processing and fabricating of crucible, further preferred technical scheme also has, and the basal layer, increases layer and tight After admittedly sealing annular element is mixed by tekite sand with binding agent, it is molded using former, then be made up of sintering process.
In order to improve the automatization level for doing manufacturing process, the production efficiency of crucible is improved, improves the shaping matter of crucible Amount, the arbitrarily thickness of regulation crucible internal walls layer and outer wall layer can be reached, further preferred technical scheme also has, the shaping Equipment is shaping spraying equipment, and shaping spraying equipment carries out circulation spraying by mechanical arm on mould inner wall, set until reaching Determine the basal layer of wall thickness, increase layer and fit sealing annular element.
In order to improve the quality of crucible internal walls layer, while and can reduces the manufacturing cost of crucible, further preferred technology Scheme also has, the outer layer that the basal layer is made up of with increasing layer to include the tekite sand of ordinary purity, and by high-purity And/or the internal layer that the tekite sand of ultra-high purity is formed.
In order to improve the quality of crucible internal walls layer, while and can reduces the manufacturing cost of crucible, further preferred technology Scheme also has, and the internal layer includes the middle internal layer being made up of the tekite sand of high-purity and the vitreous silica by ultra-high purity The appearance internal layer that sand is formed.
In order to improve the quality of crucible internal walls layer, while and can reduces the manufacturing cost of crucible, further preferred technology Scheme also has, and the tekite sand purity of the ordinary purity is 99.9%, and the tekite sand purity of high-purity is 99.995%, the tekite sand purity of ultra-high purity is 99.9999%.
In order to improve the quality of crucible, while and can reduces the manufacturing cost of crucible, and further preferred technical scheme is also Have, the basal layer and the wall thickness sum for increasing layer are 18mm~22mm.
The advantages of the utility model and beneficial effect are:The variable crucible of the outstanding internal capacity have it is simple in construction, make With it is convenient, volume size is variable, inexpensive, high-purity, high density, quartz ceramic crucible inner surface is smooth, be not easy sizing, easily The features such as cleaning is tied, structure is uniform.The crucible is suitably applied in the manufacturing of large size, thin walled crucible, can meet to require increasingly severe The requirement of the polycrystalline cast ingot industry at quarter.The crucible is to carry out rational grain size distribution simultaneously on the basis of different purity quartz raw material Quartzy slurry is made, spray parameters can be optimized, forms simple a set of technique, efficiency high, the cycle is short, cost is low, structure Uniformly, density height, purity and the 3D-FGM printing techniques of the free transition of material gradient.
Brief description of the drawings
Fig. 1 is the main cross section structure diagram of the variable crucible of the utility model internal capacity;
Fig. 2 is the main structure diagram of the variable crucible of the utility model internal capacity;
Fig. 3 is one of variable overlooking the structure diagram of crucible of the utility model internal capacity;
Fig. 4 is the two of the overlooking the structure diagram of the variable crucible of the utility model internal capacity.
In figure:1st, basal layer;2nd, layer is increased;3rd, ladder buckle structure;4th, bulge loop;5th, fit sealing annular element;6th, groove; 7th, outer layer;8th, middle internal layer;9th, appearance internal layer.
Embodiment
With reference to the accompanying drawings and examples, specific embodiment of the present utility model is further described.Implement below Example is only used for clearly illustrating the technical solution of the utility model, and can not limit protection model of the present utility model with this Enclose.
As shown in figures 1-4, the utility model is a kind of variable crucible of internal capacity, and the crucible includes the base of crucible Plinth layer 1, increase layer 2 at least provided with one layer on the basal layer 1, the basal layer 1 is with increasing layer 2 and increasing layer 2 with increasing It is mutually linked between layer 2 by ladder buckle structure 3, being located at upper interface position with increasing the outer surface of layer 2 in basal layer 1 is provided with Bulge loop 4 or projection uniform in a ring, fit sealing annular element 5, fit sealing annular element are provided with the bulge loop 4 or projection 5 are used for basal layer 1 and increase layer 2 and increase layer 2 and increase and fix between layer 2 and seal.
Basal layer 1 is sleeved on securely for the ease of fit sealing annular element 5 and increases layer 2, or is increased layer 2 and increased layer Interface between 2, and will not rotate, the utility model preferred embodiment is in the basal layer 1 and to increase layer 2 outer surface is provided with vertical fin and/or groove 6, is provided with and fin and/or recessed in the inside of the fit sealing annular element 5 The groove and/or fin that groove 6 is adapted.
For the ease of the processing and fabricating of crucible, the utility model preferred embodiment also has, and the basal layer 1 is with increasing The trapezoidal barrel-like structure in section of layer 2.
For the ease of the use of crucible, suitable for the different types of article of skilled worker, the further preferred reality of the utility model The scheme of applying also has, and the basal layer 1, increases 5 rounded barrel-like structure of layer 2 and fit sealing annular element, or oval tubbiness Structure, or rectangle barrel-like structure.
For the ease of the processing and fabricating of crucible, the utility model further preferred embodiment also has, the basal layer 1st, increase layer 2 and after fit sealing annular element 5 mixes by tekite sand with binding agent, be molded using former, then pass through Sintering process is made.
In order to improve the automatization level for doing manufacturing process, the production efficiency of crucible is improved, improves the shaping matter of crucible Amount, the arbitrarily thickness of regulation crucible internal walls layer and outer wall layer can be reached, the utility model further preferred embodiment is also Having, the former is shaping spraying equipment, and shaping spraying equipment carries out circulation spraying by mechanical arm on mould inner wall, Until reach the basal layer 1 of setting wall thickness, increase layer 2 and fit sealing annular element 5.
In order to improve the quality of crucible internal walls layer, while and can reduces the manufacturing cost of crucible, and the utility model is further Preferred embodiment also has, the outer layer 7 that the basal layer 1 is made up of with increasing layer 2 to include the tekite sand of ordinary purity, And the internal layer being made up of the tekite sand of high-purity and/or ultra-high purity.
In order to improve the quality of crucible internal walls layer, while and can reduces the manufacturing cost of crucible, and the utility model is further Preferred embodiment also has, and the internal layer includes the middle internal layer 8 being made up of the tekite sand of high-purity and by ultra-pure The appearance internal layer 9 that the tekite sand of degree is formed.
In order to improve the quality of crucible internal walls layer, while and can reduces the manufacturing cost of crucible, and the utility model is further Preferred embodiment also has, and the tekite sand purity of the ordinary purity is 99.9%, and the tekite sand of high-purity is pure Spend for 99.995%, the tekite sand purity of ultra-high purity is 99.9999%.
In order to improve the quality of crucible, while and can reduces the manufacturing cost of crucible, and the utility model is further preferred Embodiment also has, and the basal layer 1 and the wall thickness sum for increasing layer 2 are 18mm~22mm.
The basal layer of the variable crucible of the utility model internal capacity can be used alone, can when if desired increasing volume Increase layer on basal layer, fit sealing annular element be then sleeved on basal layer with adding the interface position of high-level external, If volume needs to continue to add again during increase to increase layer, the volume of crucible can be increased several times by that analogy, can also made With the basal layer of minimum.
Described above is only preferred embodiment of the present utility model, it is noted that for the common skill of the art For art personnel, on the premise of the utility model technical principle is not departed from, some improvements and modifications can also be made, these change Enter and retouch and also should be regarded as the scope of protection of the utility model.

Claims (10)

1. the variable crucible of a kind of internal capacity, it is characterised in that the crucible includes crucible basal layer, on the basal layer Increase layer at least provided with one layer, the basal layer and increase layer and increase layer and increase mutual by ladder buckle structure between layer Linking, it is located at upper interface position in basal layer and the outer surface for increasing layer and is provided with bulge loop or projection uniform in a ring, described Bulge loop or projection are provided with fit sealing annular element, and fit sealing annular element is used for basal layer with increasing layer and increasing layer with adding Fix and seal between high level.
2. the variable crucible of internal capacity as claimed in claim 1, it is characterised in that in the basal layer and increase the outer of layer Surface is provided with vertical fin, and the groove being adapted with fin is provided with the inside of the fit sealing annular element;Or described Basal layer is provided with vertical groove with increasing the outer surface of layer, is provided with the inside of the fit sealing annular element and is adapted with groove Fin.
3. the variable crucible of internal capacity as claimed in claim 2, it is characterised in that the basal layer and the section for increasing layer Trapezoidal barrel-like structure.
4. the variable crucible of internal capacity as claimed in claim 3, it is characterised in that the basal layer, increase layer and fastening Seal the rounded barrel-like structure of annular element, or oval barrel-like structure, or rectangle barrel-like structure.
5. the variable crucible of internal capacity as claimed in claim 4, it is characterised in that the basal layer, increase layer and fastening After sealing annular element is mixed by tekite sand with binding agent, it is molded using former, then be made up of sintering process.
6. the variable crucible of internal capacity as claimed in claim 5, it is characterised in that the former sets for shaping spraying Standby, shaping spraying equipment carries out circulation spraying by mechanical arm on mould inner wall, until reaching the basal layer of setting wall thickness, adding High-rise and fit sealing annular element.
7. the variable crucible of internal capacity as claimed in claim 6, it is characterised in that the basal layer and increase layer include by The outer layer that the tekite sand of ordinary purity is formed, and by any one in the tekite sand of high-purity or ultra-high purity Or the internal layer of a variety of compositions.
8. the variable crucible of internal capacity as claimed in claim 7, it is characterised in that the internal layer is included by the molten of high-purity The middle internal layer of fused silica sand composition and the appearance internal layer being made up of the tekite sand of ultra-high purity.
9. the variable crucible of internal capacity as claimed in claim 7, it is characterised in that the tekite sand of the ordinary purity Purity is 99.9%, and the tekite sand purity of high-purity is 99.995%, and the tekite sand purity of ultra-high purity is 99.9999%.
10. the variable crucible of internal capacity as in one of claimed in any of claims 1 to 9, it is characterised in that the basal layer Wall thickness sum with increasing layer is 18mm~22mm.
CN201720263741.8U 2017-03-17 2017-03-17 A kind of variable crucible of internal capacity Active CN207159416U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108514902A (en) * 2018-04-10 2018-09-11 东海县太阳光新能源有限公司 A kind of quartz multilayer segmented crucible
CN110560191A (en) * 2018-12-11 2019-12-13 中国航空工业集团公司北京长城计量测试技术研究所 High-temperature eutectic point crucible with dynamically-variable volume

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108514902A (en) * 2018-04-10 2018-09-11 东海县太阳光新能源有限公司 A kind of quartz multilayer segmented crucible
CN110560191A (en) * 2018-12-11 2019-12-13 中国航空工业集团公司北京长城计量测试技术研究所 High-temperature eutectic point crucible with dynamically-variable volume

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