CN207082008U - A kind of control system of micro-reactor apparatus - Google Patents

Abstract

The utility model discloses a kind of control system of micro-reactor apparatus, including：Harvester, interactive device and controller；Wherein, the harvester, for gathering the field data of the micro-reactor apparatus；The interactive device, for receiving the configuration information to the micro-reactor apparatus；The controller, for according to the field data collected, and/or the configuration information received, control signal is generated, to be controlled at least one of the raw material input process of the micro-reactor apparatus, flow control process, temperature controlled processes, line clear process, output of products process, security protection detection process.Scheme of the present utility model, it can overcome and control the defects of difficulty is big, function is few and security is poor in the prior art, realize the beneficial effect that control difficulty is small, function is more and security is good.

Description

A kind of control system of micro-reactor apparatus

Technical field

The utility model belongs to micro-reacting tcchnology field, and in particular to a kind of control system of micro-reactor apparatus, especially relates to A kind of and electric control system of microreactor.

Background technology

Micro-reactor apparatus (such as：Microreactor, micro passage reaction etc.), be it is a kind of by means of special micro-processing, With solid matrix manufacture available for the three-dimensional structure element to be chemically reacted.In micro-reactor apparatus, usually contain size compared with Small (such as：Equivalent diameter is less than 500 μm), the small passage of various informative property, fluid flows in these passages, and requires at this Required reaction occurs in a little passages, which results in have in the chemical device of micro-structure very big surface area/ Volume ratio.

The micro-reactor apparatus set by modularization, it is possible to achieve micro-reacting tcchnology, i.e.,：Make necessary Essential Chemistry engineering Operate the technology being carried out, such as mixing, reaction, heat exchange and the operation more implemented by micro-structural mode.Due to micro- Fine feature of the consersion unit in terms of micro-structure so that the precision that is controlled in micro-reacting tcchnology to micro-reactor apparatus and The requirements such as stability are higher, to be more accurately controlled to the chemical reaction process based on micro-reacting tcchnology.

In current micro-reacting tcchnology, the function being controlled to micro-reactor apparatus is few, such as：Long-range control can not be realized System, on-line checking and the control such as monitoring in real time, are unfavorable for operating personnel and chemical reaction process are preferably monitored.

It can be seen that in existing micro-reacting tcchnology, the defects of control difficulty is big, function is few and security is poor be present.

Utility model content

The purpose of this utility model is, for drawbacks described above, there is provided a kind of control system of micro-reactor apparatus, to solve The problem of remote control, on-line checking and the control such as monitoring in real time cause to control difficulty big can not be realized in the prior art, reached Reduce the effect of control difficulty.

The utility model provides a kind of control system of micro-reactor apparatus, including：Harvester, interactive device and control Device；Wherein, the harvester, for gathering the field data of the micro-reactor apparatus；The interactive device, for reception pair The configuration information of the micro-reactor apparatus；The controller, for according to the field data that collects, and/or receiving The configuration information, generate control signal, with raw material input process, flow control process, the temperature to the micro-reactor apparatus At least one of degree control process, line clear process, output of products process, security protection detection process are controlled.

Alternatively, wherein, the field data, including：Flow, temperature, pressure, liquid level, weight, live video information, At least one of status information；And/or the configuration information, including：Production requirement, raw material parameter, target flow, target At least one of temperature, target level, cleaning parameter, security protection parameter.

Alternatively, in addition to：Performs device；The performs device, under the control of said control signal to described Raw material input process, the flow control process, the temperature controlled processes, the line clear process, the output of products The control of at least one of process, the security protection detection process.

Alternatively, the performs device, including：In servo-drive system, heat-exchange system, cleaning systems, control valve at least it One；Wherein, the servo-drive system, for the raw material input flow rate and/or output of products stream by controlling the micro-reactor apparatus Amount, realizes the control to the flow control process；The heat-exchange system, for by controlling cold medium flux, realizing to described The control of temperature controlled processes；The cleaning systems, for by controlling cleaning mode, realizing to the line clear process Control；The control valve, it is auxiliary for entering at least one of the servo-drive system, the heat-exchange system, the cleaning systems Help control.

Alternatively, the harvester, including：Flow sensor, temperature sensor, pressure sensor, liquid level sensor, At least one of weight sensor, video acquisition system；Wherein, the flow sensor, set for gathering micro- reaction At least one of standby raw material input flow rate, output of products flow；The temperature sensor, set for gathering micro- reaction At least one of standby reaction temperature, refrigerant temperature of heat-exchange system；The pressure sensor, for gathering micro- reaction In the base pressure of the raw material input pod of equipment, the loine pressure of reaction channel, the base pressure of output of products container extremely It is one of few；The liquid level sensor, the liquid level of the raw material input pod for gathering the micro-reactor apparatus, Jie of reaction channel At least one of matter liquid level, liquid level of output of products container；The weight sensor, for gathering the micro-reactor apparatus At least one of raw material input weight, output of products weight；The video acquisition system, for gathering the micro-reactor apparatus Live video information and at least one of status information.

Alternatively, the harvester, in addition to：Analogue collection module；The analogue collection module, for adopting The field data collected carries out the processing of at least one of data conversion, signal filtering；And/or the controller, bag Include：At least one of industrial computer, single-chip microcomputer, DSP Processor, PLC.

Alternatively, in addition to：Memory cell；The memory cell, for store the micro-reactor apparatus raw material into Divide the corresponding relation with density；And/or the interactive device, it is additionally operable to the field data collected, the institute received At least one of configuration information is stated to be shown；And/or export prompt message during the security protection detection.

Alternatively, the interactive device, including：In first display unit, the second display unit, Tip element at least it One；First display unit, for receiving the configuration information to the micro-reactor apparatus；And/or described second is aobvious single Member, for being shown at least one of the field data collected, the configuration information received；And/or The Tip element, for initiating the prompt message of at least one of voice, acousto-optic form.

Alternatively, the interactive device, in addition to：Analog input mModule, analog output module, I/O input and output At least one of module；Wherein, the Analog input mModule, for also including the first display unit when the interactive device When, after the configuration information that is received to first display unit is changed, input to the controller；And/or institute Analog output module is stated, for when the system also includes performs device, simulation controlled quentity controlled variable to be exported to the performs device； And/or the I/O input/output modules, the switching value information sent for receiving the controller；And/or when the system also During including performs device, the on-off model is exported at least one of the interactive device, the performs device.

Scheme of the present utility model, by harvester, interactive device and controller (such as：Industrial computer) adaptation set Put, it is possible to achieve remote control, on-line checking and the control such as monitoring in real time, be advantageous to operating personnel and chemical reaction process is carried out Preferably monitor so that the control function of micro-reactor apparatus increases, and the control difficulty to micro-reactor apparatus greatly reduces.

Further, scheme of the present utility model, by performs device (such as：Servo-drive system, heat-exchange system and warning device Deng) and controller adaptation set, can preferably monitor chemical reaction process, once find chemical reaction process in occur it is different Often it can find and solve in time, advantageously ensure that personal security, pole is also able to the security that micro-reactor apparatus is controlled The big control security and hommization degree for being lifted and then lifting micro-reactor apparatus.

Thus, scheme of the present utility model, by harvester, interactive device and controller (such as：Industrial computer) it is suitable With setting, it is possible to achieve the various control function of micro-reactor apparatus (such as：Realize remote control, on-line checking and monitoring in real time Deng control), solution can not realize that remote control, on-line checking and the control such as monitoring in real time cause to control difficulty big in the prior art The problem of, so as to overcome and control the defects of difficulty is big, function is few and security is poor in the prior art, realization control difficulty is small, work( The beneficial effect that energy is more and security is good.

Other features and advantages of the utility model will illustrate in the following description, also, partly from specification In become apparent, or understood by implementing the utility model.

Below by drawings and examples, the technical solution of the utility model is described in further detail.

Brief description of the drawings

Fig. 1 is the structural representation of an embodiment of the control system of micro-reactor apparatus of the present utility model；

Fig. 2 is the structural representation of another embodiment of the control system of micro-reactor apparatus of the present utility model；

Fig. 3 is the structural representation of the another embodiment of the control system of micro-reactor apparatus of the present utility model；

Fig. 4 is the principle schematic of the embodiment that course of reaction controls in system of the present utility model；

Fig. 5 is the principle schematic of the embodiment that raw material input process controls in system of the present utility model；

Fig. 6 is the principle schematic of the embodiment that flow controls in system of the present utility model；

Fig. 7 is the principle schematic of a temperature controlled embodiment in system of the present utility model；

Fig. 8 is the principle schematic of an embodiment of line clear process control in system of the present utility model；

Fig. 9 is the principle schematic of an embodiment of the quantitative output procedure control of product in system of the present utility model.

With reference to accompanying drawing, reference is as follows in the utility model embodiment：

10- harvesters；11- flow sensors；12- temperature sensors；13- pressure sensors；14- liquid level sensors； 15- weight sensors；16- video acquisition systems；17- analogue collection modules；20- controllers；21- industrial computers；22- monolithics Machine；23-DSP processors；24-PLC controllers；30- interactive devices；The display units of 31- first；The display units of 32- second；33- Tip element；34- Analog input mModules；35- analog output modules；36-I/O input/output modules；40- performs devices； 41- servo-drive systems；42- heat-exchange systems；43- cleaning systems；44- control valves；50- memory cell.

Embodiment

It is specific below in conjunction with the utility model to make the purpose of this utility model, technical scheme and advantage clearer Technical solutions of the utility model are clearly and completely described for embodiment and corresponding accompanying drawing.Obviously, described embodiment Only it is the utility model part of the embodiment, rather than whole embodiments.Based on the embodiment in the utility model, this area The every other embodiment that those of ordinary skill is obtained under the premise of creative work is not made, belongs to the utility model The scope of protection.

According to embodiment of the present utility model, there is provided a kind of control system of micro-reactor apparatus, this practicality as shown in Figure 1 The structural representation of one embodiment of new system.The control system of the micro-reactor apparatus can include：Harvester 10, hand over Mutual device 30 and controller 20.

In an optional example, the harvester 10, it can be used for the field data for gathering the micro-reactor apparatus. Such as：The harvester 10, setting can be adapted to the micro-reactor apparatus.

Wherein, the field data, can include：Flow (such as：The raw material input flow rate of micro-reactor apparatus, micro- reaction Output of products flow of equipment etc.), temperature (such as：The reaction temperature of micro-reactor apparatus, refrigerant temperature of heat-exchange system 42 etc.), Pressure (such as：The base pressure of the accumulator of micro-reactor apparatus, loine pressure of the reaction channel of micro-reactor apparatus etc.), liquid level (such as：The medium liquid level of the accumulator of micro-reactor apparatus, the medium liquid level of the reaction channel of micro-reactor apparatus, micro-reactor apparatus The medium liquid level of output of products device etc.), weight (such as：The weight of the storage of raw materials, micro- reaction in the accumulator of micro-reactor apparatus Weight, the weight of output of products of micro-reactor apparatus etc. of the raw material input of equipment), live video information, status information (example Such as：At least one of there is the status information during fortuitous events such as liquid leakage, burning, blast in scene).

Such as：Status information, it can include：May be due to visible smog, flame, blast etc. caused by leakage accident etc. Visual physical phenomenon.

Alternatively, the harvester 10, can include：Flow sensor 11, temperature sensor 12, pressure sensor 13rd, at least one of liquid level sensor 14, weight sensor 15, video acquisition system 16.

In an optional specific example, the flow sensor 11, it can be used for the original for gathering the micro-reactor apparatus Expect at least one of input flow rate, output of products flow.

Such as：Flow sensor 11 can be used for detecting reaction medium flow velocity, and system detects according to flow sensor 11 Value of feedback, the rotating speed of each rate-of flow pump is adjusted in real time by pid control algorithm, to reach the accurate control to reaction medium ratio System.

Such as：The flow sensor 11, setting can be adapted to the flow pump, can be used for gathering the flow pump The feed flow of the raw material is conveyed to the micro-reactor apparatus.

Such as：The flow sensor 11, it can be used for the current media flow for gathering the reaction channel.

In an optional specific example, the temperature sensor 12, it can be used for gathering the anti-of the micro-reactor apparatus Answer temperature, at least one of the refrigerant temperature of heat-exchange system 42.

Such as：Temperature sensor 12 can be used for detecting each several part temperature, and system is according to the value of feedback of temperature sensor 12 And setting value, the cold medium flux of heat-exchange system 42 is controlled in real time by pid control algorithm, so as to accurately control each reaction medium The temperature of input temp and course of reaction, to reach stable course of reaction, ensure the purpose of product quality.

Such as：The temperature sensor 12, it can be used for the current reaction of reaction channel for gathering the micro-reactor apparatus Temperature.

In an optional specific example, the pressure sensor 13, it can be used for the original for gathering the micro-reactor apparatus Expect at least one of base pressure, the loine pressure of reaction channel, the base pressure of output of products container of input pod.

More alternatively, in raw material input process, the pressure sensor 13, can be adapted to be arranged at it is described it is micro- reaction set The bottom of standby accumulator, it can be used for gathering the pressure that the storage of raw materials applies to the accumulator bottom in the accumulator.

Such as：In raw material input process, the pressure sensor 13, adaptation is arranged at the bottom of the input product container Portion, it can be used for the current pressure for gathering the input product container bottom.

More alternatively, during security protection detection, the pressure sensor 13, it can be also used for gathering micro- reaction and set The loine pressure of standby reaction channel.

Such as：Pressure sensor 13 can be used for detecting reaction channel and accumulator pressure, pass through the pressure of diverse location Sensor 13 detects valve system and is used for medium in calculation medium weight or the blocking of detection reaction channel and passage whether there is, and passes through measurement Value and all kinds of threshold values of system relatively control and protected course of reaction, avoid liquid leakage, line clogging accident generation simultaneously It can also avoid wriggling without medium in flow pump body and may cause the generation of diaphragm damage accident.

In an optional specific example, the liquid level sensor 14, it can be used for the original for gathering the micro-reactor apparatus Expect at least one of liquid level, the medium liquid level of reaction channel, the liquid level of output of products container of input pod.

Such as：Liquid level sensor 14 can be used for detecting liquid level, system according to the detection signal of liquid level sensor 14, Can interpolate that input medium and whether transfinite, output medium whether store transfinite and production process in the storage of some accessory substances Whether medium transfinites, may so as to avoid each quality accident and danger medium caused by each storage medium transfinites spilling from overflowing The danger brought.

Such as：During security protection detection, the liquid level sensor 14, it can be also used for gathering the micro-reactor apparatus At least one of the liquid level of raw material input pod, the medium liquid level of reaction channel, liquid level of output of products container.

In an optional specific example, the weight sensor 15, it can be used for the original for gathering the micro-reactor apparatus Expect at least one of input weight, output of products weight.

Such as：The weighing sensor, the input product container that can be used for gathering the micro-reactor apparatus it is current defeated Go out product weight.

Such as：The weighing sensor, it can be used for the current production output quantity for gathering the micro-reactor apparatus.

In an optional specific example, the video acquisition system 16, it can be used for gathering the micro-reactor apparatus At least one of live video information and status information.

Such as：Video acquisition system 16, it can be used for obtaining and transmitting working site video information, monitor various kinds of equipment The generation of the unusual condition such as state of appearance and gas, liquid leakage, burning, blast.

Such as：The video acquisition system 16, the reaction scene for being arranged at the micro-reactor apparatus, Ke Yiyong can be adapted to In the live video information and status information that gather the reaction scene.

Thus, by the sensor of diversified forms, much information can be obtained, is advantageous to lifting and micro-reactor apparatus is controlled Convenience and reliability.

Alternatively, the harvester 10, can also include：Analogue collection module 17.

In an optional specific example, the analogue collection module 17, it can be used for the scene to collecting Information progress data conversion (such as：Analog-to-digital conversion), signal filtering at least one of processing.

Such as：Analogue collection module 17, it can be used for receiving temperature sensor 12, pressure sensor 13, flow sensing The detection signal of the grade of device 11, system (such as：The system that controller 20 controls) according to the analog signalses of collection be converted to numeral Signal is simultaneously shown, while can do different reactions automatically according to the actual valve system of unlike signal, so as to realize system Automated closed-loop control requirement.

Such as：The analogue collection module 17, setting also is adapted to the controller 20, can be used for working as the collection When device 10 can include video acquisition system 16, modulus is carried out at least one of the reaction information, the field data After conversion, at least one of signal filtering are handled, transmit to the controller 20.

Thus, can be to the gathered data of each sensor by being adapted to the analog acquisition device set with each sensor It is further processed, is advantageous to improve the accuracy and security of controller control.

In an optional example, the interactive device 30, it can be used for receiving the setting letter to the micro-reactor apparatus Breath.

Wherein, the configuration information, can include：Production requirement, raw material parameter (such as：The composition of raw material to be entered, match somebody with somebody When quality), target flow, target temperature, target level, cleaning parameter, at least one of security protection parameter.

In an optional example, the interactive device 30, can be also used for collect the field data, reception To at least one of the configuration information shown；And/or export prompt message during the security protection detection. Such as：The interactive device 30, setting can be adapted to the micro-reactor apparatus.

Alternatively, the interactive device 30, can include：First display unit 31, the second display unit 32, Tip element At least one of 33.

Wherein, the display processing of the first display unit 31 and the display processing of the second display unit 32, can be aobvious at one Show and completed on unit, can also be completed on two display units.

In an optional specific example, first display unit 31, it can be used for receiving to the micro-reactor apparatus The configuration information.

More alternatively, in raw material input process, first display unit 31, it can be used for setting micro- reaction and set The composition of standby raw material to be entered, with when quality.

Such as：In raw material input process, first display unit 31, can be also used for setting the raw material into Divide, the velocity of medium of proportioning and the raw material in the reaction channel of the micro-reactor apparatus.

Such as：In raw material input process, first display unit 31, it can be also used for setting the micro-reactor apparatus To the production requirement of its input product container.

More alternatively, in temperature controlled processes, first display unit 31, can be also used for setting micro- reaction The goal response temperature of the reaction channel of equipment, and/or the target refrigerant temperature of the heat-exchange system 42.

Such as：In temperature controlled processes and/or flow control process, first display unit 31, it can be also used for Set at least one of setting reaction temperature, setting rate-of flow of the reaction channel of the micro-reactor apparatus.

More alternatively, during line clear, first display unit 31, can be also used for setting micro- reaction The line clear parameter of equipment.

More alternatively, during security protection detection, first display unit 31, can be also used for：Set described micro- anti- The set information at the reaction scene of equipment, and/or the stop condition of the course of reaction of the setting micro-reactor apparatus are answered, and/or Set the theoretical field data, and the setting loine pressure, the reaction temperature, the medium liquid level is respective described At least one of setting value.

More alternatively, during output of products, first display unit 31, can be also used for setting micro- reaction The setting output products weight of the product input pod of equipment.

Such as：First display unit 31, it can be used for the theoretical output of products amount for setting the micro-reactor apparatus.

Such as：First display unit 31 can include touch screen.

In an optional specific example, second display unit 32, it can be used for the scene letter to collecting At least one of described configuration information cease, received is shown.

Such as：Second display unit 32, it can be used for when the interactive device 30 can include video acquisition system 16, Show at least one of live video information and status information that the video acquisition system 16 collects.

Such as：Second display unit 32, it is displayed for the field data of the micro-reactor apparatus.

Such as：Second display unit 32 can include monitor screen.

In an optional specific example, the Tip element 33, it can be used for initiating at least one of voice, acousto-optic The prompt message of form.

Such as：In security protection detection control process, Tip element 33, it can be used for when fortuitous event, such as liquid occurs in scene During the generation of situations such as body leakage, burning, blast, under the control of controller 20, (example is prompted in time according to video processing results Such as：Operating personnel are notified according to video processing results and alarm and the very first time) so that operating personnel can be according to not sympathizing with Condition takes different processing schemes.

Such as：Tip element 33, it can include：Alarm.The alarm, it can be used for the control in the controller 20 System is lower to initiate prompting or alarm.Such as：It the alarm, can be used under the control of the controller 20, initiate acousto-optic, language At least one alarm of sound.

Thus, by the interactive device of diversified forms, convenience and the flexibility of man-machine interaction can be improved.

Alternatively, the interactive device 30, can also include：Analog input mModule 34, analog output module 35, I/ At least one of O input/output modules 36.

In an optional specific example, the Analog input mModule 34, it can be used for when the interactive device 30 may be used also It is defeated after the configuration information that is received to first display unit 31 is changed during with including the first display unit 31 Enter to the controller 20.

Such as：The Analog input mModule 34, it can be used for when the performs device 40 can include servo-drive system 41 When, setting is adapted to the servo-drive system 41, can be used for providing Setting signal for the servo-drive system 41.

In an optional specific example, the analog output module 35, it can be used for when the system can also include During performs device 40, simulation controlled quentity controlled variable is exported to the performs device 40.

Such as：The analog output module 35, into servo-drive system 41, heat-exchange system 42, cleaning systems 43 at least One of the corresponding simulation controlled quentity controlled variable of output.

Such as：Analog output module 35, it can be used for providing Setting signal, the basis of servo-drive system 41 for servo-drive system 41 The given signal of analog output module 35 is handled and is converted into the tach signal of flow pump and is controlled.

Such as：The analog output module 35, it can be used for the proportional flow control valve to heat-exchange system, output and setting The analog quantity temperature control amount of target refrigerant temperature adaptation.

In an optional specific example, the I/O input/output modules 36, it can be used for receiving the controller 20 and send out The switching value information gone out.And/or when the system can also include performs device 40, to the interactive device 30, the execution At least one of device 40 exports the on-off model.

Such as：I/O input/output modules 36, can be used for exporting and/or receive control valve 44 (such as：Button, magnetic valve Deng), interactive device 30 (such as：Tip element 33 can be including indicator lamp etc.), harvester 10 (such as：Liquid level sensor 14 Deng) etc. all kinds of on-off models, system judge according to all kinds of on-off models and export different working conditions.

Such as：The I/O input/output modules 36, when the system can include performs device 40, respectively with the control The adaptation connection of at least one of device 20, the performs device 40 and described harvester 10 processed, can be used for exporting and/or receives The on-off model being adapted to at least one of the controller 20, the performs device 40 and the harvester 10.

Thus, by being adapted to the data-processing interface set with a variety of interactive devices, data interaction and processing can be lifted Reliability and security, and property easy to use is good.

In an optional example, the controller 20, can be used for according to the field data that collects, and/or The configuration information received, control signal is generated, was controlled with the raw material input process to the micro-reactor apparatus, flow At least one of journey, temperature controlled processes, line clear process, output of products process, security protection detection process are controlled.Example Such as：The controller 20, setting can be adapted to the harvester 10 and the interactive device 30 respectively.

Alternatively, the controller 20, can include：Industrial computer 21, single-chip microcomputer 22, DSP Processor 23, PLC At least one of 24.

Thus, by the controller of diversified forms, flexibility and the versatility of control can be lifted.

In an optional specific example, raw material input process, it can include：The controller 20, can be used for basis The pressure, the composition, the proportioning and the quality, determine whether the input quantity of the raw material reaches default demand Amount.And when the input quantity reaches the demand, stop input of the raw material to the micro-reactor apparatus；Or work as When the input quantity is not up to the demand, continue input of the raw material to the micro-reactor apparatus.

Wherein, the controller 20 determines whether the input quantity of the raw material reaches default demand, can specifically wrap Include：According to the composition of the raw material, determine the raw material memory cell (such as：Database) it is corresponding with the composition close in 50 Degree.And the density according to the pressure of the raw material, the shape of the accumulator and the raw material, determine the accumulator The current weight of the middle storage of raw materials；And/or institute needed for the micro-reactor apparatus is determined with when quality according to the raw material State the target weight of raw material.

Further, controller 20 determines the current weight of the raw material and the first difference of target weight, if reaches During the first predetermined threshold value, determine that the input quantity reaches the demand；Or to be not up to described first pre- when first difference If during threshold value, determine that the input quantity is not up to the demand.

More alternatively, in raw material input process, can also include：The controller 20, it can be also used for according to The composition of raw material, with when velocity of medium, determine the simulation controlled quentity controlled variable needed for the servo-drive system 41.

More alternatively, in raw material input process, can also include：The controller 20 determines the institute of servo-drive system 41 The simulation controlled quentity controlled variable needed, can specifically include：According to the raw material with when velocity of medium, each composition in the raw material is determined Mass flow；And the composition according to the raw material, determine corresponding with the composition close in the raw material memory cell 50 Degree；And density and mass flow according to each composition in the raw material, determine the volume flow of each composition in the raw material.

More alternatively, in raw material input process, can also include：The controller 20, it can be also used for according to The shape of current pressure and the input product container, determine whether the product weight to be output in the input product container is full The production requirement set enough.When the output products weight is unsatisfactory for the production requirement, the output products weight is determined When being unsatisfactory for production requirement, by the alarm, alarm is initiated, to remind operating personnel to adjust in the input product container Product weight to be output.

More alternatively, when control valve 44 can also include raw material transfer valve, the controller 20, can be also used for out The raw material transfer valve is opened, to input the raw material to the micro-reactor apparatus.Or close the raw material transfer valve, with stop to The micro-reactor apparatus inputs the raw material.

In an optional specific example, flow control process, it can include：It is adapted to, also sets up with the controller 20 There is pid control module.The controller 20, it can be also used for inputting the rate-of flow to the pid control module, pass through The pid control module carries out flow correction to the rate-of flow, obtains revised analog quantity flow correction value；And The analog quantity flow correction value is inputted to the servo-drive system 41 again, makes the servo-drive system 41 drive the motor to turn It is dynamic, so circulation.

Such as：The controller 20, it can be also used for determining whether the current media flow meets the setting medium Flow.When the current media flow is unsatisfactory for the setting rate-of flow, pass through the servo-drive system 41, the flow pump With the motor, the current media flow of the reaction channel is adjusted.

In an optional specific example, in temperature controlled processes, it can include：The controller 20, can be also used for The heat-exchange system 42 is opened, until when the current refrigerant temperature of the heat-exchange system 42 reaches the target refrigerant temperature, is opened The micro-reactor apparatus is moved, and the analog quantity temperature control amount is exported by the analog output module 35, so that described Proportional flow valve events, the cold medium flux is controlled.

More alternatively, in temperature controlled processes, can also include：The controller 20, it can be also used for working as described Preceding reaction temperature is inputted to the pid control module, is carried out temperature adjustmemt by the pid control module, is obtained analog quantity temperature Spend correction value；And again by the analog output module 35, the analog quantity temperature corrected value is exported to the ratio Example flow valve, by controlling the cold medium flux that the current reaction temperature is adjusted, so to circulate.

Such as：Controller 20, it can be also used for determining whether the current reaction temperature meets the setting reaction temperature, When the current reaction temperature is unsatisfactory for the setting reaction temperature, by the heat-exchange system 42, it is logical to adjust the reaction The current reaction temperature in road.

In an optional specific example, during line clear, it can include：The controller 20, can also be used In when the course of reaction stops, it is determined whether needs clean to the micro-reactor apparatus.When needs are to described micro- anti- When answering the equipment to be cleaned, start the cleaning systems 43.

More alternatively, during line clear, can also include：The controller 20, it can be used for when described micro- anti- When answering the course of reaction of equipment to stop, according to the line clear parameter, start the switching equipment；And start the stream Pump is measured, the cleaning agent that the cleaning agent is stored in pipeline is pumped into the passage tube of the micro-reactor apparatus, with using described clear The clean dose of reaction channel to the micro-reactor apparatus carries out a line clear.

More alternatively, during line clear, can also include：It the controller 20, can be also used for that institute ought be used When stating cleaning agent and carrying out a line clear to the reaction channel of the micro-reactor apparatus and finish, it is determined whether need to carry out gas Cleaning, to be again started up the switching equipment when needing to carry out gas cleaning.

In an optional specific example, during security protection detection, it can include：Controller 20, can be used for basis The live video information and status information for the micro-reactor apparatus that second display unit 32 monitors, using appropriate video signal transacting Algorithm Analysis video.When fortuitous event occurs in scene, during generation such as situations such as liquid leakage, burning, blast, at video The prompting in time of reason result notice interactive device 30 (such as：According to video processing results and alarm and very first time notice operation Personnel) so that operating personnel can take different processing schemes according to different situations.

More alternatively, during security protection detection, can also include：The controller 20, can be also used for described in determination Whether live video information and/or status information meet set information, when the live video information and/or status information are discontented with During the foot set information, the alarm is initiated by the alarm.

Wherein, the live video information and/or status information are unsatisfactory for the set information, can include：It is described micro- The raw material leakage at the reaction scene of consersion unit, poison gas is exceeded, ambient temperature and humidity is at least one of abnormal.

More alternatively, during security protection detection, can also include：The controller 20, it can be also used for when described existing When field video information and/or status information meet the set information, start the course of reaction of the micro-reactor apparatus, and determine Whether at least one of described loine pressure, the rate-of flow, the reaction temperature in the course of reaction reach respective Setting value；And when at least one of the loine pressure in the course of reaction, rate-of flow, reaction temperature do not reach When reaching the stop condition to the respective setting value, and/or the course of reaction, stop the course of reaction.

Wherein, the live video information and/or status information are unsatisfactory for the set information, can also include：It is described It is each to be not up to its at least one of the loine pressure of medium, the reaction temperature, described medium liquid level in micro-reactor apparatus From the setting value.

In an optional specific example, during output of products, it can also include：The controller 20, can be with For determining whether the current output products weight reaches the setting output products weight.When the current output products weight When amount is not up to the setting output products weight, the output of products valve and the plunger device are controlled, to the input product The output of products amount of container is adjusted.

Such as：The controller 20, it can be also used for determining the current production output quantity and the setting output of products Second difference of amount, if reach the second predetermined threshold value, institute is closed when second difference reaches second predetermined threshold value State output of products valve.

Such as：The controller 20, it can be used for the valve port mouth for by the plunger device, adjusting the output of products valve Footpath, to carry out adaptation regulation to the current production output quantity.

Such as：The controller 20, it can be also used for setting when the product input quantity of an output of products container reaches When determining output products weight, the defeated pipeline of the product of the micro-reactor apparatus is switched into next output of products container, after Continue the quantitative output control of next product.

Thus, controlled, can be lifted to micro-reactor apparatus based on the adaptation of harvester and interactive device by controller The reliability and security of control, control difficulty substantially reduce.

In an optional embodiment, it can also include：Performs device 40, it may refer to the example shown in Fig. 2.Example Such as：The performs device 40, setting can be adapted to the controller 20, it is right under the control of said control signal to can be used for The raw material input process, the flow control process, the temperature controlled processes, the line clear process, the product The control of at least one of output procedure, the security protection detection process.

In an optional example, the performs device 40, it can be used for entering action under the control of the controller 20 Make, to realize to the raw material input process, the flow control process, the temperature controlled processes, the line clear mistake The control of at least one of journey, the output of products process, the security protection detection process.

Alternatively, the performs device 40, can include：Servo-drive system 41, heat-exchange system 42, cleaning systems 43, control At least one of valve 44.

In an optional specific example, the servo-drive system 41, it can be used for by controlling the micro-reactor apparatus Raw material input flow rate and/or output of products flow, realize the control to the flow control process.

Such as：Servo-drive system 41 can be used for accurate control flow rate, the amount given according to system and flow The actual value that sensor 11 feeds back, each channel media real-time traffic is accurately controlled by PID control.

Such as：With servo-drive system 41, also adaptation is provided with motor and flow pump.In raw material input process, the servo System 41 is adapted to setting with the motor, can be used for the running speed for by the simulation controlled quentity controlled variable, being converted to the motor, with The motor is driven to rotate.The motor is adapted to setting with the flow pump, can be used for rotating with the running speed, with band The dynamic flow pump action.The flow pump is adapted to setting with the micro-reactor apparatus, can be used for the micro-reactor apparatus Reaction channel convey the raw material.

Such as：The servo-drive system 41, setting is adapted to the flow pump, can be used for the control in the controller 20 Under, control being turned on and off for the flow pump.The flow pump, it can be used for controlling the unlatching of the course of reaction or stop Only.

Such as：During raw material input process and/or output of products, the servo-drive system 41, fitted with the flow pump With setting, it can be used under the control of the controller 20, control being turned on and off for the flow pump.The flow pump, It can be used for the unlatching or stopping for controlling the course of reaction.

In an optional specific example, the heat-exchange system 42, it can be used for, by controlling cold medium flux, realizing to institute State the control of temperature controlled processes.Such as：The heat-exchange system 42, setting is adapted to the micro-reactor apparatus, can be used for controlling Make the reaction temperature of the reaction channel of the micro-reactor apparatus.

Such as：Heat-exchange system 42 can be used for controlling reaction temperature, according to system set point temperature and temperature sensor 12 The actual value of feedback, each channel for heat exchange cold medium flux is accurately controlled by PID control, so as to the temperature of each medium of indirect control And the temperature of course of reaction.

In an optional specific example, the cleaning systems 43, can be used for by control cleaning mode (such as：Liquid Body cleaning mode, gas cleaning mode), realize the control to the line clear process.

Such as：The cleaning systems 43, it can be used under the control of the controller 20, the micro-reactor apparatus entered Row cleaning.

Such as：Cleaning systems 43, it can include：Switch equipment, flow pump, cleaning agent storage pipeline and devil liquor recovery pipe Road.Wherein, the switching equipment, can be used for, by the feedstock transportation pipeline of the micro-reactor apparatus, being switched to the cleaning agent Store pipeline；And/or the output of products pipeline by the micro-reactor apparatus, it is switched to the devil liquor recovery pipeline.

Such as：Cleaning systems 43, it can also include：During clean gas pipeline, the switching equipment, it can be also used for institute State raw material intake line and be switched to the clean gas pipeline, to carry out line clear again to the reaction channel.

In an optional specific example, the control valve 44, it can be used for the servo-drive system 41, the heat exchange system At least one of system 42, described cleaning systems 43 enter to aid in control.

More alternatively, control valve 44, can include：Raw material transfer valve.The raw material transfer valve, with the micro-reactor apparatus Feedstock input adaptation set, can be used for being turned on and off the feedstock input.

More alternatively, control valve 44, proportional flow control valve can be included.It is adapted to heat-exchange system, can be with Set scale stream Measure valve.The proportional flow control valve, setting is adapted to the heat-exchange system 42, can be used for the refrigerant for controlling the heat-exchange system 42 Flow.

More alternatively, control valve 44, button and/or magnetic valve, the button and the magnetic valve can also be included, respectively Setting is adapted to the controller 20.Wherein, the button, it can be used for receiving and the course of reaction opened or stopped Manual control signal.The magnetic valve, can be used for receive the course of reaction is opened or stopped automatically controlling Signal.

Such as：The button, it can be used for receiving the manual control that the process of the line clear is opened or stopped Signal processed.The magnetic valve, it can be used for receiving and the process of the line clear opened or what is stopped automatically controlling letter Number.

More alternatively, control valve 44, can include：Output of products valve and plunger device.During output of products, the production Product delivery valve and the plunger device, it is adapted to setting with the input product container respectively.

Such as：The output of products valve, setting is adapted to the output of products mouth of the micro-reactor apparatus, can be used for opening Or close the output of products mouth of the micro-reactor apparatus.

Such as：The plunger device, setting is adapted to the output of products valve, can be used for increasing or to reduce the product defeated Go out the valve port bore of valve.

Such as：When the performs device 40 can also include switching equipment, the switching equipment, can be also used for institute The defeated pipeline of product of micro-reactor apparatus is stated, next output of products container is switched to by an output of products container.

In an optional embodiment, it can also include：Memory cell 50 (such as：Raw material memory cell), Ke Yican Example as shown in Figure 3.

In an optional example, the memory cell 50, the raw material that can be used for storing the micro-reactor apparatus into Divide the corresponding relation with density.

In an optional specific example, in raw material input process, it can obtain and treat by inquiring about memory cell 50 Input density corresponding to the composition of raw material.

Thus, set by the adaptation of memory cell, the convenience and accuracy of data search can be lifted.

In an optional embodiment, the control system of the micro-reactor apparatus (such as：Microreactor control dress Put), it can include：Interactive device (such as：Two display units), controller 20 (such as：Industrial computer 21, PID controller 20), Harvester 10 (such as：Video acquisition system 16, temperature sensor 12, pressure sensor 13, flow sensor 11, liquid level pass The detection means such as sensor 14, analogue collection module 17), alarm, performs device 40 (such as：Servo-drive system 41, heat-exchange system 42 etc.) and interactive device 30 (such as：Analog input mModule 34, I/O input/output modules 36) etc..

Such as：The microreactor control device, can include：Two display units, industrial computer 21, analogue collection module 17th, Analog input mModule 34, I/O input/output modules 36, video acquisition system 16, liquid level sensor 14, pressure sensor 13rd, temperature sensor 12, flow sensor 11, servo-drive system 41 and heat-exchange system 42.

In an optional example, the interactive device, it can include：First display unit 31.

Alternatively, first display unit 31, with the controller 20 (such as：Industrial computer 21) adaptation connection (such as： Be attached by video connecting line), may be used to provide operation and control interface (such as：To the micro-reactor apparatus carry out operation and The touch interface of control), and/or all kinds of parameters needed for being chemically reacted to the micro-reactor apparatus instruction input information and State is shown.

More alternatively, the first display unit 31 can include：Touch-display unit.

Such as：First display unit 31 is touch-display unit, is connected with industrial computer 21 by video connecting line, Ke Yiyong In all kinds of parameter instruction inputs and all kinds of status displays needed for display and operation interface, micro- anti-device reaction.

In an optional example, the interactive device, it can include：Second display unit 32.The harvester 10, It can include：Video acquisition system 16.

Alternatively, the video acquisition system 16, connection is adapted to second display unit 32, can be used for gathering institute The video information and status information at the reaction scene of micro-reactor apparatus are stated, and is transmitted to second display unit 32.

Such as：Video acquisition system 16 is used for obtaining and transmitting working site video information, monitors the outward appearance of various kinds of equipment The generation of the unusual condition such as situation and gas, liquid leakage, burning, blast.

More alternatively, the video acquisition system 16, can include：Camera.

Alternatively, second display unit 32, connection is adapted to the video acquisition system 16, also with the controller 20 (such as：Industrial computer 21) adaptation connection (such as：Can be attached by video connecting line), it is displayed for described regard The video information and/or the status information that frequency acquisition system 16 collects.

More alternatively, second display unit 32, can include：Display screen.

Alternatively, the controller 20, connection is adapted to the alarm, can be used for using at default vision signal Adjustment method, the video information and/or the status information are analyzed and processed, obtain analysis result.The analysis is tied Fruit and the default secure threshold at the reaction scene are contrasted, that is, judge whether the analysis result exceeds the default safety Threshold value.When the analysis result exceeds the default secure threshold, it is (i.e. unexpected to determine that safety problem occurs in the reaction scene Situation, such as situations such as liquid leakage, burning, blast), and start the alarm, initiate alarm.

Alternatively, it the alarm, can be used under the control of the controller 20, alarm initiated, with described in notice The safety problem at the scene of being reacted described in operating personnel's timely processing of micro-reactor apparatus.

Such as：Second display unit 32 is connected by video connecting line with industrial computer 21, be can be used for monitoring and is passed through video The reactor live video information and status information that acquisition system 16 collects, system can use appropriate video signal transacting to calculate Method analyzes video, and when fortuitous event occurs in scene, during generation such as situations such as liquid leakage, burning, blast, system is according to video Simultaneously the very first time notifies operating personnel for result and alarm, and operating personnel can take different processing according to different situations Scheme.

In an optional example, the harvester 10, it can include：Temperature sensor 12, pressure sensor 13, stream Quantity sensor 11, liquid level sensor 14 etc..Further, the harvester 10, can also include：Analogue collection module 17。

Alternatively, the analog acquisition device 10, connection is adapted to the controller 20, can be used for receiving the temperature The detection signal of the detection means such as sensor 12, pressure sensor 13, flow sensor 11, liquid level sensor 14 is spent, and is transmitted To the controller 20.

More alternatively, the liquid level sensor 14, it can be used for the liquid level signal for detecting fluid in the micro-reactor apparatus.

Such as：Liquid level sensor 14 can be used for detecting liquid level, system according to the detection signal of liquid level sensor 14, Can interpolate that input medium and whether transfinite, output medium whether store transfinite and production process in the storage of some accessory substances Whether medium transfinites, may so as to avoid each quality accident and danger medium caused by each storage medium transfinites spilling from overflowing The danger brought.

More alternatively, the temperature sensor 12, it can be used for the temperature for detecting the scene of being reacted in the micro-reactor apparatus Information.

Such as：Temperature sensor 12 can be used for detecting each several part temperature, and system is according to the value of feedback of temperature sensor 12 And setting value, the cold medium flux of heat-exchange system 42 is controlled in real time by pid control algorithm, so as to accurately control each reaction medium The temperature of input temp and course of reaction, to reach stable course of reaction, ensure the purpose of product quality.

More alternatively, the flow sensor 11, it can be used for the flow velocity for detecting reaction medium in the micro-reactor apparatus Information.

Such as：Flow sensor 11 can be used for detecting reaction medium flow velocity, and system detects according to flow sensor 11 Value of feedback, the rotating speed of each rate-of flow pump is adjusted in real time by pid control algorithm, to reach the accurate control to reaction medium ratio System.

More alternatively, the pressure sensor 13, it can be used for reaction channel and/or the storage for detecting the micro-reactor apparatus The pressure information of glassware.

Such as：Pressure sensor 13 can be used for detecting reaction channel and accumulator pressure, pass through the pressure of diverse location Sensor 13 detects valve system and is used for medium in calculation medium weight or the blocking of detection reaction channel and passage whether there is, and passes through measurement Value and all kinds of threshold values of system relatively control and protected course of reaction, avoid liquid leakage, line clogging accident generation simultaneously It can also avoid wriggling without medium in flow pump body and may cause the generation of diaphragm damage accident.

Alternatively, the controller 20, can be used for after the detection signal is converted into data signal by analog signal, Send to the first display unit 31 and shown.And/or the actual value according to the different detection signals, adaptation regulation institute Micro-reactor apparatus is stated, so that the micro-reactor apparatus carries out the chemical reaction matched with the actual value, with to micro- reaction The chemical reaction process of equipment carries out closed-loop control.

Such as：Analogue collection module 17 is used for receiving temperature sensor 12, pressure sensor 13, flow sensor 11 etc. Detection signal, system is converted to data signal according to the analog signalses of collection and shows, while according to unlike signal Actual valve system can do different reactions automatically, so as to realize the automated closed-loop of system control requirement.

In an optional example, the performs device 40, it can include：Servo-drive system 41.Further, the interaction Device 30, it can include：Analog input mModule 34.

Alternatively, the Analog input mModule 34, setting is adapted to the servo-drive system 41, can be used for watching to be described Dress system 41 provides Setting signal.

Such as：Analog output module 35 is used for providing Setting signal for servo-drive system 41, and servo-drive system 41 is according to simulation The given signal of amount output module 35 is handled and is converted into the tach signal of flow pump and is controlled.

Alternatively, the servo-drive system 41, respectively the flow pump with the controller 20 and the micro-reactor apparatus be adapted to Set, can be used for carrying out adaptation processing according to the Setting signal, and be converted to the tach signal of flow pump, to the flow The rotating speed of pump is controlled.

Such as：Servo-drive system 41 can be used for accurate control flow rate, the amount given according to system and flow The actual value that sensor 11 feeds back, each channel media real-time traffic is accurately controlled by PID control.

In a more optional example, the interactive device 30, it can also include：I/O input/output modules 36.Further Ground, it is adapted to, is additionally provided with the flow pump：Button, indicator lamp and magnetic valve etc..

Alternatively, the I/O input/output modules 36, respectively with the controller 20 and the button, the instruction The adaptation connection of at least one of lamp, the magnetic valve, described liquid level sensor 14 etc., can be used for exporting and/or described in receiving At least one on-off models such as button, the indicator lamp, the magnetic valve, the liquid level sensor 14.

Alternatively, it the controller 20, can be used for according to the on-off model, determine working as the micro-reactor apparatus Preceding working condition.

Such as：I/O input/output modules 36 can be used for exporting and receive button, indicator lamp, magnetic valve, liquid level sensor All kinds of on-off models such as 14, system judge according to all kinds of on-off models and export different working conditions.

In an optional example, the performs device 40, it can include：Heat-exchange system 42.

Alternatively, the heat-exchange system 42, setting is adapted to the controller 20, can be used for controlling micro- reaction to set Standby reaction temperature.

Such as：Heat-exchange system 42 can be used for controlling reaction temperature, according to system set point temperature and temperature sensor 12 The actual value of feedback, each channel for heat exchange cold medium flux is accurately controlled by PID control, so as to the temperature of each medium of indirect control And the temperature of course of reaction.

Through substantial amounts of verification experimental verification, using the technical scheme of the present embodiment, pass through harvester 10, interactive device 30 and control Device 20 processed (such as：Industrial computer 21) adaptation set, it is possible to achieve remote control, on-line checking and in real time monitoring etc. control, have Chemical reaction process is preferably monitored beneficial to operating personnel so that the control function of micro-reactor apparatus increases, to micro- The control difficulty of consersion unit greatly reduces.

According to embodiment of the present utility model, a kind of micro- reaction of the control system corresponding to micro-reactor apparatus is additionally provided The control system of equipment.The control system of the micro-reactor apparatus can include：Control based on above-described micro-reactor apparatus System, to the raw material input process of the micro-reactor apparatus, the flow control process, the temperature controlled processes, institute At least one of line clear process, the output of products process, described security protection detection process is stated to be controlled.

In an optional example, the control system of the micro-reactor apparatus, it can include：

The reaction information of step 1, the collection micro-reactor apparatus.Wherein, the reaction information, can include：Raw material is defeated Enter at least one of amount, flow, temperature, pressure, output of products amount.

Step 2, receive to the configuration information of the micro-reactor apparatus.

Step 3, according to the configuration information and/or the reaction information, the raw material of the micro-reactor apparatus was inputted During journey, the course of reaction including at least flow and/or temperature, line clear process, production detection process, output of products At least two processes are controlled.

In an optional example, the control system of the micro-reactor apparatus, it can also include：

Under the control of the controller 20, deliberate action is performed, to realize that the intervention to any process controls； And/or the field data at the collection reaction scene；And/or export the field data of the micro-reactor apparatus, warning message, At least one of described reaction information.

In an optional specific example, the control to the raw material input process of the micro-reactor apparatus, it can include：

Gather the pressure that the storage of raw materials applies to the accumulator bottom in the accumulator.

Set the composition of the raw material to be entered of the micro-reactor apparatus, with when quality.

According to the pressure, the composition, the proportioning and the quality, determine whether the input quantity of the raw material reaches Default demand.And

When the input quantity reaches the demand, stop input of the raw material to the micro-reactor apparatus；Or work as When the input quantity is not up to the demand, continue input of the raw material to the micro-reactor apparatus.

Optionally it is determined that whether the input quantity of the raw material reaches default demand, can specifically include：

According to the composition of the raw material, density corresponding with the composition in the raw material memory cell 50 is determined.And According to the density of the pressure of the raw material, the shape of the accumulator and the raw material, determine to store original in the accumulator The current weight of material.And/or

According to the target weight matched somebody with somebody when quality, determine the raw material needed for the micro-reactor apparatus of the raw material.

And

Determine the current weight of the raw material and the first difference of target weight, if when reaching the first predetermined threshold value, really The fixed input quantity reaches the demand.Or when first difference is not up to first predetermined threshold value, it is determined that described Input quantity is not up to the demand.

Alternatively, to the control of the raw material input process of the micro-reactor apparatus, can also include：

The feedstock input is turned on and off.

The raw material transfer valve being adapted to the feedstock input is opened, to input the raw material to the micro-reactor apparatus. Or the raw material transfer valve is closed, to stop inputting the raw material to the micro-reactor apparatus.

In an optional example application, pass through the adaptation of the first display unit 31, pressure sensor 13 and controller 20 Set, it is possible to achieve raw material (raw material of i.e. pending chemical reaction) input process of the micro-reactor apparatus is controlled System.Such as：Can in the system of the present utility model with reference to shown in Fig. 5 the embodiment that raw material input process controls principle signal Figure, further illustrate the detailed process of raw material input process control.

Such as：Example shown in Figure 5, the step of can be used for control input raw material, it can include：

Step S101, described first display unit 31, the raw material that can be used for setting the micro-reactor apparatus to be entered Composition, with when quality.

Such as：Raw material (i.e. raw material) composition, formula rate and product weight are set by the first display unit 31.

Step S102, described controller 20, can be used for the composition according to the raw material, from default raw material memory cell In 50, the density of the raw material corresponding with the composition of the raw material is extracted.And/or according to the raw material with when matter Amount, it is determined that the target weight of the required raw material.

Such as：System is extracted corresponding to composition by the composition of raw material of setting from system raw material memory cell 50 Density p, and the weight according to needed for formula rate and product quality calculate each composition.

Step S103, the feedstock input with the micro-reactor apparatus is adapted to, and is provided with raw material transfer valve.The raw material is defeated Enter valve and connection is adapted to the controller 20, the controller 20 controls the unlatching of the raw material transfer valve.

Such as：System control raw material transfer valve is opened, and inputs raw material.

Step S104, described pressure sensor 13, adaptation are arranged on the bottom of the accumulator of the micro-reactor apparatus, can be with For detecting the pressure of the storage of raw materials in the accumulator.

Such as：To detect each raw material real-time by being installed on the pressure sensor 13 of raw hopper bottom for system detectio Pressure P.

Step S105, described controller 20, setting is adapted to the pressure sensor 13, can be used for according to the raw material Pressure, the density of the shape of the accumulator and the raw material, determine the current weight of raw material in the accumulator.

Such as：System calculates each raw material actual weight in real time according to pressure P and accumulator shape and material density ρ.

Step S106, described controller 20, each original can be judged by the target weight and current weight of more each raw material Whether the input quantity of material reaches predetermined demand.

Such as：The scope that makes it is judged whether by more each raw material actual weight and set component weight.

Step S107, when the input quantity of certain raw material is not up to demand, then the shape of the raw material transfer valve unlatching is maintained State, continue to add.When the input quantity of certain raw material reaches demand, then close the raw material transfer valve, stop the raw material after It is continuous to launch, and reminded.

Such as：If system detectio raw material quality is less than default tolerance, continue to add.When system detectio former material When the actual mass of material reaches sets requirement, close raw material input valve and stop launching.And the system prompt raw material prepares Finish, after all raw materials are ready, all raw materials of system prompt are ready to be processed.

In an optional specific example, the reaction for comprising at least flow and/or temperature to the micro-reactor apparatus In the control of journey, the control to the flow, it can include：

Set the Jie of the composition, proportioning and the raw material of the raw material in the reaction channel of the micro-reactor apparatus Mass flow speed.

Servo-drive system 41 is set, according to the composition of the raw material, with when velocity of medium, it is determined that with the micro-reactor apparatus Simulation controlled quentity controlled variable needed for the servo-drive system 41 of adaptation.

By the simulation controlled quentity controlled variable, the running speed for the motor being adapted to the servo-drive system 41 is converted to, to drive State motor rotation.

The motor is set to be rotated with the running speed, to drive the flow pump being adapted to motor action, to described The reaction channel of micro-reactor apparatus conveys the raw material.

Optionally it is determined that the simulation controlled quentity controlled variable needed for the servo-drive system 41, can include：

According to the mass flow matched somebody with somebody when velocity of medium, determine each composition in the raw material of the raw material.And

According to the composition of the raw material, density corresponding with the composition in the raw material memory cell 50 is determined.And

According to the density and mass flow of each composition in the raw material, the volume flow of each composition in the raw material is determined.

Alternatively, to the control of the flow, can also include：

Gather the rate-of flow that the flow pump conveys the raw material to the micro-reactor apparatus.

The rate-of flow is inputted to default pid control module, by the pid control module to the medium flow field Amount carries out flow correction, obtains revised analog quantity flow correction value.And

The analog quantity flow correction value is inputted to the servo-drive system 41 again, the servo-drive system 41 is driven institute State motor rotation, so circulation.

In an optional example application, passed by the first display unit 31, servo-drive system 41, flow pump, motor, flow The adaptation of sensor 11 and controller 20 is set, it is possible to achieve to reaction medium flow in the reaction channel of the micro-reactor apparatus Control.Such as：Can in the system of the present utility model with reference to shown in Fig. 6 the embodiment that flow controls principle schematic, enter One step illustrates the detailed process of flow control process.

Such as：Example shown in Figure 6, the step of can be used for controlling flow, it can include：

Step S201, described first display unit 31, it can be used for setting and stay in progress chemistry in the micro-reactor apparatus The composition of the raw material of reaction, with parameters such as when velocity of medium.

Such as：The various parameters such as composition of raw material, formula rate and speed of production are set by the first display unit 31.

Step S202, described controller 20, can be determined according to the raw material with when velocity of medium in the raw material The Theoretical Mass flow of each composition.

Such as：System calculates each Theory of Components mass flow according to formula rate and speed of production.

Wherein, mass flow is in the unit interval, and fluid passes through closed conduct or the fluid mass of open channel effective cross-section.

Step S203, described controller 20, can be according to the composition of the raw material, from default raw material memory cell 50 The density of the raw material corresponding with the composition of the raw material is extracted, and according to the mass flowmenter of each composition in the raw material Calculate the volume flow of each composition.

Such as：System by the composition of raw material of setting extract density p corresponding to composition and according to calculate it is each into Point mass flow calculation goes out the volume flow of each composition.

Step S204, described controller 20, the volume flow can be converted to the simulation needed for servo-drive system 41 Amount.

Such as：System servo-drive system 41 is converted into according to gross data according to the volume flow calculated needed for analog quantity.

Step S205, described servo-drive system 41, the analog quantity can be converted into motor speed and be exported.

Such as：The motor speed according to corresponding to being converted into the analog quantity that control system is transmitted of servo-drive system 41 exports.

Step S206, described motor is run with the motor speed, is driven flow pump action, is exported the raw material.

Such as：Motor driven flow pump acts, and exports flow of raw materials.

Step S207, described flow sensor 11, detects the rate-of flow in the raw material output procedure, and feed back to institute State controller 20.

Such as：The rate-of flow of the detection output of flow sensor 11, and instantaneous value is fed back into control system.

Step S208, described controller 20, the rate-of flow can be inputted to default pid control module, carried out Correcting process, and obtain revised analog output value.

Such as：The flow pid control module that the flow value of acquisition is input in system by system is handled, and obtains the mould of amendment Analog quantity output valve.

Step S209, described controller 20, the analog output value can be inputted again to the servo-drive system 41.

Such as：The analog output value for correcting completion is inputted servo-drive system 41 by system again.

Step S210, the described drive motor of servo-drive system 41 rotates, so circulation.

Such as：So circulation, form closed-loop control.

In an optional specific example, the reaction for comprising at least flow and/or temperature to the micro-reactor apparatus In the control of journey, the control to the temperature, it can include：

Setting is adapted to the target refrigerant temperature of the heat-exchange system 42 set with the micro-reactor apparatus.

The heat-exchange system 42 is opened, until the current refrigerant temperature of the heat-exchange system 42 reaches the target refrigerant temperature When spending, start the micro-reactor apparatus, and adjust by the heat-exchange system 42 the anti-of the reaction channel of the micro-reactor apparatus Answer temperature.

By default analog output module 35, to the proportional flow control valve being adapted to the heat-exchange system 42, output with The analog quantity temperature control amount of the target refrigerant temperature adaptation, so that the proportional flow valve events, control the heat exchange system The cold medium flux of system 42.

Alternatively, to the control of the temperature, can also include：

The goal response temperature of the reaction channel of the micro-reactor apparatus is set, and gathers the reaction of the micro-reactor apparatus The current reaction temperature of passage.

The current reaction temperature is inputted to default pid control module, trip temperature is entered by the pid control module Amendment, obtains analog quantity temperature corrected value.And

Again by the analog output module 35, the analog quantity temperature corrected value is exported to the proportional flow Valve, by controlling the cold medium flux that the current reaction temperature is adjusted, so to circulate.

In an optional example application, passed by the first display unit 31, heat-exchange system 42, proportional flow control valve, temperature The adaptation of sensor 12 and controller 20 is set, it is possible to achieve the control to reaction temperature in the reaction channel of the micro-reactor apparatus System.Such as：Can in the system of the present utility model with reference to shown in Fig. 7 a temperature controlled embodiment principle schematic, enter one The detailed process of step explanation temperature controlled processes.

Such as：Example shown in Figure 7, the step of can be used for controlling reaction temperature, it can include：

Step S301, described first display unit 31, each reaction channel that can be used for setting the micro-reactor apparatus The refrigerant temperature of reaction temperature, and/or the heat-exchange system 42.

Such as：Reactor each several part is set by the first display unit 31 and controls temperature and the refrigerant temperature of heat-exchange system 42.

Step S302, described controller 20, can start the heat-exchange system 42, until cold in the heat-exchange system 42 Matchmaker reaches the default refrigerant temperature.

Such as：System starts heat-exchange system 42 and waits refrigerant to reach preset temperature.

Step S303, described controller 20, proportional flow control valve action, control can be controlled by analog output module 35 Cold medium flux processed.

Such as：System controls proportional flow control valve to act by analog output, controls cold medium flux.

Step S304, described temperature sensor 12, the current reaction temperature of the micro-reactor apparatus can be detected, and will inspection Survey result and feed back to the controller 20.

Such as：Temperature sensor 12 detects reactor Current Temperatures and detected value is fed back into control system.

Step S305, described controller 20, the current reaction temperature can be inputted to default pid control module, Processing is modified, obtains carrying out the analog output value after temperature modification, i.e. reaction temperature correction value.

Such as：Temperature feedback value is input to temperature PID control resume module in system by system, obtains the analog quantity of amendment Output valve.

Step S306, described controller 20, the reaction temperature correction value can be exported cold to proportional flow control valve, control Matchmaker's flow.

Such as：The temperature control analog value of amendment is output to proportional flow control valve by system, controls cold medium flux.

Step S307, described controller 20, the refrigerant temperature of the heat-exchange system 42 can be monitored, when the refrigerant temperature Reach and start the microreactor after default controlling value and reacted.

Such as：Start reaction after reaching controlling value Deng temperature of reactor.

Step S308, described controller 20, according to the testing result of the temperature sensor 12, proportional flow control valve is controlled, Adjust cold medium flux, so controlling reaction temperature, circulation.

Such as：Temperature that the real-time detection temperature sensor 12 of system detects simultaneously by system timely processing and feeds back to ratio Example flow valve, control cold medium flux, so circulation.

It can be seen that by detection temperature and feeding back to control system, the flow of refrigerant is further controlled, can more precisely, more The reliably medium temperature at control reaction scene, be advantageous to lift reaction effect.

In an optional specific example, the reaction for comprising at least flow and/or temperature to the micro-reactor apparatus Journey (such as：Security protection detection process) control, can include：

Show the field data of the micro-reactor apparatus.

Determine whether the field data meets set information, when the field data is unsatisfactory for the set information, The alarm is initiated by the alarm.

Wherein, the field data is unsatisfactory for the set information, can include：The reaction scene of the micro-reactor apparatus Raw material leakage, poison gas is exceeded, ambient temperature and humidity is at least one of abnormal.

Alternatively, can be with to the control of the course of reaction for comprising at least flow and/or temperature of the micro-reactor apparatus Including：

The loine pressure of the reaction channel of the micro-reactor apparatus is gathered, gathers the reaction channel of the micro-reactor apparatus Reaction temperature, gather the medium liquid level of the reaction channel of the micro-reactor apparatus.

When the field data meets the set information, start the course of reaction of the micro-reactor apparatus, and determine Whether at least one of described loine pressure, the rate-of flow, the reaction temperature in the course of reaction reach respective Setting value.And

When at least one of the loine pressure in the course of reaction, rate-of flow, reaction temperature are not up to respective The setting value, and/or course of reaction when reaching the stop condition, stop the course of reaction.

Wherein, the field data is unsatisfactory for the set information, can also include：Medium in the micro-reactor apparatus At least one of the loine pressure, the reaction temperature, described medium liquid level are not up to its respective described setting value.

Alternatively, can be with to the control of the course of reaction for comprising at least flow and/or temperature of the micro-reactor apparatus Including：

Set the set information at the reaction scene of the micro-reactor apparatus, and/or the reaction of the setting micro-reactor apparatus The stop condition of process, and/or the setting theoretical field data, and the setting loine pressure, the reaction temperature, institute Give an account of at least one of respective described setting value of matter liquid level.

And/or

By being adapted to the servo-drive system 41 set and flow pump with the micro-reactor apparatus, opening for the course of reaction is controlled Open or stop.

And/or

When the system can also include performs device 40, the performs device 40 can also include button and/or electricity Magnet valve, the button and the magnetic valve, it is adapted to setting with the controller 20 respectively.Wherein,

The button, it can be used for receiving the manual control signal that the course of reaction is opened or stopped.

The magnetic valve, it can be used for receiving the automatic control signal that the course of reaction is opened or stopped.

And/or

When the system can also include performs device 40, the performs device 40 can also include：Cleaning systems 43.

The controller 20, it can be also used for when the course of reaction stops, it is determined whether needing to micro- reaction Equipment is cleaned.When needing to clean the micro-reactor apparatus, start the cleaning systems 43.

It the cleaning systems 43, can be used under the control of the controller 20, the micro-reactor apparatus carried out clear Wash.

In an optional example application, pass through the first display unit 31, pressure sensor 13, temperature sensor 12, liquid Level sensor 14, alarm, servo-drive system 41, flow pump, the adaptation of cleaning systems 43 and controller 20 are set, it is possible to achieve right The control of reaction medium flow in the reaction channel of the micro-reactor apparatus.Such as：Can be of the present utility model with reference to shown in Fig. 4 The principle schematic for the embodiment that course of reaction controls in system, further illustrate the detailed process of course of reaction control.

Such as：A kind of example shown in Figure 4, procedures system that can be used for microreactor control, can include：

Step S401, described first display unit 31, it can be used for setting and stay in the micro-reactor apparatus original reacted Parameter needed for the various reactions such as composition, proportioning, rate-of flow and the reaction temperature of material.

Such as：Set by the first display unit 31 needed for the various reactions such as raw material information, formula information, flow, temperature Parameter.

Step S402, described controller 20, it may be determined that the pressure of fluid, temperature, liquid level, report in the micro-reactor apparatus Whether alert device etc. reaches predetermined condition, if otherwise adjustment in time.

Such as：The various state preparations such as system detectio pressure, temperature, liquid level, safety device whether in place, if any different Often person skilled is arranged to be handled, if normal continue.

Step S403, described second display unit 32, it can be used for monitoring reaction scene and whether there is abnormal conditions.

Such as：Production scene is observed with the presence or absence of abnormal by the second display unit 32, as found to have raw material leakage, poisonous Gas is exceeded, ambient temperature and humidity is abnormal (such as：More than default temperature humidity range) situations such as close system immediately and assign specialty Technical staff is handled to scene, if normal continue.

Step S404, described controller 20, can start the course of reaction of the micro-reactor apparatus, and react described Rate-of flow and reaction temperature in journey are controlled.

Such as：Start course of reaction, accurate flow control and reaction temperature.

Step S405, described controller 20, reaction channel can be detected in the course of reaction of the micro-reactor apparatus Whether the parameters such as loine pressure, channel capacity and reaction temperature are in the range of given threshold, if otherwise interrupting course of reaction.

Such as：In course of reaction the various technical indicators such as system detectio loine pressure, channel capacity, reaction temperature whether Within security settings threshold range, stop servo-drive system 41 immediately if any pathological system, close flow pump, stop reaction.

Step S406, in the course of reaction, also servo-drive system can be stopped manually by default manual operation button 41 outputs, close flow pump, interrupt course of reaction.

Such as：Servo-drive system 41 can be stopped in course of reaction manually to export, close flow pump, stopped reaction.

Step S407, described controller 20, can stop reacting when respective reaction reaches default stop condition Journey.

Such as：As if not stopping or pathological system occur being automatically stopped manually, system is by root during system response According to setting stop condition, it is automatically stopped after reaching stop condition.

Step S408, default cleaning systems 43, can be selected according to user, to institute under the control of the controller 20 Micro-reactor apparatus is stated to be cleaned.

Such as：Manually select and whether cleaned as needed after the completion of system response, if it is not needed, control flow knot Beam, if necessary to enter cleaning process.

Step S409, described controller 20, it can close micro- reaction after the cleaning systems 43 complete cleaning and set It is standby.

Such as：After the completion of cleaning, control flow terminates.

In an optional specific example, to the line clear process of the micro-reactor apparatus, it can include：

Set the line clear parameter of the micro-reactor apparatus.

When the course of reaction of the micro-reactor apparatus stops, according to the line clear parameter, starting and described micro- anti- The switching equipment for answering equipment adaptation to set.By the switching equipment, by the feedstock transportation pipeline of the micro-reactor apparatus, switching Pipeline is stored to the cleaning agent that setting is adapted to the micro-reactor apparatus.And/or the output of products pipe by the micro-reactor apparatus Road, it is switched to the devil liquor recovery pipeline for being adapted to and setting with the micro-reactor apparatus.

And

Start the flow pump for being adapted to and setting with the micro-reactor apparatus, the cleaning agent is stored into the detergent pump in pipeline Enter the passage tube of the micro-reactor apparatus, to be carried out once to the reaction channel of the micro-reactor apparatus using the cleaning agent Line clear.

Alternatively, to the line clear process of the micro-reactor apparatus, can also include：

When being finished using a reaction channel progress line clear of the cleaning agent to the micro-reactor apparatus, it is determined that Whether need to carry out gas cleaning, to be again started up the switching equipment when needing to carry out gas cleaning.

By the switching equipment, the raw material intake line is switched to the clear of setting is adapted to the micro-reactor apparatus Clean gas piping, to carry out line clear again to the reaction channel.

And/or

By be adapted to the micro-reactor apparatus set button, receive the process of the line clear is opened or The manual control signal of stopping.

And/or

By being adapted to the magnetic valve set with the micro-reactor apparatus, receive and the process of the line clear is opened Or the automatic control signal stopped.

In an optional example application, by the first display unit 31, feedstock transportation pipeline, cleaning agent store pipeline, Devil liquor recovery pipeline, switch the suitable of equipment, flow pump, detergent pump, clean gas pipeline, manual control button and controller 20 With setting, it is possible to achieve carry out cleaning control to pipeline in the reaction channel of the micro-reactor apparatus.Such as：Fig. 8 can be combined The principle schematic of an embodiment of line clear process control in shown system of the present utility model, further illustrate that pipeline is clear Clean detailed process.

Such as：Example shown in Figure 8, the step of can be used for line clear, it can include：

Step S501, described first display unit 31, it can be used for determination information and the cleaning for receiving pipeline cleaning mode The set information of parameter.

Such as：Cleaning parameter into line clear pattern and is set by the selection of the first display unit 31.

Step S502, described switching equipment, can be according to the line clear pattern of determination, by the control of the controller 20 Object is switched to cleaning agent storage pipeline by raw material output pipe, and output of products pipeline is switched into devil liquor recovery pipeline.

Such as：System switches raw material output pipe and stores pipeline to cleaning agent, and switches output pipe to devil liquor recovery Pipeline.

Step S503, described controller 20, flow pump is started, the cleaning agent is stored into the cleaning agent in pipeline is pumped into pipe Road, for cleaning the reaction channel of the micro-reactor apparatus.Such as：System starts flow pump, and cleaning agent is pumped into pipeline and is used for Clean reaction channel.

Step S504, described cleaning device, can be cleaned according to the cleaning parameter of setting.

Such as：Cleaned according to the cleaning liquid technological parameter of setting.

Step S505, by default hand push button, can carry out stopping cleaning manually during cleaning.

Such as：Cleaning liquid can stop cleaning manually in completing.

Step S506, described controller 20, can be after the completion of aforesaid liquid cleaning, it is determined whether selection gas cleaning mould Formula.Gas cleaning is carried out if selection, terminates cleaning process if not selecting.

Such as：If not selecting gas to clean after the completion of liquid is settled accounts, then terminate cleaning mode.If select gas clear It is clean, then into gas cleaning mode.

Step S507, described switching equipment, the raw material output pipe can be switched when selecting gas cleaning mode To gas cleaning channels.

Such as：System switches intake line to clean gas pipeline (i.e. gas cleaning channels).

Step S508, by air cleaning device, cleaning agent remaining in reaction channel and flow pump can be carried out two Secondary cleaning.

Such as：Clean gas blows clean cleaning agent remaining in reaction channel and flow pump into pipeline, avoids influenceing Lower secondary response.

Step S509, by default hand push button, gas cleaning can be stopped during gas cleaning.

Such as：It can stop cleaning manually in gas cleaning.

Step S510, described controller 20, cleaning mode can be exited when gas cleans completion.

Such as：After the completion of cleaning parameter cleaning according to the gas of setting, system exits cleaning mode and awaited orders.

In an optional example application, pass through the first display unit 31, input product container, pressure sensor 13, stream Quantity sensor 11, temperature sensor 12, weighing sensor, servo-drive system 41, flow pump, motor, output valve, plunger device and control The adaptation of device 20 processed is set, it is possible to achieve the reaction scene to the micro-reactor apparatus carries out on-line checking.

Such as：System detectio system, it can include：

Step S601, described first display unit 31, can be used for setting the parameters such as pressure, temperature, flow, weight.

Such as：The detection numerical value such as pressure, temperature, flow, weight is set by the first display unit 31.

Step S602, described pressure sensor 13, the pressure of input product container bottom can be detected.The controller 20, output products weight can be determined according to the pressure and input product container shapes of the input product container bottom detected Whether amount meets production requirement, starts alarm if being unsatisfactory for.

Such as：By detecting input product container bottom pressure, output products weight is calculated according to input product container shapes Whether amount meets production requirement, if being unsatisfactory for system alarm prompting, operating personnel adjust input product weight according to prompting.

Step S603, described flow sensor 11, the current media of the reaction channel of the micro-reactor apparatus can be detected Flow.The controller 20, it may be determined that whether the current media flow velocity meets technological requirement, and servo is controlled if being unsatisfactory for System 41 is adjusted.

Such as：Detect whether reaction channel actual flow meets technological requirement by flow sensor 11, if be unsatisfactory for System is adjusted by changing the flow pump motor speed of servo-drive system 41.

Step S604, described temperature sensor 12, can detect the current reaction of the reaction channel of the micro-reactor apparatus Temperature.The controller 20, it may be determined that whether the current reaction temperature meets technological requirement, and heat exchange is controlled if being unsatisfactory for System 42 is adjusted.

Such as：Detect whether reaction channel actual temperature meets technological requirement by temperature sensor 12, if be unsatisfactory for System is controlled by adjusting heat exchange cold medium flux.

Step S605, described weighing sensor, the output products weight of the micro-reactor apparatus can be detected.The control Device 20, can detect whether the output products weight reaches setting numerical value, by exporting gate valve and plunger device if not up to It is adjusted.

Such as：Detect whether output products weight reaches setting numerical value by weighing sensor, if discontented pedal system By controlling output valve and plunger device to be adjusted.

In an optional specific example, the control of the production detection process to the micro-reactor apparatus, it can include：

Set production requirement of the micro-reactor apparatus to its input product container.

Gather the current pressure of the input product container bottom of the micro-reactor apparatus.

According to the shape of the current pressure and the input product container, determine in the input product container treat it is defeated Go out the production requirement whether product weight meets setting.When the output products weight is unsatisfactory for the production requirement, it is determined that When the output products weight is unsatisfactory for production requirement, by being adapted to the alarm set with the micro-reactor apparatus, report is initiated It is alert, to remind operating personnel to adjust the product weight to be output in the input product container.

Wherein, the alarm, can include：At least one alarm of acousto-optic, voice.

Alternatively, the control of the production detection process to the micro-reactor apparatus, can also include：

Set at least one of setting reaction temperature, setting rate-of flow of the reaction channel of the micro-reactor apparatus.

The current media flow of the reaction channel is gathered, and gathers the current reaction temperature of the reaction channel.

Determine whether the current media flow meets the setting rate-of flow.When the current media flow is unsatisfactory for During the setting rate-of flow, by being adapted to the servo-drive system 41, flow pump and the motor that set, regulation with the micro-reactor apparatus The current media flow of the reaction channel.And/or

Determine whether the current reaction temperature meets the setting reaction temperature, when the current reaction temperature is unsatisfactory for During the setting reaction temperature, by being adapted to the heat-exchange system 42 set with the micro-reactor apparatus, the reaction channel is adjusted Current reaction temperature.

Wherein,

By the servo-drive system 41, being turned on and off for the flow pump is controlled.By the flow pump, described in control The unlatching or stopping of course of reaction.And/or by the heat-exchange system 42, adjust the reaction channel of the micro-reactor apparatus Reaction temperature.

Alternatively, the control of the production detection process to the micro-reactor apparatus, can also include：

Set the setting output products weight of the product input pod of the micro-reactor apparatus.

Gather the current output products weight of the input product container of the micro-reactor apparatus.

Determine whether the current output products weight reaches the setting output products weight.When the current output production When product weight is not up to the setting output products weight, it is defeated that control is adapted to the product set with the input product container respectively Go out valve and plunger device, the output of products amount of the input product container is adjusted.

In an optional specific example, the control to the output of products process of the micro-reactor apparatus, it can include：

Set the theoretical output of products amount of the micro-reactor apparatus.

Gather the current production output quantity of the micro-reactor apparatus.

Determine the second difference of the current production output quantity and the setting output of products amount, if it is default to reach second Threshold value, close when second difference reaches second predetermined threshold value and be adapted to the output of products mouth of the micro-reactor apparatus The output of products valve of setting.

Wherein, by the output of products valve, it is turned on and off the output of products mouth of the micro-reactor apparatus.

Alternatively, to the control of the output of products process of the micro-reactor apparatus, can also include：

By being adapted to the plunger device set with the output of products valve, the valve port bore of the output of products valve is adjusted, with Adaptation regulation is carried out to the current production output quantity.

And/or

When the product input quantity of an output of products container reaches setting output products weight, by micro- reaction The defeated pipeline of product of equipment switches to next output of products container, continues the quantitative output control of next product.

By the switching equipment, by the defeated pipeline of the product of the micro-reactor apparatus, by an output of products container Switch to next output of products container.

In an optional example application, by the first display unit 31, output valve, weighing sensor, plunger device, cut The adaptation of converting mechanism and controller 20 is set, it is possible to achieve the quantitative output procedure of product of the micro-reactor apparatus is controlled System.Such as：Can in the system of the present utility model with reference to shown in Fig. 9 an embodiment of the quantitative output procedure control of product principle Schematic diagram, further illustrate the detailed process of the quantitative output procedure control of product.

Such as：Example shown in Figure 9, the quantitative output control step of product

Step S701, described first display unit 31, the output products that can be used for setting the micro-reactor apparatus are set It is quantitative.

Such as：Output products quantitative value is set by the first display unit 31.

Step S702, described controller 20, can control output valve, be entered with opening output valve control output products Default product container.

Such as：Open output valve control output products and enter container.

Step S703, described weighing sensor, the reality output amount of output of products can be detected.

Such as：Weighing sensor Real-time Feedback output products weight.

Step S704, described controller 20, it can be determined that the reality output amount for the output of products that weighing sensor detects Whether approached with set amount, if degree of closeness within the specific limits if close outflow valve door, stop output.

Such as：Judge whether weighing sensor detection numerical value approaches with setting numerical value, if close in the range of certain numerical value When close outflow valve door.

Step S705, described controller 20, can be when the reality output amount be not up to set amount, pilot plunger device, Until reality output amount is consistent with set amount.

Such as：By the fine adjustment output products of plunger device, it is consistent until with setting numerical value.

Step S706, described controller 20, it can switch product container after the completion of the output of current production container, enter A certain amount of output control under row.

Such as：After the completion of, system switching container, a certain amount of output control under.

The processing and function realized by the system of the present embodiment essentially correspond to earlier figures 1 to the system shown in Fig. 3 Embodiment, principle and example, therefore not detailed part in the description of the present embodiment, may refer to mutually speaking on somebody's behalf in previous embodiment It is bright, it will not be described here.

Through substantial amounts of verification experimental verification, using the technical solution of the utility model, by performs device 40 (such as：Servo system System 41, heat-exchange system 42 and warning device etc.) and controller 20 adaptation setting, can preferably monitor chemical reaction process, Once it was found that occurring exception in chemical reaction process can find and solve in time, personal security is advantageously ensured that, to micro- reaction The security that equipment is controlled also is able to significant increase and then lifts the control security and hommization degree of micro-reactor apparatus.

To sum up, it will be readily appreciated by those skilled in the art that on the premise of not conflicting, above-mentioned each advantageous manner can be certainly Combined, be superimposed by ground.

Embodiment of the present utility model is the foregoing is only, and may not be usable for limiting the utility model, for this For the technical staff in field, the utility model can have various modifications and variations.It is all in the spirit and principles of the utility model Within, any modification, equivalent substitution and improvements made etc., it should be included within right of the present utility model.

Claims (9)

1. A kind of 1. control system of micro-reactor apparatus, it is characterised in that including：Harvester, interactive device and controller；Its In,

   The harvester, for gathering the field data of the micro-reactor apparatus；

   The interactive device, for receiving the configuration information to the micro-reactor apparatus；

   The controller, for according to the field data collected, and/or the configuration information received, generation control Signal processed, with to the raw material input process of the micro-reactor apparatus, flow control process, temperature controlled processes, line clear mistake At least one of journey, output of products process, security protection detection process are controlled.
2. 2. system according to claim 1, it is characterised in that wherein,

   The field data, including：In flow, temperature, pressure, liquid level, weight, live video information, status information at least One of；

   And/or

   The configuration information, including：Production requirement, raw material parameter, target flow, target temperature, target level, cleaning parameter, At least one of security protection parameter.
3. 3. system according to claim 1, it is characterised in that also include：Performs device；

   The performs device, for controlling under the control of said control signal the raw material input process, the flow During journey, the temperature controlled processes, the line clear process, the output of products process, the security protection detection at least One of control.
4. 4. system according to claim 3, it is characterised in that the performs device, including：Servo-drive system, heat-exchange system, At least one of cleaning systems, control valve；Wherein,

   The servo-drive system, it is real for the raw material input flow rate and/or output of products flow by controlling the micro-reactor apparatus Now to the control of the flow control process；

   The heat-exchange system, for by controlling cold medium flux, realizing the control to the temperature controlled processes；

   The cleaning systems, for by controlling cleaning mode, realizing the control to the line clear process；

   The control valve, for entering auxiliary at least one of the servo-drive system, the heat-exchange system, the cleaning systems Control.
5. 5. according to the system described in one of claim 1-4, it is characterised in that the harvester, including：Flow sensor, At least one of temperature sensor, pressure sensor, liquid level sensor, weight sensor, video acquisition system；Wherein,

   The flow sensor, for gathering in the raw material input flow rate of the micro-reactor apparatus, output of products flow at least One of；

   The temperature sensor, for gathering in the reaction temperature of the micro-reactor apparatus, the refrigerant temperature of heat-exchange system extremely It is one of few；

   The pressure sensor, the base pressure of the raw material input pod for gathering the micro-reactor apparatus, reaction channel At least one of loine pressure, base pressure of output of products container；

   The liquid level sensor, the liquid level of the raw material input pod for gathering the micro-reactor apparatus, the medium of reaction channel At least one of liquid level, liquid level of output of products container；

   The weight sensor, for gathering in the raw material input weight of the micro-reactor apparatus, output of products weight at least One of；

   The video acquisition system, in the live video information and status information for gathering the micro-reactor apparatus at least it One.
6. 6. according to the system described in one of claim 1-4, it is characterised in that the harvester, in addition to：Analog acquisition Module；

   The analogue collection module, for being carried out to the field data collected in data conversion, signal filtering extremely A kind of few processing；

   And/or

   The controller, including：At least one of industrial computer, single-chip microcomputer, DSP Processor, PLC.
7. 7. according to the system described in one of claim 1-4, it is characterised in that also include：Memory cell；

   The memory cell, for the composition of raw material and the corresponding relation of density for storing the micro-reactor apparatus；

   And/or

   The interactive device, be additionally operable to in the field data collected, the configuration information received at least it One is shown；And/or export prompt message during the security protection detection.
8. 8. according to the system described in one of claim 1-4, it is characterised in that the interactive device, including：First display is single At least one of member, the second display unit, Tip element；

   First display unit, for receiving the configuration information to the micro-reactor apparatus；

   And/or

   Described second aobvious unit, in the field data collected, the configuration information received at least it One is shown；

   And/or

   The Tip element, for initiating the prompt message of at least one of voice, acousto-optic form.
9. 9. according to the system described in one of claim 1-4, it is characterised in that the interactive device, in addition to：Analog input At least one of module, analog output module, I/O input/output modules；Wherein,

   The Analog input mModule, for when the interactive device also includes the first display unit, being shown to described first single After the configuration information that member receives is changed, input to the controller；

   And/or

   The analog output module, for when the system also includes performs device, simulation control to be exported to the performs device Amount processed；

   And/or

   The I/O input/output modules, the switching value information sent for receiving the controller；And/or when the system is also wrapped When including performs device, the on-off model is exported at least one of the interactive device, the performs device.