CN207071303U - Ozone purifying plant and ozone purification system - Google Patents

Ozone purifying plant and ozone purification system Download PDF

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Publication number
CN207071303U
CN207071303U CN201720799263.2U CN201720799263U CN207071303U CN 207071303 U CN207071303 U CN 207071303U CN 201720799263 U CN201720799263 U CN 201720799263U CN 207071303 U CN207071303 U CN 207071303U
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China
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ozone
condenser pipe
purifying plant
sleeve pipe
described sleeve
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CN201720799263.2U
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Chinese (zh)
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孙丙礼
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Baoding Race Scientific Instrument Research And Development Co Ltd
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Baoding Race Scientific Instrument Research And Development Co Ltd
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Abstract

The utility model discloses a kind of ozone purifying plant and ozone purification system.Including refrigerant storing apparatus, the ozone separator being arranged inside the refrigerant storing apparatus.Ozone separator includes:For the condenser pipe of enclosed construction, including first entrance and first outlet.In the helix tube that the condensation inner axial tube is set, the helix tube includes second entrance and second outlet.The first entrance and the second entrance UNICOM, cavity and the first outlet UNICOM of the second outlet by the condenser pipe.It is sheathed on the sleeve pipe of the outer wall of the condenser pipe.The outer wall of the inwall of described sleeve pipe and the condenser pipe is arranged at intervals, and described sleeve pipe bottom is provided with heating unit.The mixed gas of ozone and oxygen can realize gas-liquid separation inside the helix tube by the difference of boiling point.The ozone purifying plant by precise control of temperature so as to improve ozone purify purity.

Description

Ozone purifying plant and ozone purification system
Technical field
It the utility model is related to ozone and field occur, more particularly to a kind of ozone purifying plant and ozone purification system.
Background technology
Ozone often is produced using high-pressure process in traditional industry, because the ozone obtained by modes such as high pressures is unable to reach surely Fixed and high concentration, this method are usually used in industrial water purification etc. for the relatively low occasion of concentration requirement.Another kind is silica gel absorption-solution Inhale the method for producing oxygen through of ozone.The method is readily incorporated impurity, general ozone concentration highest 80%.Silica gel particle can greatly increase Add the surface area of absorption ozone.But because adsorption area is big, partial impurities easily mix wherein, cause caused ozone bag Containing except ozone and oxygen others impurity, the further raising of ozone purity is limited.Additionally need and often change silica gel Grain, safeguard that cumbersome and cost is high.
Utility model content
Based on this, it is necessary to for produced in conventional processes ozone purity it is low the problem of, there is provided one kind can produce high-purity The ozone purifying plant and ozone purification system of ozone.
A kind of ozone purifying plant, including:
Refrigerant storing apparatus;
Ozone separator, it is arranged inside the refrigerant storing apparatus, including:
Condenser pipe, is enclosed construction, including first entrance and first outlet;
Helix tube, being set in the condensation inner axial tube, the helix tube includes second entrance and second outlet, and described the One entrance and the second entrance UNICOM, cavity and the first outlet UNICOM of the second outlet by the condenser pipe;
Sleeve pipe, the outer wall of the condenser pipe being sheathed on, the outer wall of the inwall of described sleeve pipe and the condenser pipe is arranged at intervals, Described sleeve pipe is provided with heating unit.
In one of the embodiments, the bottom of the condenser pipe is provided with reservoir, and the diameter of the reservoir is less than The diameter of the condenser pipe.
In one of the embodiments, the heating unit is heating ring, and the heating ring is arranged at described sleeve pipe bottom, The heating ring and the coaxial setting of described sleeve pipe.
In one of the embodiments, the heating ring is laminated structure, and along the reservoir axially to described cold Direction extension where solidifying pipe.
In one of the embodiments, it is provided with sealing ring between the condenser pipe and sleeve pipe.
In one of the embodiments, in addition to it is arranged at the temperature measuring unit of described sleeve pipe bottom.
In one of the embodiments, in addition to be arranged at it is described condensation pipe outer wall explosion-proof monitoring device.
In one of the embodiments, in addition to explosion-proof tank, the refrigerant storing apparatus are arranged inside the explosion-proof tank, The explosion-proof tank is provided with gas escape route.
In one of the embodiments, the refrigerant storing apparatus is provided with liquid level monitoring control device.
A kind of ozone purification system, including ozone generating-device, in addition to described ozone purifying plant, the ozone carry Pure device is connected with the ozone generating-device.
In ozone purifying plant and ozone purification system provided by the utility model, the refrigerant of the ozone purifying plant holds Receive and refrigerant is housed in device, low temperature can be transmitted to the helix tube.The heating unit can transmit high to the helix tube Temperature.The outer wall of the inwall of described sleeve pipe and the condenser pipe is arranged at intervals the speed for being capable of retarding heat transmission, and the heating is single Member can reduce thermograde with the inwall of described sleeve pipe and the spaced cooperation of outer wall of the condenser pipe, so as to accurately control Temperature in helix tube processed.Heat transfer can be made to be more uniformly distributed efficiently.The mixed gas of ozone and oxygen can be by described First entrance realizes gas-liquid separation inside the helix tube into second entrance by the difference of boiling point.The helix tube can Increasing mixed gas, residence time is to increase the heat-exchange time of mixed gas in the helix tube, so as to improve oxygen and smelly The separative efficiency of oxygen.
Brief description of the drawings
Fig. 1 is the ozone purifying plant structure chart that the utility model embodiment provides;
Fig. 2 is the ozone separator front view that the utility model embodiment provides;
Fig. 3 is the ozone separator explosive view that the utility model embodiment provides;
Fig. 4 is the ozone separator profile that the utility model embodiment provides;
Fig. 5 is the ozone purification system structure chart that the utility model embodiment provides;
Fig. 6 is the ozone purification system explosion-proof tank explosive view that the utility model embodiment provides.
Main element symbol description
Ozone purifying plant 10, ozone separator 20, condenser pipe 100, first entrance 110, first outlet 120, liquid storage Groove 130, measurement mouth 140, sleeve pipe 200, sealing ring 210, bakelite geometrical clamp 220, helix tube 300, second entrance 310, second go out Mouthfuls 320, heating unit 330, temperature measuring unit 340, explosion-proof monitoring device 350, ozone purifying plant 10, refrigerant storing apparatus 400, Liquid level monitoring control device 410, high liquid level (HLL) monitoring device 411, low liquid level monitoring arrangement 412, clip 420, lid 430, heating Joint 440, explosion-proof tank 500, gas escape route 510, front shroud 521, implosion guard 522, pressing plate 523, body seal circle 524th, liquid nitrogen ingress interface 525, ozone inlet interface 526, ozone outlet interface 527, pressure tap 528, liquid level monitoring connect Mouth 529, condenser electrode interface 530, LED interface 531, theft-proof box fixture 532, alarm lamp 533, liquid nitrogen entrance 540th, control unit 550, ozone purification system 30, ozone generating-device 600.
Embodiment
In order that the purpose of this utility model, technical scheme and technique effect are more clearly understood, below in conjunction with accompanying drawing pair Specific embodiment of the utility model is described.It should be appreciated that specific embodiment described herein is only explaining this Utility model, it is not used to limit the utility model.
Fig. 1 is referred to, the utility model embodiment provides a kind of ozone purifying plant 10.The ozone purifying plant 10 wraps Include refrigerant storing apparatus 400 and ozone separator 20.The ozone separator 20 is arranged at the refrigerant storing apparatus 400 It is internal.The ozone purifying plant 10 can separate the mixed gas of oxygen and ozone to reach the purpose of purification ozone.It is smelly The boiling point of oxygen is -111 DEG C, and oxygen is that boiling point is -183 DEG C.Using the difference of ozone and oxygen boiling point, purified by the ozone Device 10 separates the ozone and oxygen.
Fig. 2-4 are referred to, the ozone separator 20 includes condenser pipe 100, sleeve pipe 200, helix tube 300, Yi Jijia Hot cell 330.Described sleeve pipe 200 is sheathed on the outer wall of the condenser pipe 100.The inwall of described sleeve pipe 200 and the condenser pipe 100 outer wall is arranged at intervals.The helix tube 300 is axially arranged in the condenser pipe 100.The condenser pipe 100 includes the One entrance 110 and first outlet 120.The helix tube 300 includes second entrance 310 and second outlet 320.Described first enters Mouth 110 and the UNICOM of second entrance 310.The cavity and described first that the second outlet 320 passes through the condenser pipe 100 Export 120 UNICOMs.The heating unit 330 is arranged at the bottom of described sleeve pipe 200.
The condenser pipe 100 is enclosed construction.The condenser pipe 100 can be hollow cylindrical structure, or empty Body-centred cube structure.One end of the condenser pipe 100 can be cecum.The first entrance 110 and the first outlet 120 The other end of the condenser pipe 100 can be arranged at.The first entrance 110 can be used for being passed through oxygen and ozone gaseous mixture Body.The first outlet 120 is used to export oxygen or ozone gas.The other end of the condenser pipe 100 can also set measurement Mouth 140.Measuring appliance can be entered inside the condenser pipe 100 by the measurement mouth 140, for measuring the condenser pipe Running parameter inside 100, can also be as the entrance of explosion-proof monitoring device 350.It is appreciated that the measurement mouth 140 also may be used Using the entrance as heating unit 330.The condenser pipe 100 can be by quartz glass, hard organic material or metal material It is made.In one embodiment, the condenser pipe 100 is quartz glass tube.
The helix tube 300 to make enter the helix tube 300 in oxygen and ozone separation.The refrigerant accommodates dress Low temperature can be passed to the helix tube 300 by putting 400.The helix tube 300 can also be in the heating of the heating unit 330 Under bring up to and can separate the temperature of oxygen and ozone to separate ozone and oxygen.The helix tube 300 can increase gaseous mixture Body residence time in the helix tube 300 to increase the heat-exchange time of mixed gas, improves the separation effect of oxygen and ozone Rate.The helix tube 300 can have less pitch to increase heat exchange area.The helix tube 200 can be by quartz glass It is made.Preferably, the helix tube 200 can be provided with angular structures close to the side wall of the reservoir 130.After ozone liquefaction Drop stress mutation can occur in surface after the position of the angular structures is flow to, can speed up ozone drop enter described in Reservoir 130.The helix tube 200 can be with the 100 coaxial setting of condenser pipe.The outer wall of the helix tube 200 is in institute Stating the inside of condenser pipe 100 and the inwall of the condenser pipe 100 has spacing distance.The spacing distance can be 15mm- 20mm.When spacing distance is 15mm-20mm, heat is uniformly transferred from the condenser pipe 100 to the helix tube 200, and Violent temperature change is not had, it is safe and efficient.
In one of the embodiments, the bottom of the condenser pipe 100 can be provided with reservoir 130.The reservoir 130 can be integrally formed with the main body of the condenser pipe 100, can also be assembled as single part with the condenser pipe 100 Shaping.The reservoir 130 can be made up of quartz glass, or ceramic material is made.One end of the reservoir 130 Connected with the condenser pipe 100, the other end of the reservoir 130 is cecum.The reservoir 130 can be hollow cylinder Body structure, or hollow cube structure.Preferably, the reservoir 130 is hollow round table structure.The hollow round table Structure includes parallel upper bottom surface and bottom surface, and the area of upper bottom surface is more than the area of bottom surface.The upper bottom surface with it is described cold The cavity connection of solidifying pipe 100.Hollow round table structure can be in order to which the liquid ozone in the hollow round table structure be to Back stroke Hair, improve the efficiency of output ozone.The diameter of the reservoir 130 can be less than the diameter of the condenser pipe 100.Ozone is in institute After stating the condensation that exchanged heat in helix tube 300, the reservoir 130 is instilled by the helix tube 300.The reservoir 130 it is straight Footpath is less than the outside that the diameter of the condenser pipe 100 can facilitate the heating unit 300 to be set in the reservoir 130, from And improve the efficiency of heating surface.The diameter of the reservoir 130 can also be not easy oxygen less than the diameter of the condenser pipe 100 simultaneously Mixed into the reservoir 130 with the ozone, be easy to the separation of ozone and oxygen.
Described sleeve pipe 200 is used for the refrigerant and the condenser pipe 100 isolated in the refrigerant storing apparatus 400.The set The shape of pipe 200 can be corresponding with the shape of the condenser pipe 100 in order to which described sleeve pipe 200 is set in the condenser pipe 100 outside.In one of the embodiments, described sleeve pipe 200 can be made up of quartz glass.
The outer wall of the inwall of described sleeve pipe 200 and the condenser pipe 100 be arranged at intervals can with the speed of retarding heat transmission, So as to accurately control the temperature in helix tube 300.Preferably, the inwall of described sleeve pipe 200 and the outer wall of condenser pipe 100 The distance between can be 5mm-10mm.Distance between the inwall and the outer wall of the condenser pipe 100 of described sleeve pipe 200 is During 5mm-10mm, the variable gradient of temperature between described sleeve pipe 200 and the condenser pipe 100 can be slowed down, it is described so as to reduce The risk of the surface temperature cataclysm of condenser pipe 100.The mixed gas of ozone and oxygen can enter the by the first entrance 110 Two entrances 310.Mixed gas can realize gas-liquid separation inside the helix tube 300 by the difference of gas with various boiling point. The heating unit 330 is arranged on the bottom of described sleeve pipe 200., can be from minimum when being heated by the heating unit 330 End is begun to warm up, so as to slowly raise the temperature of the condenser pipe 100.Pass through such special setting so that heating During heat slowly through the space between the inwall and the outer wall of the condenser pipe 100 of described sleeve pipe 200 to described sleeve pipe 200 one end away from the bottom are transmitted, so as to be slowly heated the mixed gas being located in the helix tube 200.At it In middle one embodiment, the space between the inwall of described sleeve pipe 200 and the outer wall of the condenser pipe 100 can be provided with grid, Void space can be divided into some small passage of heats by the grid, so as to so that heat transfer is more uniformly distributed efficiently.Institute The position setting and the gap between described sleeve pipe 200 and the condenser pipe 100 for stating heating unit 330 cooperate, so as to To cause ozone separator 20 of the present utility model slowly, stably to regulate and control to temperature, so as to realize ozone and oxygen Separation, be easy to the accurate control to ozone and oxygen mixed gas.In addition, the heating unit 330 passes through described sleeve pipe 200 Space between the condenser pipe 100 can avoid heating unit with isolating with the refrigerant in the refrigerant storing apparatus 400 330 make the explosion of described sleeve pipe 200 cause danger with the excessive temperature difference of refrigerant.
It is and described also, mixed gas is to be moved along the inwall of the helix tube 200 to the bottom of described sleeve pipe 200 The heat transfer direction contrary of heating unit 330, therefore the utilization ratio of heat energy can be improved, the energy can be saved.
In one of the embodiments, the heating unit 330 is heating ring.The heating ring and described sleeve pipe 200 are same It is axially arranged.The heating ring can be heating the helix tube 300.When needing to separate ozone and oxygen, institute can be passed through State the temperature that the temperature adjustment of the helix tube 300 is less than ozone boiling point by heating ring to the boiling point higher than oxygen.The heating The cyclic structure of ring make it is described heating ring in the condenser pipe 100 helix tube 300 heating be more uniformly distributed, beneficial to heat from The bottom up transmission of described sleeve pipe 200.
In one of the embodiments, the heating ring is laminated structure, and along the reservoir 130 axially to described The place direction of condenser pipe 100 extends.The heating ring of laminated structure can increase heat exchange area, improve the efficiency of temperature transmission.Institute The reservoir 130 can be surrounded after stating the place direction of condenser pipe 100 extension described in heating ring.The heating ring is to the storage Temperature rise after liquid bath 130 heats in the reservoir 130.Oxygen is easier to away from the reservoir 130 at high temperature Direction motion, therefore can accelerate separation speed.
In one of the embodiments, the ozone purifying plant 10 also includes the survey for being arranged at the bottom of described sleeve pipe 200 Warm unit 340.The temperature measuring unit 340 can be with the temperature in condenser pipe described in at-once monitor 100, and is adjusted according to temperature back The heating power of heating unit 330, to realize accurate adjustment separation temperature.In one of the embodiments, the temperature measuring unit 340 can enter the bottom of described sleeve pipe 200 by the measurement mouth 140.Further, the temperature measuring unit 340 can be set In the side wall for the reservoir 130 that the heating unit 300 is surrounded.The temperature measuring unit 340 is arranged on above-mentioned position The temperature of the reservoir 130 can be accurately measured, it is single so as to be heated described in the temperature adjustment according to the reservoir 130 The heating power of member 330.When needing ozone gas, the temperature of liquid ozone can be accurately improved, so that liquid ozone It is changed into gaseous ozone.
In one of the embodiments, the ozone purifying plant 10 also includes being arranged at the outer wall of condenser pipe 100 Explosion-proof monitoring device 350.When explosion time occurs for system, the explosion-proof monitoring device 350 can make company by safety mutually-locking device The pneumatic operated valve for connecing external device is closed automatically, so as to protect cavity and related pump group.
Refrigerant in the refrigerant storing apparatus 400 can be liquid nitrogen.The refrigerant storing apparatus 400 can include lid 430.The lid 430 is sealing the refrigerant storing apparatus 400.The refrigerant storing apparatus 400 can include clip 420, the clip 420 is used to fix the ozone separator 20.The inwall of described sleeve pipe 200 and the condenser pipe 100 Outer wall, which is arranged at intervals, can slow down the speed conducted heat between described sleeve pipe 200 and the condenser pipe 100, improve the precision of temperature control. It is appreciated that there can be space between the outer wall of the inwall of described sleeve pipe 200 and the condenser pipe 100.Can in the space With the non-conductor of filling heat.
In one of the embodiments, after the sealing ring 210 seals described sleeve pipe 200 and the condenser pipe 100, Dry air can be sealed between described sleeve pipe 200 and the condenser pipe 100.Dry air cost is low, and poor thermal conductivity can Transmission of the retarding heat between described sleeve pipe 200 and the condenser pipe 100, so as to accurately control the condenser pipe 100 Temperature.After the sealing ring 210 is folded between described sleeve pipe 200 and the condenser pipe 100, it can be fixed by bakelite Folder 220 is fixedly connected with described sleeve pipe 200 and the condenser pipe 100.The bakelite geometrical clamp 220 can pass through fastening screw and spiral shell Mother is fixed.The bakelite geometrical clamp 220 has certain elasticity, is not easy that described sleeve pipe 200 and the condenser pipe 100 are caused to hinder Evil.The refrigerant storing apparatus 400 can include two bar shaped observation windows to observe inside the refrigerant storing apparatus 400 Situation.The heating unit 330 can be connected by heating, vacuum joint with control system.The heating, vacuum joint can be KF16 joints, the purpose of the sealing of high vacuum can be reached.Control system can also by the heating, vacuum joint with it is explosion-proof Supervising device connects.
Adjustment height pad can be provided between the ozone separator 20 and the refrigerant storing apparatus 400.Institute It can be U-shaped teflon gasket to state adjustment height pad.The one piece of use of several 1mm, 2mm, 5mm, 10mm pads is The regulation height of ozone separator 20 can be haveed the function that, the work for buffering the ozone separator 20 can also be played With, while also reduce the stress between the ozone separator 20 and the refrigerant storing apparatus 400.
In one of the embodiments, the refrigerant storing apparatus 400 is provided with liquid level monitoring control device 410.It is described Liquid level monitoring control device 410 can also include high liquid level (HLL) monitoring device 411 and low liquid level monitoring arrangement 412.The high liquid level (HLL) Monitoring device 411 can include the closed tubule in one end and the thermocouple for thermometric.The thermocouple is placed in tubule.Work as liquid nitrogen When liquid level did not had the thermocouple, the temperature of thermocouple reaches liquid nitrogen temperature.The high liquid level (HLL) monitoring device 411 passes through Temperature-control Monitoring table Lowest temperature is set, and when reaching lowest temperature, temp controlled meter sends lower limit alarm signal, and automatically turns on liquid nitrogen perfusion system.Institute Liquid nitrogen perfusion system is stated when receiving this signal, stops pouring into for liquid nitrogen.The low liquid level monitoring arrangement 412 can be used for controlling The automatic of liquid nitrogen pours into.The low liquid level monitoring arrangement 412 can also include the closed tubule in one end and the thermocouple for thermometric. The thermocouple is placed in tubule.The preset temperature upper limit, when liquid nitrogen liquid level is less than thermocouple, the temperature of the thermocouple will be above liquid Nitrogen temperature.Upper limit alarm signal is sent when the temperature of thermocouple sensing reaches temperature upper limit, and opens automatic liquid nitrogen perfusion System, start pouring into for liquid nitrogen.Automatic liquid nitrogen perfusion system passes through the high liquid level (HLL) monitoring device 411 and the low liquid level monitoring Device 412 and control program can automatically control the perfusion of liquid nitrogen.Liquid nitrogen liquid level is maintained between low liquid level and high liquid level (HLL) to protect Card system liquid nitrogen liquid level is operated in safe range always.
Fig. 5-6 are referred to, in one of the embodiments, the ozone purifying plant 10 also includes explosion-proof tank 500.Institute Refrigerant storing apparatus 400 is stated to be arranged inside the explosion-proof tank 500.The explosion-proof tank 500 can prevent from accommodating in the refrigerant The explode backward environment of device 400 splashes the external world is damaged.The explosion-proof tank 500 is provided with gas escape route 510.Institute State gas escape route 510 and be directly connected to exhaust emission tube road.Exhaust emission tube road can be with connecting inside the explosion-proof tank 500 It is logical.Therefore the gas escape route 510 can avoid outside vapor and air enter explosion-proof tank 500 inside cause steam to coagulate Knot, while the equilibrium of inside and outside atmospheric pressure can be maintained.
It is front shroud 521 that the front of explosion-proof tank 500 can also include setting gradually, implosion guard 522, pressing plate 523, main Body sealing ring 524.The front shroud 521 can also be included to control the control unit that the ozone purifying plant 20 works 550, to the alarm lamp 533 alarmed.The side wall of the explosion-proof tank 500 can include liquid nitrogen ingress interface 525, ozone enters Mouth interface 526, ozone outlet interface 527, pressure tap 528, liquid level monitoring interface 529, condenser electrode interface 530, LED Lamp interface 531, liquid nitrogen entrance 540.The bottom of the explosion-proof tank 500 is additionally provided with to the antitheft of the fixation explosion-proof tank 500 Case fixture 532.
The utility model embodiment also provides a kind of ozone purification system 30.The ozone purification system 30 is sent out including ozone Generating apparatus 600 and described ozone purifying plant 10.The ozone separator 20 connects with the ozone generating-device 600 Connect.The mixed gas of ozone and oxygen caused by the ozone generating-device 600 can pass through the first entrance 110 and and institute State second entrance 310 and enter the helix tube 300.After the mixture of the ozone and oxygen separates in the helix tube 300, The ozone that liquefies is collected in the reservoir 130, and oxygen enters the cavity of the condenser pipe 100 by the second outlet 320 In, and moved to the direction away from the condenser pipe 100, the condenser pipe 100 is then discharged by the first outlet 120.
The industrial ozone generator that the ozone generating-device 600 can seal using VCR.The ozone occurs Device can reach the sealing of ultrahigh vacuum, can ensure ozone purity.Ozonation system electronic control unit 550 can using PLC as Core, mainly it is made up of precision DC source, vacuum gauge, pneumatic operated valve and safety protection circuit.Intelligent control formula can read temperature The parameters such as degree, pressure, run according to the control model that user is set on touch screen and parameter.The ozone generator Add all multiple securities mechanisms, it is ensured that the safety of system and stably.
The ozone purification system 30 can also include ozonation system gas circuit.The ozonation system gas circuit includes pipeline, machine Tool pump, valve etc..The ozone purification system 30 may provide for the gas circuit control of oxygen, nitrogen, ozone etc. and safety is protected The function of shield.
The utility model embodiment also provide it is a kind of using the ozone purification system 30 purify ozone method, including with Lower step:
S110, the ozone separator 20 is soaked in the refrigerant storing apparatus 400 for filling liquid nitrogen;
S120, the condenser pipe 100 is heated by the heating unit 330, the condenser pipe 100 is warming up to oxygen Temperature among gas boiling point and the ozone boiling point;
S130, the mixed gas of ozone and oxygen is passed through the condenser pipe 100 and separated.
The ozone separator 20 is soaked in and fills the refrigerant storing apparatus 400 of liquid nitrogen and can make the ozone The temperature of separator 20 reaches the temperature of liquid nitrogen., can be by described when needing to separate the mixed gas of the ozone and oxygen Heating unit 330 heats to the condenser pipe 100 so that the condenser pipe 100 is warming up to oxygen boiling point and is boiled with the ozone Temperature among point, in said temperature section, gaseous ozone can be condensed into liquid ozone.The boiling point of oxygen is less than ozone Boiling point, oxygen remain in that gaseous state.Therefore the mixed gas of ozone and oxygen is passed through into the condenser pipe 100 to be separated, can So that ozone is stayed in the ozone separator 20, oxygen is discharged from the ozone separator 20.Reach efficient purification The purpose of ozone.
In the step 120, the temperature of the condenser pipe 100 can be adjusted between -111 DEG C, -183 DEG C.Preferably, institute The temperature control of condenser pipe 100 is stated at -140 DEG C to -150 DEG C, the separating effect of ozone and oxygen is best.
In step s 130, collected after ozone liquefaction in the reservoir 130.The oxygen is from the second outlet 320 export and are discharged by the cavity of the condenser pipe 100 from the first outlet 120.In one of the embodiments, it is described First outlet 120 can be connected with aspiration pump.Further, the mixed gas can pass through the ozone generating-device 600 Electrion obtains.
The mixed gas of ozone and oxygen is passed through during the condenser pipe separated, the temperature measuring unit 340 The temperature inside described sleeve pipe can be monitored in real time with the heating-up temperature of heating unit described in feedback control 330.
The explosion-proof monitoring device 350 can be connected and interlock with ozone generating-device 600.If inside described sleeve pipe 200 Break down, the explosion-proof monitoring device 350 sends signal to the ozone generating-device 600 makes the ozone generating-device 600 are stopped.
In step s 130, the liquid level monitoring control device 410 can monitor in the refrigerant storing apparatus 400 in real time Coolant quantity:
The ozone purification system also includes Temperature-control Monitoring table.Temperature upper limit and temperature are set by the Temperature-control Monitoring table Spend lower limit;
When the temperature that the high liquid level (HLL) monitoring device 411 monitors is temperature upper limit value, sends signal and stop refrigerant filling Injection system injects refrigerant to the refrigerant storing apparatus 400;
When the temperature that the low liquid level monitoring arrangement 412 monitors is temperature upper limit, it is automatic cold to send signal unlatching Matchmaker irrigates system, starts to inject refrigerant to the refrigerant storing apparatus 400.
After the mixed gas separation of the ozone and oxygen, stop the heating unit 330 and heat, by the condenser pipe 100 temperature recalls to the temperature of refrigerant with safe storage refrigerant again.
During using ozone after purification, heated by the heating unit 330, make the temperature of the condenser pipe 100 to smelly More than oxygen boiling point, liquid ozone is changed into gaseous ozone, and by the first outlet 120, outwardly equipment exports.Described in use Before ozone, the amount of collection ozone can be intuitively observed by being arranged at the bar shaped viewing mask of the ozone purifying plant 10. Preferably, the supply of ozone can be accurately and stably controlled by the height and valve for controlling temperature.
It should be noted that when element is referred to as " being fixed on " another element, it can be directly on another element Or there may also be element placed in the middle.When an element is considered as " connection " another element, it can be directly connected to To another element or it may be simultaneously present centering elements.On the contrary, when element be referred to as " directly existing " another element " on " when, In the absence of intermediary element.Term as used herein " vertically ", " horizontal ", "left", "right" and similar statement are For illustrative purposes.
Embodiment described above only expresses several embodiments of the present utility model, and its description is more specific and detailed, But therefore it can not be interpreted as the limitation to the utility model patent scope.It should be pointed out that for the common of this area For technical staff, without departing from the concept of the premise utility, various modifications and improvements can be made, these all belong to In the scope of protection of the utility model.Therefore, the protection domain of the utility model patent should be determined by the appended claims.

Claims (10)

  1. A kind of 1. ozone purifying plant, it is characterised in that including:
    Refrigerant storing apparatus (400);
    Ozone separator (20), refrigerant storing apparatus (400) inside is arranged at, including:
    Condenser pipe (100), is enclosed construction, including first entrance (110) and first outlet (120);
    Helix tube (300), axially arranged in the condenser pipe (100), the helix tube (300) includes second entrance (310) With second outlet (320), the first entrance (110) and the second entrance (310) UNICOM, the second outlet (320) are led to Cross cavity and the first outlet (120) UNICOM of the condenser pipe (100);
    Sleeve pipe (200), it is sheathed on the outer wall of the condenser pipe (100), inwall and the condenser pipe of described sleeve pipe (200) (100) outer wall is arranged at intervals, and described sleeve pipe (200) is provided with heating unit (330).
  2. 2. ozone purifying plant as claimed in claim 1, it is characterised in that the bottom of the condenser pipe (100) is provided with storage Liquid bath (130), the diameter of the reservoir (130) are less than the diameter of the condenser pipe (100).
  3. 3. ozone purifying plant as claimed in claim 2, it is characterised in that the heating unit (330) is heating ring, described Heating ring is arranged at described sleeve pipe (200) bottom, the heating ring and described sleeve pipe (200) coaxial setting.
  4. 4. ozone purifying plant as claimed in claim 3, it is characterised in that the heating ring is laminated structure, and along described Reservoir axially extends to direction where the condenser pipe (100).
  5. 5. ozone purifying plant as claimed in claim 1, it is characterised in that the condenser pipe (100) and described sleeve pipe (200) Between be provided with sealing ring (210).
  6. 6. ozone purifying plant as claimed in claim 1, it is characterised in that also include being arranged at described sleeve pipe (200) bottom Temperature measuring unit (340).
  7. 7. ozone purifying plant as claimed in claim 1, it is characterised in that also include being arranged at the condenser pipe (100) outside The explosion-proof monitoring device (350) of wall.
  8. 8. ozone purifying plant as claimed in claim 1, it is characterised in that also accommodated including explosion-proof tank (500), the refrigerant Device (400) is arranged at the explosion-proof tank (500) inside, and the explosion-proof tank (500) is provided with gas escape route (510).
  9. 9. ozone purifying plant as claimed in claim 1, it is characterised in that the refrigerant storing apparatus (400) is provided with liquid Face monitor controller (410).
  10. 10. a kind of ozone purification system, including ozone generating-device (600), it is characterised in that also include such as claim 1-9 Ozone purifying plant (10) described in any one, the ozone purifying plant (10) are connected with the ozone generating-device (600).
CN201720799263.2U 2017-07-04 2017-07-04 Ozone purifying plant and ozone purification system Active CN207071303U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720799263.2U CN207071303U (en) 2017-07-04 2017-07-04 Ozone purifying plant and ozone purification system

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Application Number Priority Date Filing Date Title
CN201720799263.2U CN207071303U (en) 2017-07-04 2017-07-04 Ozone purifying plant and ozone purification system

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Publication Number Publication Date
CN207071303U true CN207071303U (en) 2018-03-06

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109200737A (en) * 2017-07-04 2019-01-15 保定赛印科学仪器研发有限公司 Ozone purifying plant and ozone purification system
CN112538637A (en) * 2020-11-23 2021-03-23 珠海格力电器股份有限公司 Ozone generating device, control method and refrigerator

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109200737A (en) * 2017-07-04 2019-01-15 保定赛印科学仪器研发有限公司 Ozone purifying plant and ozone purification system
CN109200737B (en) * 2017-07-04 2024-04-26 保定赛印科学仪器研发有限公司 Ozone purification device and ozone purification system
CN112538637A (en) * 2020-11-23 2021-03-23 珠海格力电器股份有限公司 Ozone generating device, control method and refrigerator
CN112538637B (en) * 2020-11-23 2023-08-08 珠海格力电器股份有限公司 Ozone generating device, control method and refrigerator

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