CN207056515U - A kind of novel reaction kettle - Google Patents
A kind of novel reaction kettle Download PDFInfo
- Publication number
- CN207056515U CN207056515U CN201721027230.2U CN201721027230U CN207056515U CN 207056515 U CN207056515 U CN 207056515U CN 201721027230 U CN201721027230 U CN 201721027230U CN 207056515 U CN207056515 U CN 207056515U
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- reaction kettle
- valve
- kettle body
- feed hose
- tracheae
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Abstract
The utility model provides a kind of novel reaction kettle, including reaction kettle body, reaction kettle body top side are provided with guide mouth, and feed hose is connected with guide mouth, and feed hose one end and the tight-lipped close connection of guide, the feed hose other end are connected with suction nozzle；The top of reaction kettle body is provided with and vacuumizes valve, vacuumize the handle that air valve is provided with valve and controls air valve switch, vacuumize and aspiration pump is connected with by tracheae on valve, tracheae one end, which is connected with, to vacuumize the external screw thread that is correspondingly provided with and can be threadedly coupled with above-mentioned threaded connector on valve with vacuumizing the threaded connector of valve dismantling connection.The purpose of this utility model is to provide a kind of simple in construction, convenient reactor of charging.
Description
Technical field
It the utility model is related to consersion unit technical field, more particularly to a kind of novel reaction kettle.
Background technology
The tetralin musk deer fragrant perfume of tonalid category polycyclic musk, its note are closer to natural macrocyclic musk, preferably
Happy musk odor is more pure, lasting, and there is dense powder fragrance to cease, fragrant of fine quality good, gives people a kind of very comfortable happy sense
Feel.Due to tonalid under acid-base neutralization sunlight it is non-discolouring, most widely used in daily chemical essence, next can be used for cigarette
In hay-scented essence, tonalid has fabulous associativity with fabric, though scrubbed, fragrance still exists, and is usually used in washing essence
In, tonalid synthesis is convenient, and cheap, its product boiling point is relatively low, has the characteristics of lasting is lasting, while tonalid is met
Light does not add lustre to non-discolouring, therefore it has more superior working condition and higher economic valency than macrocyclic musk and nitro musk
Value.The synthesis of tonalid is typically broadly divided into two steps, first, by toluene or the derivative and alkene, alcohol initial ring of contraposition substitution
Change, generation intermediate hexamethyl tetrahydronaphthalene (HMT)；Second, HMT dealings with alcohol, using Fu's formula acylation reaction, preparation, which is told, receives musk deer
Fragrant (AHMT), typically also needs to add corresponding catalyst in whole preparation process.Therefore in view of this, for how to find
Just it is particularly important to a kind of simple in construction, convenient reactor structure of charging.
In the prior art, reaction kettle body bottom is provided with discharge gate, and discharge gate is in communication with the outside by a drainage conduit, drainage conduit
On outlet valve is installed, during discharge, the bottom in reactor is easily sticked in after the residue cooling of reaction kettle body bottom；In discharge
Afterwards, because temperature reduces, there is the material of residual in outlet valve, and outlet valve is typically switched using rotatable handle, adhesion has material
Valve element easily infringement, it is necessary to often change outlet valve, the production and processing to reactor is made troubles.Therefore, for how to seek
It is convenient to find a kind of discharging, reduces the reactor structure that material remains and is just particularly important.
The content of the invention
The purpose of this utility model is overcome the deficiencies in the prior art, there is provided one kind is simple in construction, charging is convenient anti-
Answer kettle.
Another object of the present utility model is to improve reactor discharging knot on the basis of aforesaid reaction vessel feeding structure
Structure, to extend the service life of reactor outlet valve.
To achieve the above object, technical scheme provided by the utility model is：
A kind of novel reaction kettle, including reaction kettle body, it is characterised in that：Reaction kettle body top side is provided with guide
Mouth, feed hose is connected with guide mouth, and feed hose one end and the tight-lipped close connection of guide, the feed hose other end are connected with suction
Mouth；The top of reaction kettle body is provided with and vacuumizes valve, vacuumizes the handle that air valve is provided with valve and controls air valve switch,
Vacuumize and aspiration pump is connected with by tracheae on valve, tracheae one end, which is connected with, to be connected with vacuumizing the screw thread of valve dismantling connection
Joint, vacuumize the external screw thread that is correspondingly provided with and can be threadedly coupled with above-mentioned threaded connector on valve.
A kind of novel reaction kettle as described above, it is characterised in that：The reaction kettle body bottom is provided with discharge gate, reaction kettle body
Bottom outside has the assisted heating structure set around discharge gate excircle, and assisted heating structure adds with the reaction on reaction kettle body
Thermal is independently set, and discharge gate is in communication with the outside by a drainage conduit, and outlet valve is provided with drainage conduit.
A kind of novel reaction kettle as described above, it is characterised in that：The outlet valve is placed in an incubator, in incubator also
Provided with electric heater unit.
A kind of novel reaction kettle as described above, it is characterised in that：The assisted heating structure be high temperature oil heat pipeline or
Electrical heating wire or high-temperature steam heating pipeline.
The utility model beneficial effect：
1st, the top side of reaction kettle body is provided with guide mouth, is connected with feed hose on guide mouth, feed hose one end with
The tight-lipped close connection of guide, the feed hose other end are connected with suction nozzle；The top of reaction kettle body is provided with and vacuumizes valve, vacuumizes gas
Air valve is installed on mouth and controls the handle of air valve switch, vacuumizes and aspiration pump, tracheae one is connected with by tracheae on valve
End, which is connected with, to be vacuumized with vacuumizing the threaded connector of valve dismantling connection and be correspondingly provided with and can connect with above-mentioned screw thread on valve
The external screw thread of joint screw thread connection, when the structure design to need charging, can be vacuumized to reactor by aspiration pump, made
Obtain and negative pressure is formed in reactor, so extraneous material can be entered in reactor by suction nozzle, feed hose, guide mouth, be tied
Structure is simple, conveniently middle to add materials.
2nd, reaction kettle body bottom is provided with discharge gate, and reaction kettle body bottom outside has the auxiliary set around discharge gate excircle
Heating arrangement, assisted heating structure are independently set with the reaction heater on reaction kettle body, and discharge gate passes through a discharge
Pipe is in communication with the outside, and outlet valve is provided with drainage conduit, and outlet valve is placed in an incubator, and electrical heating dress is additionally provided with incubator
Put.When discharge is to coda, assisted heating device is begun to warm up, and the electric heater unit in incubator is initially powered up heating, such thing
Material is in liquid all the time, when temperature is low, can effectively avoid material from being remained in reactor bottom and outlet valve, discharge is more dry
Only, residue is few in outlet valve, is advantageous to extend the service life of outlet valve.
Brief description of the drawings
Fig. 1 is the utility model structure diagram.
Embodiment
With reference to specific embodiment, the utility model is described in further detail：
As shown in figure 1, a kind of novel reaction kettle, including reaction kettle body 1, the top side of reaction kettle body 1 are provided with guide mouth
100, feed hose 101 is connected with guide mouth 100, and the one end of feed hose 101 is closely connected with guide mouth 100, feed hose
101 other ends are connected with suction nozzle 102；The top of reaction kettle body 1 is provided with and vacuumizes valve 200, vacuumizes and is provided with valve 200
The handle that air valve 201 and control air valve 201 switch, vacuumizes and is connected with aspiration pump 4, tracheae 3 by tracheae 3 on valve 200
One end be connected with can with vacuumize the threaded connector 31 of valve dismantling connection, vacuumize be correspondingly provided with valve 200 can with it is upper
State the external screw thread of the threaded connection of threaded connector 31.The utility model is preferable to carry out in example, and reaction kettle body 1 is by that can be fitted close
Kettle body 11 and kettle cover 21 form, guide mouth 100 be arranged in kettle body 11 and with reactor inside connect, vacuumize valve 200
It is arranged on kettle cover 21.
In use, suction nozzle 102 is immersed in material liquid bucket, aspiration pump 4 is evacuated, and the air pressure in reaction kettle body 1 reduces, material
Material liquid in liquid bucket enters in reaction kettle body 1 through suction nozzle 102, feed hose 101 and guide mouth 100, completes the addition of feed liquid,
Simple in construction, addition is convenient.
Further improve：The bottom of reaction kettle body 1 is provided with discharge gate, and the bottom outside of reaction kettle body 1 has cylindrical around discharge gate
The assisted heating structure 5 that week is set, assisted heating structure 5 are independently set with the reaction heater 13 on reaction kettle body 1,
Discharge gate is in communication with the outside by a drainage conduit 301, and outlet valve 6 is provided with drainage conduit 301, and outlet valve 6 is placed in an incubator 7
It is interior, it is additionally provided with electric heater unit in incubator 7.
Assisted heating structure 5 can be that high temperature oil heats pipeline or electrical heating wire or high-temperature steam heats pipeline.This practicality is new
In type, 5 preferred high temperature oil of assisted heating structure heating pipeline, high temperature oil heating pipeline two ends are respectively equipped with high temperature oil joint
51。
Examples of implementation described above are only the preferred embodiment of the utility model, are not limited with this of the present utility model
Practical range, therefore the change that all shape, principles according to the utility model are made, all should cover in the scope of protection of the utility model
It is interior.
Claims (4)
1. a kind of novel reaction kettle, including reaction kettle body, it is characterised in that：Reaction kettle body top side is provided with guide mouth,
Feed hose is connected with guide mouth, feed hose one end and the tight-lipped close connection of guide, the feed hose other end are connected with suction nozzle；
The top of reaction kettle body is provided with and vacuumizes valve, vacuumizes the handle that air valve is provided with valve and controls air valve switch, takes out
Aspiration pump is connected with by tracheae on vacuum valve, tracheae one end is connected with can be with vacuumizing the threaded connection of valve dismantling connection
Head, vacuumize the external screw thread that is correspondingly provided with and can be threadedly coupled with above-mentioned threaded connector on valve.
A kind of 2. novel reaction kettle according to claim 1, it is characterised in that：The reaction kettle body bottom is provided with discharge gate,
Reaction kettle body bottom outside has an assisted heating structure set around discharge gate excircle, on assisted heating structure and reaction kettle body
Reaction heater independently set, discharge gate is in communication with the outside by a drainage conduit, and outlet valve is provided with drainage conduit.
A kind of 3. novel reaction kettle according to claim 2, it is characterised in that：The outlet valve is placed in an incubator, is protected
Electric heater unit is additionally provided with incubator.
A kind of 4. novel reaction kettle according to claim 2, it is characterised in that：The assisted heating structure heats for high temperature oil
Pipeline or electrical heating wire or high-temperature steam heating pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721027230.2U CN207056515U (en) | 2017-08-16 | 2017-08-16 | A kind of novel reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721027230.2U CN207056515U (en) | 2017-08-16 | 2017-08-16 | A kind of novel reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207056515U true CN207056515U (en) | 2018-03-02 |
Family
ID=61515598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721027230.2U Active CN207056515U (en) | 2017-08-16 | 2017-08-16 | A kind of novel reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207056515U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115322835A (en) * | 2022-08-11 | 2022-11-11 | 黄山市巨龙生物能源科技有限公司 | Integrated device for extracting fir essential oil and extraction method |
-
2017
- 2017-08-16 CN CN201721027230.2U patent/CN207056515U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115322835A (en) * | 2022-08-11 | 2022-11-11 | 黄山市巨龙生物能源科技有限公司 | Integrated device for extracting fir essential oil and extraction method |
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