CN206996525U - A kind of firpene isomerization reaction tank - Google Patents
A kind of firpene isomerization reaction tank Download PDFInfo
- Publication number
- CN206996525U CN206996525U CN201720620078.2U CN201720620078U CN206996525U CN 206996525 U CN206996525 U CN 206996525U CN 201720620078 U CN201720620078 U CN 201720620078U CN 206996525 U CN206996525 U CN 206996525U
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- Prior art keywords
- agitating shaft
- firpene
- tank body
- tank
- isomerization reaction
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Abstract
The utility model discloses a kind of firpene isomerization reaction tank, including tank body, stirring motor and charging aperture are provided with the top of the tank body, the tank interior is provided with agitating shaft, the agitating shaft is extended at the top of the tank body by the tank interior and is connected with the stirring motor, fixed rack is provided with the agitating shaft, the fixed rack is internally provided with accommodating cavity, the sieve aperture for connecting the tank interior and the accommodating cavity is provided with the fixed rack, catalyst is filled with the accommodating cavity, the bottom of the agitating shaft is provided with auger piece, the radius of spin of auger piece gradually expands from the bottom up along agitating shaft, the tank interior is provided with heating coil, the heating coil is set around the auger piece, extend the tank body to form oil inlet and oil-out in the both ends of the heating coil.The utility model, which aims to solve the problem that, has the problem of reaction efficiency is low, and filler easily blocks in existing firpene isomerization reaction.
Description
Technical field
It the utility model is related to firpene technical field of processing equipment, and in particular to a kind of firpene isomerization reaction tank.
Background technology
The turpentine oil overwhelming majority of China's production is masson pine gum turpentine, and its main component is A-Pinene.A-Pinene is
Important industrial chemicals, the A-Pinene of artificial camphor, terpinol, linalool, terpene resin and spices etc. are two ring monoterpenes, can be occurred
A variety of chemical reactions such as isomery, addition, oxidation, wherein isomerization reaction are an important chemical property of A-Pinene.
Catalytic isomerization is the most of research in A-Pinene isomerization reaction, and the performance of catalyst determines the side of isomerization reaction
Be solid catalyst to, wherein most catalyst, in existing firpene isomerization reaction substantially by by firpene at high temperature
The filler for being mounted with catalyst is flowed through to be reacted, and this kind of reactive mode reaction efficiency is relatively low, and firpene flow velocity is slower, when long
Between after use, filler easily blocks, and influences the catalytic efficiency of isomery sensing.
Utility model content
For above-mentioned technical problem, the utility model provides a kind of firpene isomerization reaction tank, existing to solve
The problem of reaction efficiency is low, and filler easily blocks in firpene isomerization reaction be present, devise a kind of new firpene isomery
Retort, the firpene isomerization reaction tank can be such that firpene fully flows with catalyst to contact, and improve reaction efficiency.
A kind of firpene isomerization reaction tank, including tank body, the tank body top are provided with stirring motor and charging aperture, the tank
Body is internally provided with agitating shaft, the agitating shaft extended to by the tank interior at the top of the tank body and with the stirring motor
Connect, be provided with fixed rack on the agitating shaft, the fixed rack is internally provided with accommodating cavity, set on the fixed rack
The sieve aperture for connecting the tank interior and the accommodating cavity is equipped with, catalyst is filled with the accommodating cavity, the agitating shaft
Bottom is provided with auger piece, and the radius of spin of auger piece gradually expands from the bottom up along agitating shaft, in the tank body
Portion is provided with heating coil, and the heating coil is set around the auger piece, and the both ends of the heating coil are extended
The tank body is to form oil inlet and oil-out.
Further, the bottom of the tank body is provided with discharging opening.
Further, the quantity of the fixed rack is 2, presents down and is arranged on the agitating shaft.
Further, it is provided with insulation jacket on the outer wall of the tank body.
This firpene isomerization reaction tank is heated by being arranged at the heating coil of bottom to firpene, reaches isomery institute
The reaction temperature needed, the fixation rack that will be filled with catalyst are arranged on agitating shaft, and the catalyst is preferably that fixation is urged
Agent, such as acid clay, titanium oxide hydrate, the rotation of the agitating shaft is driven by stirring motor, and agitating shaft drives again
The rotation of the fixed rack, so that keeping sufficient relative flow to contact between catalyst and firpene, so as to effectively
Catalytic action of the catalyst to firpene isomerization reaction is improved, while the auger piece for being arranged at shaft bottom can be the bottom of by
The firpene in portion is lifted upward, further improves the mobility of firpene.
Brief description of the drawings
, below will be to embodiment in order to illustrate more clearly of the utility model embodiment or technical scheme of the prior art
Or the required accompanying drawing used is briefly described in description of the prior art, it should be apparent that, drawings in the following description are only
It is some embodiments of the utility model, for those of ordinary skill in the art, is not paying the premise of creative work
Under, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is a kind of structural representation of firpene isomerization reaction tank.
Embodiment
The utility model discloses a kind of firpene isomerization reaction tank, the firpene isomerization reaction tank can make firpene and catalyst
Fully flowing contact, improves reaction efficiency.
Below in conjunction with the accompanying drawing in the utility model, the technical scheme in the utility model is carried out clearly and completely
Description, it is clear that described only the utility model part of the embodiment, rather than whole embodiments.Based on this practicality
Embodiment in new, those of ordinary skill in the art are obtained every other on the premise of creative work is not made
Embodiment, belong to the scope of the utility model protection.
Shown in Figure 1, the utility model discloses a kind of firpene isomerization reaction tank, including tank body 1, the tank body 1 pushes up
Portion is provided with stirring motor 2 and charging aperture 4, and the tank body 1 is internally provided with agitating shaft 11, and the agitating shaft 11 is by the tank body
The top of tank body 1 is extended to inside 1 and is connected with the stirring motor 2, fixed rack 3, institute are provided with the agitating shaft 1
State fixed rack 3 and be internally provided with accommodating cavity, be provided with the fixed rack and connect the tank interior and the accommodating cavity
Sieve aperture, be filled with catalyst in the accommodating cavity, the bottom of the agitating shaft 11 is provided with auger piece 8, auger
The radius of spin of piece 8 gradually expands from the bottom up along agitating shaft 11, and the tank body 1 is internally provided with heating coil 9, the heating
Coil pipe 9 is set around the auger piece 8, and the tank body 1 is extended to form oil inlet 10 in the both ends of the heating coil 9
Conduction oil is imported with oil-out 5. by oil inlet 10 to heat tank body, conduction oil is flowed out by the oil-out 5.
The bottom of the tank body 1 is provided with discharging opening 7, is discharged after the completion of isomerization reaction by discharging opening 7.
The quantity of the fixed rack 3 is 2, presents down and is arranged on the agitating shaft 11.
Insulation jacket 6 is provided with the outer wall of the tank body 1.
This firpene isomerization reaction tank is heated by being arranged at the heating coil of bottom to firpene, reaches isomery institute
The reaction temperature needed, the fixation rack that will be filled with catalyst are arranged on agitating shaft, and the catalyst is preferably that fixation is urged
Agent, such as acid clay, titanium oxide hydrate, the rotation of the agitating shaft is driven by stirring motor, and agitating shaft drives again
The rotation of the fixed rack, so that keeping sufficient relative flow to contact between catalyst and firpene, so as to effectively
Catalytic action of the catalyst to firpene isomerization reaction is improved, while the auger piece for being arranged at shaft bottom can be the bottom of by
The firpene in portion is lifted upward, further improves the mobility of firpene.
Above content is to combine specific preferred embodiment further detailed description of the utility model, it is impossible to
Assert that specific implementation of the present utility model is confined to these explanations.For the ordinary skill of the utility model art
For personnel, without departing from the concept of the premise utility, some simple deduction or replace can also be made, should all be regarded
To belong to the scope of protection of the utility model.
Claims (4)
1. a kind of firpene isomerization reaction tank, it is characterised in that including tank body, stirring motor and charging are provided with the top of the tank body
Mouthful, the tank interior is provided with agitating shaft, the agitating shaft extended to by the tank interior at the top of the tank body and with institute
Stirring motor connection is stated, is provided with fixed rack on the agitating shaft, the fixed rack is internally provided with accommodating cavity, described solid
Determine to be provided with the sieve aperture for connecting the tank interior and the accommodating cavity on rack, catalyst, institute are filled with the accommodating cavity
The bottom for stating agitating shaft is provided with auger piece, and the radius of spin of auger piece gradually expands from the bottom up along agitating shaft,
The tank interior is provided with heating coil, and the heating coil is set around the auger piece, the heating coil
Extend the tank body to form oil inlet and oil-out in both ends.
2. a kind of firpene isomerization reaction tank according to claim 1, it is characterised in that the bottom of the tank body is provided with out
Material mouth.
3. a kind of firpene isomerization reaction tank according to claim 1, it is characterised in that the quantity of the fixed rack is 2
It is individual, present down and be arranged on the agitating shaft.
4. a kind of firpene isomerization reaction tank according to claim 1, it is characterised in that be provided with the outer wall of the tank body
Insulation jacket.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201720620078.2U CN206996525U (en) | 2017-05-31 | 2017-05-31 | A kind of firpene isomerization reaction tank |
Applications Claiming Priority (1)
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CN201720620078.2U CN206996525U (en) | 2017-05-31 | 2017-05-31 | A kind of firpene isomerization reaction tank |
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CN206996525U true CN206996525U (en) | 2018-02-13 |
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CN201720620078.2U Active CN206996525U (en) | 2017-05-31 | 2017-05-31 | A kind of firpene isomerization reaction tank |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113856606A (en) * | 2021-11-15 | 2021-12-31 | 盐城工学院 | Solution deoxygenation device for potential step method and deoxygenation method thereof |
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2017
- 2017-05-31 CN CN201720620078.2U patent/CN206996525U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113856606A (en) * | 2021-11-15 | 2021-12-31 | 盐城工学院 | Solution deoxygenation device for potential step method and deoxygenation method thereof |
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