CN206995934U - One kind precipitation separating box - Google Patents
One kind precipitation separating box Download PDFInfo
- Publication number
- CN206995934U CN206995934U CN201720881787.6U CN201720881787U CN206995934U CN 206995934 U CN206995934 U CN 206995934U CN 201720881787 U CN201720881787 U CN 201720881787U CN 206995934 U CN206995934 U CN 206995934U
- Authority
- CN
- China
- Prior art keywords
- mozzle
- spacer
- base spacer
- level
- overfall
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
One kind precipitation separating box, including casing, mother liquor pipe, even overfall, base spacer, mozzle, storage tank.The even base spacer has polylith that casing is divided into some grades of units, and connects base spacer step by step and reduce successively, and mother liquor pipe and overfall are located at the first order and afterbody respectively.Setting top spacer and company's base spacer are parallel and interlaced from the second level and later each unit, and overfall is slightly below last cascade base spacer.Mozzle is opened up in the rear end bottom of every grade of unit, sets regulating valve, each mozzle to be connected after coming together in water conservancy diversion house steward with less than its storage tank on mozzle.Methanol solution all is exported from bottom per one-level, and the storage tank less than its position is flowed into after collecting, is to be collected without pressure.Regulating valve is provided with mozzles at different levels can realize the cooperation control of unit not at the same level, the solution on the dynamic only top of liquid crossflow, and the meeting fast hierarchical under the elicitation effect of top spacer.Real three-level separation is realized, three-level is collected.Separative efficiency greatly improves.Equipment volume can be saved, shortens the process time.
Description
Technical field
The utility model belongs to chemical technology field, is related to a kind of fluid separation device, and in particular to a kind of precipitating type point
Liquid case.
Background technology
, can be according to lower leaf in proportion size due to immiscible and lamination between the liquid of opposed polarity be present.Change
Often opposed polarity mixing liquid is separated using this characteristic in work technique.For example in the technique of extraction life cottonseed protein
In, organic solvent and methanol solution can be used, is respectively used to grease extraction and removing techniques.Again by mixed liquor in follow-up technique
Separated, the method for separation is typically to utilize the precipitation method.Methanol solution wherein soluble in water can be in lower floor, and organic molten
Liquid and grease can then be in upper strata.The techniques such as evaporative condenser are recycled to be separated organic solution and grease afterwards.Technique end
End obtains methanol solution and organic solvent, repeats extraction and dephenolizing process of the circulation for preamble.
For example extraction production cottonseed protein follows disclosed in the Chinese patent specification of Application No. 201420359987.1
Ring dephenolize device, disclose a kind of precipitation separating box.It is that casing is divided into three-level using dividing plate, and upper solution climbs over dividing plate and entered
Enter the upper strata of next stage, the lower floor that lower floor's solution passes through conduit progress next stage.In underlying collection methanol solution, in afterbody
Upper strata overfall collect organic solution and grease mixed liquor.Channelling is serious between the settling tank is at different levels, it is impossible to fast and stable, shadow
The efficiency and effect of separation are rung.
Utility model content
The purpose of this utility model is to provide a kind of device for unstable phase fast hierarchical, is exactly a kind of use
In methanol solution and the liquid distributing device of organic solution precipitated and separated.
Precipitation separating box of the present utility model, including casing, mother liquor pipe, even overfall, base spacer, mozzle, storage tank.Institute
The company's of stating base spacer has polylith that casing is divided into some grades of units, and connects base spacer step by step and reduce successively, mother liquor pipe and overfall point
Wei Yu not the first order and afterbody.Set top spacer and even base spacer parallel simultaneously from the second level and later each unit
Interlaced, overfall is slightly below last cascade base spacer.Mozzle is opened up in the rear end bottom of every grade of unit, on mozzle
Regulating valve is set, and each mozzle is connected after coming together in water conservancy diversion house steward with less than its storage tank.Preferred, the described company bottom of the program
Dividing plate and top spacer have 2 pieces respectively, and casing is divided into three-level.Described mother liquor pipe stretches into bottom half, and in its port
Place sets erosion control cap.
After design as above, methanol solution all is exported from bottom per one-level, and is flowed into after collecting and is less than its position
Storage tank, be without pressure collect.Regulating valve is provided with mozzles at different levels can realize the cooperation control of unit not at the same level, liquid transverse direction
The solution on the only top of flowing, and can fast hierarchical under the elicitation effect of top spacer.Realize real three fraction
From three-level is collected.Separative efficiency greatly improves.Equipment volume can be saved, shortens the process time.
Brief description of the drawings
Fig. 1 is the structural representation of the utility model precipitation separating box.
Embodiment
Such as Fig. 1, one kind precipitation separating box, including casing 1, mother liquor pipe 2, even overfall 4, base spacer 7, mozzle 6, storage tank
5.The even base spacer 7 has 2 pieces casing 1 is divided into three-level unit, and connect base spacer 7 step by step reduces successively.Mother liquor pipe 2 and overfall
4 are located at the first order and afterbody respectively.Set top spacer 8 parallel with even base spacer 7 in the second level and third level unit
It is and interlaced.Overfall 4 is slightly below last block and connects base spacer 7.Mozzle 6, water conservancy diversion are set in the rear end bottom of every grade of unit
Regulating valve 9 is set on pipe 6, and each mozzle 6 is connected after coming together in water conservancy diversion house steward 10 with less than its storage tank 5.Described mother liquor pipe 2
The bottom of casing 1 is stretched into, and erosion control cap 3 is set at its port.
Methanol solution comes together in storage tank 5 after mozzle collection, and organic mixed solution（Organic solvent and grease）From overflow
Head piece 4 enters evaporation rectification working process after collecting, continue isolated grease and organic solvent.
The precipitation separating box can apply in addition to the present embodiment, the similar mixing liquid separation that can precipitate separation
In process.
Claims (3)
1. one kind precipitation separating box, including casing（1）, mother liquor pipe（2）, overfall（4）, even base spacer（7）, mozzle（6）, storage
Tank（5）, it is characterised in that the even base spacer（7）There is polylith by casing（1）It is divided into some grades of units, and connects base spacer step by step
（7）Reduce successively, mother liquor pipe（2）And overfall（4）It is located at the first order and afterbody respectively, from the second level and later each
Top spacer is set in unit（8）With even base spacer（7）It is parallel and interlaced, overfall（4）Slightly below last cascade bottom
Dividing plate（7）；Mozzle is opened up in the rear end bottom of every grade of unit（6）, mozzle（6）Upper setting regulating valve（9）, each mozzle
（6）Come together in water conservancy diversion house steward（10）Afterwards with the storage tank less than it（5）Connection.
2. precipitation separating box as claimed in claim 1, it is characterised in that described company's base spacer（7）And top spacer（8）Point
There are not 2 pieces, by casing（1）It is divided into three-level.
3. precipitation separating box as claimed in claim 1 or 2, it is characterised in that described mother liquor pipe（2）Stretch into casing（1）Bottom
Portion, and erosion control cap is set at its port（3）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720881787.6U CN206995934U (en) | 2017-07-19 | 2017-07-19 | One kind precipitation separating box |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720881787.6U CN206995934U (en) | 2017-07-19 | 2017-07-19 | One kind precipitation separating box |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206995934U true CN206995934U (en) | 2018-02-13 |
Family
ID=61455313
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720881787.6U Expired - Fee Related CN206995934U (en) | 2017-07-19 | 2017-07-19 | One kind precipitation separating box |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206995934U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111807592A (en) * | 2020-07-17 | 2020-10-23 | 河北兰升生物科技有限公司 | Continuous liquid separation device and organic solvent separation method using same |
| CN112955427A (en) * | 2019-04-04 | 2021-06-11 | 株式会社Lg化学 | System for continuous purification of esterification reaction products |
| CN113853245A (en) * | 2019-09-19 | 2021-12-28 | 株式会社Lg化学 | Neutralization/water separation tank for esterification product and neutralization/water separation method for esterification product |
| CN112955427B (en) * | 2019-04-04 | 2024-04-19 | 株式会社Lg化学 | System for continuous purification of esterification reaction products |
-
2017
- 2017-07-19 CN CN201720881787.6U patent/CN206995934U/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112955427A (en) * | 2019-04-04 | 2021-06-11 | 株式会社Lg化学 | System for continuous purification of esterification reaction products |
| CN112955427B (en) * | 2019-04-04 | 2024-04-19 | 株式会社Lg化学 | System for continuous purification of esterification reaction products |
| CN113853245A (en) * | 2019-09-19 | 2021-12-28 | 株式会社Lg化学 | Neutralization/water separation tank for esterification product and neutralization/water separation method for esterification product |
| EP3943480A1 (en) * | 2019-09-19 | 2022-01-26 | Lg Chem, Ltd. | Neutralization/water separation tank for esterification product and method for neutralization/water separation of esterification product |
| EP3943480A4 (en) * | 2019-09-19 | 2022-04-20 | Lg Chem, Ltd. | Neutralization/water separation tank for esterification product and method for neutralization/water separation of esterification product |
| CN111807592A (en) * | 2020-07-17 | 2020-10-23 | 河北兰升生物科技有限公司 | Continuous liquid separation device and organic solvent separation method using same |
| CN111807592B (en) * | 2020-07-17 | 2022-04-15 | 河北兰升生物科技有限公司 | Continuous liquid separation device and organic solvent separation method using same |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180213 Termination date: 20190719 |