CN206905412U - Microwave vacuum freeze-drying device - Google Patents

Microwave vacuum freeze-drying device Download PDF

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Publication number
CN206905412U
CN206905412U CN201720268986.XU CN201720268986U CN206905412U CN 206905412 U CN206905412 U CN 206905412U CN 201720268986 U CN201720268986 U CN 201720268986U CN 206905412 U CN206905412 U CN 206905412U
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CN
China
Prior art keywords
microwave
storehouse
dry storehouse
drying device
rotating disk
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Expired - Fee Related
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CN201720268986.XU
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Chinese (zh)
Inventor
向军辉
李飞
乐弦
赛华征
关运龙
付蕊
章婷
杨虎
贾欢欢
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YOUPENG (JIAXING) NEW MATERIALS TECHNOLOGY Co.,Ltd.
Original Assignee
Peng Shu (beijing) New Mstar Technology Ltd
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Priority to CN201720268986.XU priority Critical patent/CN206905412U/en
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Abstract

The utility model provides a kind of microwave vacuum freeze-drying device,The microwave vacuum freeze-drying device includes microwave storehouse,Dry storehouse,The microwave generator of transmission power continuously adjustabe,Refrigeration system,Vacuum water-trapping system,Pressure regulating system,Vavuum pump and micro computer central control system,The dry storehouse is arranged on the inside in the microwave storehouse,The microwave generator of the transmission power continuously adjustabe is fixed on the side wall in the microwave storehouse,Arranged around the dry storehouse uniform crossover,The refrigeration system is connected with the dry storehouse and the vacuum water-trapping system,The vacuum water-trapping system is connected with the vavuum pump and the dry storehouse,The pressure regulating system is connected with the vavuum pump and the dry storehouse,Pump is connected with the dry storehouse,Pump is connected with the dry storehouse,The micro computer central control system is connected with the microwave generator and the pressure regulating system respectively,To control microwave power and pressure.

Description

Microwave vacuum freeze-drying device
Technical field
A kind of freeze drying equipment is the utility model is related to, the vacuum freeze drying more particularly to using microwave as heating source is set It is standby
Background technology
Vacuum Freezing & Drying Technology is thorough due to being dehydrated, can retained product to greatest extent pattern and microstructure, and Rehydration is fast, is increasingly valued by people.It is that water-containing materials are frozen into below eutectic temperature, makes the moisture in material Directly distilled without thawing as a kind of dry technology of gas discharge in the case of condition of high vacuum degree with other solvents.Tradition The mode of vacuum freeze drying generally use heat transfer the heat of sublimation is provided, length arid cycle of this mode of heating, energy disappears Consumption is big, and cost is costly.Meanwhile this mode of heating is carried out at a higher temperature, when food is dried Also the nutritional ingredient of food can be destroyed, is also easy to breed bacteria, the health of people is threatened.These shortcomings seriously govern The development of Vacuum Freezing & Drying Technology.
Microwave vacuum freeze dry technology can overcome disadvantages mentioned above.It is to be substituted with microwave heating in traditional freeze drying technology Supplier as latent heat of sublimation of conduction or infrared radiation heating.Under microwave action, the dipole inside heated material Molecule high-frequency reciprocating moves, and produces " interior frictional heat " and makes to be heated temperature of charge rise, without any heat transfer process, with regard to energy Make material inside and outside while heat while heat up, will not cause to heat non-uniform phenomenon.
However, a greatest problem in microwave vacuum freeze technical field of drying puzzlement researcher is existed using microwave Heated under lower pressure and glow discharge easily occurs.In microwave drying process, due to the raising of vacuum, gas is reduced Disruptive field intensity, gas molecule is set to be easy to be ionized into ion, so as to which glow discharge phenomenon occur.This can lose microwave energy significantly Amount, it is possible to cause to damage to equipment, drying sample can be also caused compared with havoc.In addition, dried in microwave vacuum freeze In the later stage, with the reduction of sample moisture content, the energy required for distilling can also gradually decrease.If constantly with high-power micro- Ripple heats to material, not only results in the quality that material is charred and influences freeze-drying prods, it is also possible to reduces the life-span of equipment.
Application No. 03249124.7, the China of entitled " the microwave freeze-drying equipment for being used for food production " are practical new Type patent, food is thermally dried using microwave magnetron, food can be made inside and outside while heated, and make product centre and outer The moisture of table is evaporated simultaneously, will not destroy by the nutritional ingredient of dried foods, the arid cycle of food is shortened into 5-6 times, Reduce the cost of large-scale production.But the patent does not solve the problems, such as glow discharge of the microwave under lower pressure.Moreover, The position geo-stationary of material and pallet, there is certain influence to the uniformity of product heating effect.
Application No. 200910181720.1, entitled " a kind of double-chamber differential pressure type microwave vacuum freeze drying equipment " Chinese invention patent application, discloses a kind of microwave vacuum freeze-drying device, and the warehouse of the equipment is split by transmission cutoff board Into the first bin and the second bin, magnetron is located at the first bin, and the vacuum of the first bin is less than electric discharge critical value, and material is held Carry setting in the second bin, the second bin is connected by shielding flowing plate with cold-trap.It is but this by magnetron and material Place space is separated, and glow discharge can not fundamentally be suppressed by allowing microwave to enter the method for material place warehouse by electromagnetic wave transparent material The generation of phenomenon, because its second bin is still in the environment of condition of high vacuum degree, microwave still meeting under such vacuum Discharge.In addition, even if microwave enters the first bin from routed entrance, it is reflected in the second bin through bulkhead and forms multi-mode microwave , but because sample position to be freezed is fixed, the uniformity of microwave heating is greatly affected.
On the other hand, for aerogel material, in the drying means mainly used at present, supercritical drying can disappear well Except the capillary tension in drying process, so as to maintain the integrality of material, but this method is high to equipment requirement, costly, And larger danger in operating process be present;Conventional vacuum is freeze-dried reduces the cost of equipment to a certain extent, but by In being dried by the way of conduction heating, uneven heating is even to cause aerogel material integrality to be destroyed;Although constant pressure and dry Dry cost is greatly reduced, but sufficient surface modification need to be carried out to material before it is dried, arid cycle is elongated, reduces Dry efficiency.Therefore, being urgently desirable to develop one kind can dry aerogel material thermally equivalent, and rate of drying is fast, And rate of drying is substantially increased, the low drying means of energy consumption.
Utility model content
The utility model proposes that the purpose of this utility model is to provide a kind of solution well regarding to the issue above The microwave vacuum freeze-drying device of glow discharge phenomenon.
To achieve these goals, according to one side of the present utility model, there is provided a kind of microwave vacuum freeze is dried Equipment, including microwave storehouse, dry storehouse, the microwave generator of transmission power continuously adjustabe, refrigeration system, vacuum water-trapping system, pressure Draught control system, vavuum pump and micro computer central control system, it is characterised in that the dry storehouse is arranged on the interior of the microwave storehouse Portion, the microwave generator of the transmission power continuously adjustabe are fixed on the side wall in the microwave storehouse, uniform around the dry storehouse Cross arrangement, the refrigeration system are connected with the dry storehouse and the vacuum water-trapping system, the vacuum water-trapping system and institute State vavuum pump with the dry storehouse to be connected, the pressure regulating system is connected with the vavuum pump and the dry storehouse, described micro- Computer central control system is connected with the microwave generator and the pressure regulating system respectively, to control the microwave generator institute The microwave power of generation and the pressure regulating system adjust obtained pressure.
According to some embodiments of the utility model, the microwave computer central control system jointly controls pattern pair with predetermined The microwave generator, the pressure regulating system are controlled so that the microwave power that is occurred of the microwave generator with The pressure that the pressure regulating system adjusts to obtain is corresponding.
According to some embodiments of the utility model, the bottom of the dry storehouse is provided with rotating horizontally for motor drive Rotating disk, be symmetrically provided with multiple miniature conveyer belts that can be moved back and forth on rotating disk.
According to some embodiments of the utility model, the micro computer central control system respectively with the rotating disk and described micro- Type conveyer belt is connected to control the transmission frequency of the slewing rate of the rotating disk and the miniature conveyer belt respectively.
According to some embodiments of the utility model, the micro computer central control system is according to jointly controlling after pattern adjusts The microwave power and the pressure adjust the rotating speed of the rotating disk.
According to some embodiments of the utility model, the rotating disk can horizontally rotate, and be worn between the rotating disk and motor The part for crossing microwave storehouse uses the metallic shield with given size sieve aperture to cross flowing plate connection, and in the position through dry storehouse It is provided with sealing gasket.
According to some embodiments of the utility model, by metal, electromagnetic wave transparent material is not made in the microwave storehouse, the dry storehouse It is made up of nonmetallic electromagnetic wave transparent material and size and the microwave storehouse is into predetermined ratio.
According to some embodiments of the utility model, the refrigeration system and the dry storehouse and the vacuum water-trapping system It is connected by pipeline, valve is provided with the pipeline, by refrigeration system described in Valve controlling and the dry storehouse and described Opening and closing between vacuum water-trapping system, the pipeline between the refrigeration system and the microwave storehouse is by with given size sieve aperture Flowing plate connection is crossed in metallic shield.
According to some embodiments of the utility model, the vacuum water-trapping system and vavuum pump, pressure regulating system and jelly Dry storehouse is connected by pipeline, and the pipeline between the vacuum water-trapping system and the microwave storehouse is by the gold with given size sieve aperture Category shielded flowing plate connection, and crossing flowing plate by the metallic shield with given size sieve aperture between the pipeline and dry storehouse connects Connect, the vacuum water-trapping system bottom is provided with defrost valve.
According to some embodiments of the utility model, the microwave generator of the transmission power continuously adjustabe is realizing transmitting While power continuously adjustabe, make the frequency constant of transmitting microwave.
One of according to microwave vacuum freeze-drying device of the present utility model, at least have the following technical effect that:
1st, effectively food can be dried, and homogeneous heating, speed are fast.
The 2nd, the effect that rotatable rotating disk produces microwave stirring is installed on dry storehouse, make microwave energy field more uniform, The generation of glow discharge under low pressure is avoided well.
3rd, central control system to Microwave emission power, refrigeration machine and the control of dry storehouse bottom rotating disk be uniformly controlled maximum The effect that ensure that material of limit.
4th, the aerogel material of extensive application prospect can also be dried for the utility model, and overcome biography Unite freeze drying process the shortcomings that time-consuming, high energy consumption, can adapt to the large-scale industrial production of aerogel material.
The utility model is described in further detail with reference to the accompanying drawings and detailed description, but not with any side Formula limits the utility model.
Brief description of the drawings
Fig. 1 is the structural representation according to the microwave vacuum freeze-drying device of the embodiment of the utility model one;
Fig. 2 is the top view of the rotating disk of microwave vacuum freeze-drying device shown in Fig. 1.
In figure:1st, the microwave generator of transmission power continuously adjustabe, 2, microwave storehouse, 3, dry storehouse, 4, vacuum water-trapping system, 5th, pressure regulating system, 6, vavuum pump, 7, refrigeration system, 8-1, valve 1,8-2, valve 2,9, sealing gasket, 10, motor, 11, band Flowing plate is crossed in the metallic shield for having regulation sieve aperture, and 12, rotating disk, 13-1, lyophilized door, 13-2, microwave door, 14, defrost valve, 15, Micro computer central control system, 16, miniature conveyer belt
Embodiment
According to embodiment of the present utility model, there is provided a kind of microwave vacuum freeze-drying device (hereinafter referred to as this practicality New equipment), including microwave storehouse, dry storehouse, the microwave generator of transmission power continuously adjustabe, refrigeration system, vacuum catch water System, pressure regulating system, vavuum pump and micro computer central control system.
Wherein the microwave generator of transmission power continuously adjustabe, pressure regulating system can be unified by micro computer central control system Control, by operator according to setting program is actually needed, so as to which the micro computer central control system being capable of automatic control and adjustment items Parameter, complete the drying of the material.
By metal, electromagnetic wave transparent material such as stainless steel is not made in microwave storehouse, and its shape can be cube.Dry storehouse is arranged on The inside in microwave storehouse, and positioned at the center of bottom, size and microwave storehouse are proportional, and generally, the ratio is 35%- 85%, preferably 40%-80%, more preferably 40%-75%, most preferably 45%-65%.
Dry storehouse is made up of nonmetallic electromagnetic wave transparent material such as polytetrafluoroethylene (PTFE), glass or ceramics, is selected in the present embodiment Polytetrafluoroethylmaterial material, the entrance of microwave was both can guarantee that, and reduced lossy microwave, there is certain intensity again, in condition of high vacuum degree Under the conditions of will not produce microwave from leakage.
The microwave generator of transmission power continuously adjustabe is fixed on the side wall in microwave storehouse, around dry storehouse uniform crossover row Row, it is connected and is controlled by it with micro computer central control system.Preferably, the microwave generator of the transmission power continuously adjustabe is being protected In the case that card transmitting microwave frequency is constant, the transmission power of continuously adjustable microwave.
Dry storehouse bottom is provided with the rotating disk that can be rotated horizontally of motor drive, and 8 are symmetrically provided with rotating disk can be The radially reciprocating miniature conveyer belt of rotating disk.The miniature conveyer belt on rotating disk and the rotating disk that can be horizontally rotated is not by The polytetrafluoroethylmaterial material for absorbing microwave is made.Part between rotating disk and motor through microwave storehouse is used with certain size sieve The metal shielding board connection in hole, while the position through dry storehouse is provided with sealing gasket.The small conveyer belt can guarantee that material It while being rotated with rotating disk, can also be moved on the direction of vertical plane, make material heated evenly.
Refrigeration system is connected with dry storehouse and vacuum water-trapping system by pipeline, can be controlled between them by valve Opening and closing.Pipeline between refrigeration system and microwave storehouse crosses flowing plate connection by the metallic shield with certain size sieve aperture.The pipe Road can use tetrafluoro glass fiber material.Tetrafluoro glass fiber material is the low damage material of microwave, and this material, which can guarantee that, to be stretched into microwave storehouse Part do not absorb microwave energy.
Vacuum water-trapping system can absorb to the sublimation gases in drying process, with vavuum pump, pressure regulating system and Dry storehouse is connected by pipeline, and the pipeline between vacuum water-trapping system and microwave storehouse is by the metallic shield with certain size sieve aperture Cross flowing plate connection.The pipeline uses tetrafluoro glass fiber material, passes through the metal screen with certain size sieve aperture between dry storehouse Flowing plate connection was covered, ensures that microwave does not enter pipeline.In addition, defrost valve is installed in the bottom of vacuum water-trapping system.
The said equipment can be used for material is dried.The base that method of the present utility model is freeze-dried in traditional vacuum On plinth, the drying that latent heat of sublimation carries out material is provided by microwave heating.
In practical operation, material is placed in dry storehouse.The microwave of microwave generator transmitting can pass through dry storehouse Wall is added on material, and the reflection that will also pass through microwave storehouse inwall for not entering into dry storehouse is eventually entered in dry storehouse by thing Material absorbs.Micro computer central control system controls to adjust the change of the changing pattern, pressure of microwave power by advance program setting Pattern and amplitude of variation, the relative change matching model of pressure and microwave power, the rotating speed of rotating disk, the motion frequency of miniature conveyer belt The parameters such as rate, so as to realize that treating lyophilized sample by applying microwave under vacuum is dried.
The method that material is dried to equipment of the present utility model and using the equipment referring now to Fig. 1 is illustrated such as Under.
Fig. 1 is a kind of structural representation of embodiment of the utility model device.It is continuous that the equipment includes transmission power Adjustable microwave generator 1, microwave storehouse 2, dry storehouse 3, vacuum water-trapping system 4, pressure regulating system 5, vavuum pump 6, refrigeration system System 7, motor 10, micro computer central control system 15, miniature conveyer belt 16 and some additional devices.
Supplier of the microwave generator 1 of the transmission power continuously adjustabe as the utility model microwave heat source, Frequency is fixed as 2450MHz, the inwall installed in microwave storehouse 2, is arranged around the uniform crossover of dry storehouse 3, thus micro- Under the conciliation of computer central control system, the microwave of release can be made more uniformly to be added on dry storehouse 3.
Microwave storehouse 2 is cubic type, and by metal, electromagnetic wave transparent material such as stainless steel is not made, in one kind in whole microwave storehouse Atmospheric pressure environment.
The dry storehouse 3 is arranged on the center position of the bottom of microwave storehouse 2, and size and microwave storehouse 2 are in certain proportion, such as should Ratio is 45%-65%.
Vacuum water-trapping system 4 passes sequentially through tetrafluoro glass fiber pipe and is connected with pressure regulating system 5, vavuum pump 6, and right side passes through Pipeline passes through microwave storehouse 2, is finally connected with dry storehouse 3, and flowing plate 11 is crossed in the part of contact with the metallic shield with certain sieve aperture It is connected, ensures that the microwave in microwave storehouse 2 is not revealed, the microwave in dry storehouse 3 does not enter among pipeline.
Pressure regulating system 5 passes through micro computer central control system in the OK range 0-100pa that pressure meets lyophilized demand Operating pressure, and then field strength threshold value corresponding to raising electric discharge can be properly increased, glow discharge phenomenon is not occurred.
The side of the refrigeration system 7 passes through microwave storehouse 2 by pipeline, is connected with the dry storehouse 3, through microwave storehouse 2 Part flowing plate connection is crossed by the metallic shield with given size sieve aperture, ensure that the microwave in microwave storehouse 2 will not be revealed.Valve 8-1 can be opened and closed, and Open valve 8-1 when pre-freeze is carried out to material, material is condensed rapidly, treat that material freezes Knot, closes valve 8-1, and vavuum pump 6 is started working.The opposite side of refrigeration system 7 connects vacuum water-trapping system 4 by pipeline, together Sample, valve 8-2 can also be opened and closed.
The part that the motor 10 is stretched into microwave storehouse 2 and dry storehouse 3 is made up of tetrafluoro glass fiber material, through microwave storehouse 2 Part flowing plate 11 crossed by the metallic shield with certain sieve aperture connected, ensure that the microwave in microwave storehouse 2 is not revealed.Through lyophilized The part in storehouse 3 is added with sealing gasket 9, the sealing and vacuum of guarantee dry storehouse 3.
Flowing plate 11 is crossed in the metallic shield with given size sieve aperture, is made up of metal copper plate, and sieve aperture above passes through Precision measuring and calculating, can accomplish to prevent microwave leakage.
Rotating disk 12 is made up of polytetrafluoroethylmaterial material, in collar plate shape.On rotating disk 12 around center be distributed with piling 8 it is micro- Type conveyer belt 16, it is miniature to send band 16 to be made up of polytetrafluoroethylmaterial material, control rotating disk to rotate by the micro computer central control system 15 Speed and miniature conveyer belt motion frequency, ensure material with rotating disk 12 rotate while, also can be in vertical plane Direction on move, be allowed to be uniformly heated.Microwave energy concentration is avoided to a certain extent, reduces generation glow discharge Odds.
Enter line program setting to micro computer central control system 15, it is automatically adjusted microwave work(in the freeze-drying process of material The changing pattern of rate, the changing pattern of pressure and amplitude of variation, the relative change matching model of pressure and microwave power, rotating disk The parameter such as motion frequency of rotating speed, miniature conveyer belt, so as to complete the drying of material.
Embodiment 1
In the present embodiment, banana pieces are freezed using the equipment shown in Fig. 1, carrying out practically process is as follows:
Microwave door 13-2 and lyophilized door 13-1 is opened, treats that lyophilized banana pieces are respectively placed on rotating disk 12 by some On miniature conveyer belt 16.Lyophilized door 13-1 and microwave door 13-2 is closed successively.The banana pieces are first cut into 1cm × 1cm in advance × 1cm cube fritter, mutual spacing about 0.5cm, is evenly spaced on Minitype transmission band 16.
Refrigeration system 7 and valve 8-1 and 8-2 are opened, freezes the banana pieces on rotating disk 12, and make vacuum water-trapping system temperature It is rapidly reduced to -20 DEG C.
Enter line program setting to micro computer central control system, it is automatically adjusted microwave work(in the freeze-drying process of banana pieces The changing pattern of rate, the changing pattern of pressure and amplitude of variation, the relative change matching model of pressure and microwave power, rotating disk The parameter such as motion frequency of rotating speed, miniature conveyer belt.
Treat that banana pieces are freezed, while closing valve 8-1, open vavuum pump 6, now the vacuum in dry storehouse 3 is rapid Improve.
When pressure regulating system 5 shows that pressure is reduced to the pressure limit such as 5-30Pa pre-set, in micro computer Control system meeting starter motor 10 and miniature conveyer belt 16, make banana pieces by given pace setting in motion.
Micro computer central control system opens the microwave generator 1 of transmission power continuously adjustabe, and microwave starts to burst into dry storehouse 3 It is interior, the banana pieces freezed are heated.
With the progress of heating, the moisture in banana pieces starts to distil, and steam is finally all inhaled into vacuum water-trapping system 4 Receive, the pressure in dry storehouse 3 is not raised.
Dry carry out during, according to pressure regulating system 5 show pressure change, ensure dry needed for pressure In the range of, micro computer central control system can suitably adjust the pressure in rise dry storehouse.In addition, micro computer central control system is according to micro- The changing pattern of wave power, the changing pattern of pressure and amplitude of variation automatically adjust the motion of the rotating speed and miniature conveyer belt of rotating disk Frequency.
As the transmission power of power continuously adjustabe microwave generator 1 gradually reduces, banana pieces drying is also close to completion.When When the pressure that pressure regulating system 5 is shown no longer changes, illustrate that banana pieces are completely dried.
When 5 registration no longer changes within the regular hour, micro computer central control system closes transmission power successively Microwave generator 1, motor 10 and the and of miniature conveyer belt 16 of continuously adjustabe, manual-lock vavuum pump 6, refrigeration system 7 and valve 8-2, the defrost valve 14 of vacuum water-trapping system 16 is opened, allows air to enter dry storehouse 3.
Treat that pressure regulating system 5 is shown as normal pressure, open microwave door 13-2 and lyophilized door 13-1 successively, take out lyophilized Banana pieces, freeze terminate.After measured, the moisture of Bananas block is down to less than 4%.
Embodiment 2
The present embodiment, specific design mode is with embodiment 1, for freezing to cellulose SiO2 aerogel composites It is dry.Carrying out practically process is as follows:
Microwave door 13-2 and lyophilized door 13-1 is opened, treats that the compound wet gels of lyophilized cellulose SiO2 are distinguished by some It is placed on the miniature conveyer belt 16 on rotating disk 12.Lyophilized door 13-1 and microwave door 13-2 is closed successively.The wet gel is Cube block or sheet material, mutual spacing about 2cm, are evenly spaced on Minitype transmission band 16.
Refrigeration system 7 and valve 8-1 and 8-2 are opened, freezes the wet gel on rotating disk 12, and make vacuum water-trapping system temperature It is rapidly reduced to -45 DEG C.
Enter line program setting to micro computer central control system, it is automatically adjusted microwave work(in the freeze-drying process of wet gel The changing pattern of rate, the changing pattern of pressure and amplitude of variation, the relative change matching model of pressure and microwave power, rotating disk The parameter such as motion frequency of rotating speed, miniature conveyer belt.
Treat that hydrogel freezes, while closing valve 8-1, open vavuum pump 6, now the vacuum in dry storehouse 3 is rapid Improve.
When pressure regulating system 5 shows that pressure is reduced to the pressure limit such as 10-30Pa pre-set, in micro computer Control system meeting starter motor 10 and miniature conveyer belt 16, the gel mass for making to freeze is by given pace setting in motion.
Micro computer central control system opens the microwave generator 1 of transmission power continuously adjustabe, and microwave starts to burst into dry storehouse 3 It is interior, the gel mass freezed is heated.
With the progress of heating, moisture and other solvents in the gel mass freezed start to distil, and the gas of distillation enters Enter vacuum water-trapping system 4, the pressure in dry storehouse 3 is not raised.
Dry carry out during, according to pressure regulating system 5 show pressure change, ensure dry needed for pressure In the range of, micro computer central control system can suitably adjust the pressure in rise dry storehouse.Meanwhile micro computer central control system is according to micro- The relative change matching model of the changing pattern of wave power, the changing pattern of pressure and amplitude of variation, pressure and microwave power is certainly The rotating speed of dynamic regulation rotating disk and the motion frequency of miniature conveyer belt.
As the transmission power of power continuously adjustabe microwave generator 1 gradually reduces, gel mass drying is also close to completion. When the pressure that pressure regulating system 5 is shown no longer changes, illustrate that wet gel has been completely dried.
When 5 registration no longer changes within the regular hour, micro computer central control system closes transmission power successively Microwave generator 1, motor 10 and the and of miniature conveyer belt 16 of continuously adjustabe, manual-lock vavuum pump 6, refrigeration system 7 and valve 8-2, the defrost valve 14 of vacuum water-trapping system 16 is opened, allows air to enter dry storehouse 3.
Treat that pressure regulating system 5 is shown as normal pressure, open microwave door 13-2 and lyophilized door 13-1 successively, take out lyophilized Aeroge, freeze terminate.After measured, the moisture of cellulose SiO2 composite aerogels is down to less than 3%.
To sum up, the advantages of the utility model has following aspects:
1st, dry storehouse is placed in microwave storehouse, and positioned at the center of bottom, the microwave that microwave generator is launched is through bursting What entrance entered is an atmospheric pressure environment, then just enters the dry storehouse in vacuum state, will not be put during this Electrical phenomena.
2nd, the microwave generator of transmission power continuously adjustabe is applied, in the case where ensureing that microwave frequency is certain, micro- electricity The program of brain central control system sets the changing pattern that can control microwave power, can change the field strength in dry storehouse, utilize pressure Regulating system, in the case where ensureing that pressure is in normal range (NR), operating pressure is properly increased, it is constantly in generation aura Under the field strength threshold value of electric discharge, the generation of electric discharge phenomena can be avoided.
3rd, the work(of microwave generator is being continuously adjusted using the microwave generator of power continuously adjustabe, micro computer central control system Rate coordinates the miniature conveyer belt on rotating disk and rotating disk to ensure that the uniformity for carrying out microwave heating to material, central control system setting Program can be according to the pressure change pattern and amplitude of variation in dry storehouse, and the relative change mating die of pressure and microwave power Formula, automatically adjust the rotating speed of rotating disk and the frequency of miniature conveyer belt motion.Each block of material is additionally, since all simultaneously two sides Motion upwards, avoids the heating problem of non-uniform that material position is fixed or material and rotating disk geo-stationary are brought.
4th, aerogel material can be dried, and dried thorough, there is provided a kind of drying of new aerogel material Method.
Although describing the utility model with reference to specific embodiment, it will be understood by those skilled in the art that not Deviate under the scope of the utility model, various change, and its alternative key element of equivalent can be carried out.Therefore, the utility model Disclosed specific embodiment is not limited to, but it includes all embodiment party fallen within the scope of the appended claims Formula.

Claims (10)

1. a kind of microwave vacuum freeze-drying device, including microwave storehouse, dry storehouse, the microwave of transmission power continuously adjustabe occur Device, refrigeration system, vacuum water-trapping system, pressure regulating system, vavuum pump and micro computer central control system,
Characterized in that,
The dry storehouse is arranged on the inside in the microwave storehouse,
The microwave generator of the transmission power continuously adjustabe is fixed on the side wall in the microwave storehouse, uniform around the dry storehouse Cross arrangement,
The refrigeration system is connected with the dry storehouse and the vacuum water-trapping system,
The vacuum water-trapping system is connected with the vavuum pump and the dry storehouse,
The pressure regulating system is connected with the vavuum pump and the dry storehouse,
The micro computer central control system is connected with the microwave generator and the pressure regulating system respectively, described micro- to control The microwave power and the pressure regulating system that wave producer is occurred adjust obtained pressure.
2. microwave vacuum freeze-drying device according to claim 1, it is characterised in that the micro computer central control system with The predetermined pattern that jointly controls is controlled to the microwave generator, the pressure regulating system, so that the microwave occurs The microwave power that device is occurred is corresponding with the pressure that the pressure regulating system adjusts to obtain.
3. microwave vacuum freeze-drying device according to claim 1 or 2, it is characterised in that the bottom of the dry storehouse Be provided with the rotating disk that can be rotated horizontally of motor drive, be symmetrically provided with the rotating disk it is multiple can be along the footpath of the rotating disk To reciprocating miniature conveyer belt.
4. microwave vacuum freeze-drying device according to claim 3, it is characterised in that the micro computer central control system point It is not connected with the rotating disk and the miniature conveyer belt to control the slewing rate of the rotating disk and the miniature transmission respectively The transmission frequency of band.
5. microwave vacuum freeze-drying device according to claim 4, it is characterised in that the micro computer central control system root The rotating speed of the rotating disk is adjusted according to the microwave power after pattern is adjusted and the pressure is jointly controlled.
6. microwave vacuum freeze-drying device according to claim 3, it is characterised in that the rotating disk horizontal can turn Dynamic, the part between the rotating disk and motor through microwave storehouse uses the metallic shield with given size sieve aperture to cross flowing plate company Connect, and the position through dry storehouse is provided with sealing gasket.
7. microwave vacuum freeze-drying device according to claim 1, it is characterised in that the microwave storehouse is impermeable by metal Wave material is made, and the dry storehouse is made up of nonmetallic electromagnetic wave transparent material and size and the microwave storehouse are into predetermined ratio.
8. microwave vacuum freeze-drying device according to claim 1, it is characterised in that the refrigeration system with it is described Dry storehouse is connected with the vacuum water-trapping system by pipeline, and valve is provided with the pipeline, passes through system described in Valve controlling Opening and closing between cooling system and the dry storehouse and the vacuum water-trapping system, between the refrigeration system and the microwave storehouse Pipeline crosses flowing plate connection by the metallic shield with given size sieve aperture.
9. microwave vacuum freeze-drying device according to claim 1, it is characterised in that the vacuum water-trapping system with it is true Empty pump, pressure regulating system and dry storehouse are connected by pipeline, the pipeline between the vacuum water-trapping system and the microwave storehouse Flowing plate connection is crossed by the metallic shield with given size sieve aperture, by being sieved with given size between the pipeline and dry storehouse Flowing plate connection is crossed in the metallic shield in hole, and the vacuum water-trapping system bottom is provided with defrost valve.
10. microwave vacuum freeze-drying device according to claim 1, it is characterised in that the transmission power continuously may be used The microwave generator of tune makes the frequency constant of transmitting microwave while transmission power continuously adjustabe is realized.
CN201720268986.XU 2017-03-17 2017-03-17 Microwave vacuum freeze-drying device Expired - Fee Related CN206905412U (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201720268986.XU CN206905412U (en) 2017-03-17 2017-03-17 Microwave vacuum freeze-drying device

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CN206905412U true CN206905412U (en) 2018-01-19

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106839661A (en) * 2017-03-17 2017-06-13 澍澎(北京)新材料科技有限公司 The drying means of microwave vacuum freeze-drying device and material
CN115307387A (en) * 2022-08-12 2022-11-08 深圳市康乐态原科技企业 Microwave vacuum freeze-drying box module, table type microwave vacuum freeze-drying device and freeze-drying process

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106839661A (en) * 2017-03-17 2017-06-13 澍澎(北京)新材料科技有限公司 The drying means of microwave vacuum freeze-drying device and material
CN115307387A (en) * 2022-08-12 2022-11-08 深圳市康乐态原科技企业 Microwave vacuum freeze-drying box module, table type microwave vacuum freeze-drying device and freeze-drying process
CN115307387B (en) * 2022-08-12 2024-05-07 深圳市康乐态原科技企业 Microwave vacuum freeze-drying box module, table type microwave vacuum freeze-drying device and freeze-drying process

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