CN206881693U - A kind of ultrasonic continuous reaction apparatus - Google Patents
A kind of ultrasonic continuous reaction apparatus Download PDFInfo
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- CN206881693U CN206881693U CN201720687687.XU CN201720687687U CN206881693U CN 206881693 U CN206881693 U CN 206881693U CN 201720687687 U CN201720687687 U CN 201720687687U CN 206881693 U CN206881693 U CN 206881693U
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Abstract
The utility model discloses a kind of ultrasonic continuous reaction apparatus, including main treatment tank device and side reaction tank arrangement, the main treatment tank device and side reaction tank arrangement include tank body, the top of tank body is fixed with upper cover plate, the upper portion side wall of the tank body of main treatment tank device has connected feed pipe and bleeder pipe, the bottom of the tank body of main treatment tank device has connected vomit pipe, and bleeder pipe is higher than feed pipe, and the lower sides of the tank body of main treatment tank device have connected conveying connecting tube；The upper portion side wall of side reaction tank arrangement has connected secondary feed pipe, recycle feed pipe and secondary bleeder pipe, and secondary bleeder pipe is higher than secondary feed pipe and recycle feed pipe.It carries out circulation hair using two tank bodies of main treatment tank device and side reaction tank arrangement and answered, its small volume, and space hold is small, it is simple in construction, and ultrasonic reaction is carried out by ultrasonic wave rod so that reaction is abundant, time is short, greatly improves reaction effect and shortens the reaction time.
Description
Technical field：
Technical field of chemical is the utility model is related to, more specifically to a kind of ultrasonic continuous reaction apparatus.
Background technology：
In existing chemical industry continuous reaction apparatus, the modes such as agitator arm are typically provided in its tank body and are stirred realization instead
Should, its mixing effect is limited, and reaction is not enough fully, it is necessary to set at least four to five continuous tank bodies to realize coupled reaction so that
Equipment volume is big, significantly space-consuming, and reaction effect or undesirable.
Utility model content：
The purpose of this utility model is overcome the deficiencies in the prior art, there is provided a kind of ultrasonic continuous reaction apparatus, it is used
Two tank bodies of main treatment tank device and side reaction tank arrangement carry out circulation hair and answered, and its small volume, space hold is small, simple in construction,
And ultrasonic reaction is carried out by ultrasonic wave rod so that reaction is abundant, and the time is short, when greatly improving reaction effect and shortening reaction
Between.
The utility model solve the technical problem scheme be：
A kind of ultrasonic continuous reaction apparatus, including main treatment tank device and side reaction tank arrangement, the main treatment tank device
Include tank body with side reaction tank arrangement, the top of tank body is fixed with upper cover plate, the upper portion side wall of the tank body of main treatment tank device
Feed pipe and bleeder pipe are connected, the bottom of the tank body of main treatment tank device has connected vomit pipe, and bleeder pipe is higher than feed pipe, main
The lower sides for reacting the tank body of tank arrangement have connected conveying connecting tube；The upper portion side wall of side reaction tank arrangement has connected secondary charging
Pipe, recycle feed pipe and secondary bleeder pipe, secondary bleeder pipe are higher than secondary feed pipe and recycle feed pipe, the tank body of side reaction tank arrangement
Bottom has connected secondary vomit pipe；
One end of bleeder pipe and secondary bleeder pipe connects main deflation balance pipe, and the outlet side of main deflation balance pipe has connected deflation
The inlet end of control valve, the outlet side of deflation control valve connect escape pipe；
The conveying connecting tube connects secondary feed pipe by the first delivery pipe.
Main feed pipe has been connected on the feed pipe, the first mother tube, the second mother tube and master have been connected on main feed pipe
Circulation pipe, the other end of main circulation pipe connect the discharge end of main circulation pump, the feed end of main circulation pump by first circulation pipe with
Vomit pipe is connected.
The secondary vomit pipe connects second circulation pipe, and the other end of second circulation pipe connects the feed end of secondary circulating pump, secondary
The discharge end of circulating pump is connected by secondary circulation pipe with recycle feed pipe, and the tank body lower part side wall of side reaction tank arrangement has connected
Finished product efferent duct, finished product efferent duct connect continuous discharge pipe.
The middle part of sliding channel of the tank body of the main treatment tank device and side reaction tank arrangement is provided with liquid level visor.
Inlet valve is equipped with first mother tube and the second mother tube.
The discharge end of the main circulation pump is provided with the first valve body, and the other end of the first valve body connects main circulation pipe, and master follows
The feed end of ring pump is provided with the second valve body, and the second valve body connects the discharge end of first circulation pipe, the other end of first circulation pipe
Vomit pipe is connected, the first vomit pipe has been connected in the middle part of first circulation pipe, the first vomit pipe is provided with the first baiting valve.
The top surface of the upper cover plate is fixed with supersonic generator, and the ultrasonic wave rod of supersonic generator is stretched into tank body.
The first probe tube has been connected in the middle part of first delivery pipe, the first sampling valve is provided with the first probe tube；Finished product
The second probe tube has been connected in the middle part of efferent duct, the second sampling valve is provided with the second probe tube.
The discharge end of the secondary circulating pump is provided with the 3rd valve body, and the other end of the 3rd valve body connects secondary circulation pipe, and pair is followed
The feed end of ring pump is provided with the 4th valve body, and the 4th valve body connects the discharge end of second circulation pipe, the other end of second circulation pipe
Secondary vomit pipe is connected, the second vomit pipe has been connected in the middle part of second circulation pipe, the second vomit pipe is provided with the second baiting valve.
Prominent effect of the present utility model is：
Compared with prior art, it circulate sending out and answered using two tank bodies of main treatment tank device and side reaction tank arrangement,
Its small volume, space hold is small, simple in construction, and carries out ultrasonic reaction by ultrasonic wave rod so that reaction is abundant, the time
It is short, greatly improve reaction effect and shorten the reaction time.
Brief description of the drawings：
Fig. 1 is easy structure schematic diagram of the present utility model；
Embodiment：
Embodiment, see as shown in figure 1, a kind of ultrasonic continuous reaction apparatus, including main treatment tank device 10 and side reaction tank
Device 20, the main treatment tank device 10 and side reaction tank arrangement 20 include tank body 1, and the top of tank body 1 is fixed with upper cover plate
2, the upper portion side wall of the tank body 1 of main treatment tank device 10 has connected feed pipe 11 and bleeder pipe 12, the tank of main treatment tank device 10
The bottom of body 1 has connected vomit pipe 13, and bleeder pipe 12 is higher than feed pipe 11, the lower sides of the tank body 1 of main treatment tank device 10
Conveying connecting tube 14 is connected；The upper portion side wall of side reaction tank arrangement 20 has connected secondary feed pipe 21, recycle feed pipe 22 and pair
Bleeder pipe 23, secondary bleeder pipe 23 are higher than secondary feed pipe 21 and recycle feed pipe 22, and the bottom of the tank body 1 of side reaction tank arrangement 20 leads to
It is connected to secondary vomit pipe 24；
One end of bleeder pipe 12 and secondary bleeder pipe 23 connects main deflation balance pipe 30, and the outlet side of main deflation balance pipe 30 leads to
The inlet end of deflation control valve 31 is connected to, the outlet side of deflation control valve 31 connects escape pipe 32；
The conveying connecting tube 14 connects secondary feed pipe 21 by the first delivery pipe 40.
Further, main feed pipe 50 has been connected on the feed pipe 11, the first raw material has been connected on main feed pipe 50
Pipe 51, the second mother tube 52 and main circulation pipe 53, the other end of main circulation pipe 53 connect the discharge end of main circulation pump 54, major cycle
The feed end of pump 54 is connected by first circulation pipe 55 with vomit pipe 13.
Further, the secondary vomit pipe 24 connects second circulation pipe 60, and the other end of second circulation pipe 60 connects pair
The feed end of circulating pump 61, the discharge end of secondary circulating pump 61 are connected by secondary circulation pipe 62 with recycle feed pipe 22, side reaction
The lower sides of tank body 1 of tank arrangement 20 have connected finished product efferent duct 25, and finished product efferent duct 25 connects continuous discharge pipe 26.
Further, the middle part of sliding channel of the tank body 1 of the main treatment tank device 10 and side reaction tank arrangement 20 is provided with liquid
Position visor 3.
Further, it is equipped with inlet valve 4 on the mother tube 52 of the first mother tube 51 and second.
Further, the discharge end of the main circulation pump 54 is provided with the first valve body 56, the other end of the first valve body 56
Main circulation pipe 53 is connected, the feed end of main circulation pump 54 is provided with the second valve body 57, and the second valve body 57 connects first circulation pipe 55
Discharge end, the other end of first circulation pipe 55 connects vomit pipe 13, and the middle part of first circulation pipe 55 has connected the first vomit pipe
58, the first vomit pipe 58 is provided with the first baiting valve 59.
Further, the top surface of the upper cover plate 2 is fixed with supersonic generator 5, the ultrasonic wave of supersonic generator 5
Rod 6 is stretched into tank body 1, and the devices such as agitator arm can also be set in tank body 1, realizes many-sided vibrations stirring so that reaction is more
Add fully.
Further, the middle part of first delivery pipe 40 has connected the first probe tube 41, is set in the first probe tube 41
There is the first sampling valve 42；The middle part of finished product efferent duct 25 has connected the second probe tube 251, and second is provided with the second probe tube 251
Sampling valve 252.
Further, the discharge end of the secondary circulating pump 61 is provided with the 3rd valve body 63, the other end of the 3rd valve body 63
Secondary circulation pipe 62 is connected, the feed end of secondary circulating pump 61 is provided with the 4th valve body 64, and the 4th valve body 64 connects second circulation pipe 60
Discharge end, the other end of second circulation pipe 60 connects secondary vomit pipe 24, and the middle part of second circulation pipe 60 has connected the second blowing
Pipe 65, the second vomit pipe 65 are provided with the second baiting valve 66.
Operation principle：First mother tube 51 and the second mother tube 52 enter main treatment tank by conveying continuous two kinds of raw materials
In the tank body 1 of device 10, by the way that sampling can check its reaction condition from the first probe tube 41 after reaction, react not abundant enough
When, run by main circulation pump 54, it is possible to achieve circular response again in main treatment tank device 10, after the extent of reaction is up to, enter
Enter in the tank body 1 of side reaction tank arrangement 20 and carry out subsequent reactions, similarly, when reacting insufficient, by secondary circulating pump 61 again
Circular response, finally, exported from continuous discharge pipe 26.
In the present embodiment, it realizes dither by the raw material of ultrasonic wave rod 6, so as to greatly improve its vibrations effect
Fruit.
Finally, embodiment of above is merely to illustrate the utility model, and is not limitation of the utility model, relevant skill
The those of ordinary skill in art field, in the case where not departing from spirit and scope of the present utility model, various changes can also be made
Change and modification, therefore all equivalent technical schemes fall within category of the present utility model, patent protection model of the present utility model
Enclosing to be defined by the claims.
Claims (9)
1. a kind of ultrasonic continuous reaction apparatus, including main treatment tank device (10) and side reaction tank arrangement (20), it is characterised in that：
The main treatment tank device (10) and side reaction tank arrangement (20) include tank body (1), and the top of tank body (1) is fixed with upper cover plate
(2), the upper portion side wall of the tank body (1) of main treatment tank device (10) has connected feed pipe (11) and bleeder pipe (12), main treatment tank
The bottom of the tank body (1) of device (10) has connected vomit pipe (13), and bleeder pipe (12) is higher than feed pipe (11), main treatment tank device
(10) lower sides of tank body (1) have connected conveying connecting tube (14)；The upper portion side wall of side reaction tank arrangement (20) has connected
Secondary feed pipe (21), recycle feed pipe (22) and secondary bleeder pipe (23), secondary bleeder pipe (23) is higher than secondary feed pipe (21) and circulation
Feed pipe (22), the bottom of the tank body (1) of side reaction tank arrangement (20) have connected secondary vomit pipe (24)；
One end of bleeder pipe (12) and secondary bleeder pipe (23) connects main deflation balance pipe (30), the outlet of main deflation balance pipe (30)
End connects the inlet end of deflation control valve (31), and the outlet side of deflation control valve (31) connects escape pipe (32)；
The conveying connecting tube (14) connects secondary feed pipe (21) by the first delivery pipe (40).
A kind of 2. ultrasonic continuous reaction apparatus according to claim 1, it is characterised in that：Connected on the feed pipe (11)
There is main feed pipe (50), the first mother tube (51), the second mother tube (52) and main circulation pipe have been connected on main feed pipe (50)
(53), the other end of main circulation pipe (53) connects the discharge end of main circulation pump (54), and the feed end of main circulation pump (54) passes through
One circulation pipe (55) is connected with vomit pipe (13).
A kind of 3. ultrasonic continuous reaction apparatus according to claim 2, it is characterised in that：The secondary vomit pipe (24) connects
Second circulation pipe (60), the other end of second circulation pipe (60) connect the feed end of secondary circulating pump (61), secondary circulating pump (61)
Discharge end is connected by secondary circulation pipe (62) with recycle feed pipe (22), tank body (1) lower side of side reaction tank arrangement (20)
Wall has connected finished product efferent duct (25), and finished product efferent duct (25) connects continuous discharge pipe (26).
A kind of 4. ultrasonic continuous reaction apparatus according to claim 3, it is characterised in that：The main treatment tank device (10) and
The middle part of sliding channel of the tank body (1) of side reaction tank arrangement (20) is provided with liquid level visor (3).
A kind of 5. ultrasonic continuous reaction apparatus according to claim 3, it is characterised in that：First mother tube (51) and
Inlet valve (4) is equipped with two mother tubes (52).
A kind of 6. ultrasonic continuous reaction apparatus according to claim 3, it is characterised in that：The discharging of the main circulation pump (54)
End is provided with the first valve body (56), and the other end of the first valve body (56) connects main circulation pipe (53), the charging of main circulation pump (54)
End is provided with the second valve body (57), and the second valve body (57) connects the discharge end of first circulation pipe (55), first circulation pipe (55)
The other end connects vomit pipe (13), and the first vomit pipe (58), the first vomit pipe (58) have been connected in the middle part of first circulation pipe (55)
It is provided with the first baiting valve (59).
A kind of 7. ultrasonic continuous reaction apparatus according to claim 1, it is characterised in that：The top surface of the upper cover plate (2) is consolidated
Surely there is supersonic generator (5), the ultrasonic wave rod (6) of supersonic generator (5) is stretched into tank body (1).
A kind of 8. ultrasonic continuous reaction apparatus according to claim 3, it is characterised in that：In first delivery pipe (40)
Portion has connected the first probe tube (41), and the first sampling valve (42) is provided with the first probe tube (41)；In finished product efferent duct (25)
Portion has connected the second probe tube (251), and the second sampling valve (252) is provided with the second probe tube (251).
A kind of 9. ultrasonic continuous reaction apparatus according to claim 3, it is characterised in that：The discharging of the secondary circulating pump (61)
End is provided with the 3rd valve body (63), and the other end of the 3rd valve body (63) connects secondary circulation pipe (62), the charging of secondary circulating pump (61)
End is provided with the 4th valve body (64), and the 4th valve body (64) connects the discharge end of second circulation pipe (60), second circulation pipe (60)
The other end connects secondary vomit pipe (24), and the second vomit pipe (65), the second vomit pipe have been connected in the middle part of second circulation pipe (60)
(65) it is provided with the second baiting valve (66).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720687687.XU CN206881693U (en) | 2017-06-14 | 2017-06-14 | A kind of ultrasonic continuous reaction apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720687687.XU CN206881693U (en) | 2017-06-14 | 2017-06-14 | A kind of ultrasonic continuous reaction apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206881693U true CN206881693U (en) | 2018-01-16 |
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ID=61318332
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720687687.XU Expired - Fee Related CN206881693U (en) | 2017-06-14 | 2017-06-14 | A kind of ultrasonic continuous reaction apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206881693U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111760517A (en) * | 2020-07-01 | 2020-10-13 | 西安交通大学 | Supercritical hydrothermal synthesis system and method capable of switching multi-material mixing mode and sequence |
-
2017
- 2017-06-14 CN CN201720687687.XU patent/CN206881693U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111760517A (en) * | 2020-07-01 | 2020-10-13 | 西安交通大学 | Supercritical hydrothermal synthesis system and method capable of switching multi-material mixing mode and sequence |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180116 Termination date: 20210614 |