CN206881639U - A kind of sulfonated graphene preparation ultrasonic mixing device - Google Patents
A kind of sulfonated graphene preparation ultrasonic mixing device Download PDFInfo
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- CN206881639U CN206881639U CN201720813139.7U CN201720813139U CN206881639U CN 206881639 U CN206881639 U CN 206881639U CN 201720813139 U CN201720813139 U CN 201720813139U CN 206881639 U CN206881639 U CN 206881639U
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- charging basket
- sulfonated graphene
- mixing device
- agitating
- inwall
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Abstract
It the utility model is related to sulfonated graphene preparing technical field, especially a kind of sulfonated graphene preparation ultrasonic mixing device, including charging basket, supersonic generator and agitating roller, the charging basket is cylindrical barrel structure, the inwall of the charging basket is provided with four mounting grooves, the supersonic generator shares four and is embedded in respectively in mounting groove, the surface in other regions on the inwall of the charging basket in addition to mounting groove is continuous fold plane, the agitating roller is arranged on bowl interior, the bottom of the agitating roller is fixedly connected with sun gear, the outer surface of the sun gear is rotatablely connected four planetary gears, the outside of planetary gear is socketed with gear ring, the gear ring is fixed with charging basket, the planetary gear is socketed in the top of agitating paddle, the outer surface of the agitating paddle is continuous fold plane.Ultrasonic wave of the present utility model can constantly be folded in charging basket by reflection, improve the efficiency of mixing.
Description
Technical field
The present invention relates to sulfonated graphene preparing technical field, more particularly to a kind of sulfonated graphene preparation to be mixed with ultrasonic wave
Attach together and put.
Background technology
The A of patent No. CN 103359782 refer to a kind of preparation method of sulfonated graphene, and its preparation process is by sulfuric acid
Ammonium and graphene oxide are 1 according to mass ratio:1~20 ratio is mixed and is dissolved in deionized water, and ultrasonic wave scattered 10~
60min, mixture is uniformly dispersed in water, then water is gone using rotary evaporation, by the above-mentioned freeze-dried place of resulting mixture
Then reason is heated to 100~300 DEG C under argon gas or nitrogen atmosphere and is incubated 30~60min, obtain black until being completely dried
Puffy sulfonated graphene powder, need to use ultrasonic mixer in its preparation process that ammonium sulfate and graphene oxide is equal
Even is mixed into deionized water, and the A of patent No. CN 102294192 refer to a kind of ultrasonic mixing device, it include charging basket,
Pump and supersonic generator, the mixed liquor in charging basket is extracted out by pump, charging basket is being sent back to after supersonic generator, is expecting
Stirring rod is additionally provided with bucket or scattered oar is stirred to mixed liquor, and in the apparatus, supersonic generator only passes through in mixed liquor
It is out-of-date to play immixture to the liquid of part, and directly the mixed liquor of bowl interior can not be mixed, efficiency compared with
Low, in order to improve efficiency, we have proposed a kind of sulfonated graphene preparation ultrasonic mixing device.
The content of the invention
The invention aims to solve shortcoming present in prior art, and prepared by a kind of sulfonated graphene proposed
Use ultrasonic mixing device.
To achieve these goals, present invention employs following technical scheme：
A kind of sulfonated graphene preparation ultrasonic mixing device, including charging basket, supersonic generator and agitating roller are designed,
The charging basket is cylindrical barrel structure, and the inwall of the charging basket is provided with four mounting grooves, and the supersonic generator shares
Four and it is embedded in respectively in mounting groove, the surface in other regions on the inwall of the charging basket in addition to mounting groove is to connect
Continuous fold plane, the agitating roller are arranged on bowl interior, and the bottom of the agitating roller is fixedly connected with sun gear, the sun gear
Outer surface be rotatablely connected four planetary gears, the outside of planetary gear is socketed with gear ring, and the gear ring is fixed with charging basket, the planet
Wheel is socketed in the top of agitating paddle, and the outer surface of the agitating paddle is continuous fold plane.
Preferably, the bottom of the agitating roller is fixedly connected through the upper surface of charging basket with the output end of stirring motor, institute
State stirring motor and be fixed on charging basket upper end.
Preferably, the angle folding of the fold plane outside the fold plane and agitating paddle on the charging basket inwall is 120 °.
Preferably, the upper surface of the charging basket is provided with charging aperture, and the bottom side of charging basket is provided with discharging opening.
A kind of sulfonated graphene preparation ultrasonic mixing device proposed by the present invention, beneficial effect are：
1st, the surface of charging basket inwall of the invention and agitating paddle is equipped with continuous fold plane, can be to ultrasonic transmitter
The ultrasonic wave sent is folded, and improves the efficiency of ultrasonic wave mixing；
2nd, by the way of agitating device of the invention is linked using agitating roller and planet gear transmission system, make agitating paddle be not only able to
Agitating roller revolution, and rotation can also be carried out, the probability that the plane of refraction on agitating paddle is reflected to ultrasonic wave is added, carries
High mixing efficiency.
Brief description of the drawings
Fig. 1 is a kind of structural representation of sulfonated graphene preparation ultrasonic mixing device proposed by the present invention；
Fig. 2 is a kind of agitating roller structural representation of sulfonated graphene preparation ultrasonic mixing device proposed by the present invention
Figure；
Fig. 3 is a kind of charging basket schematic cross-section of sulfonated graphene preparation ultrasonic mixing device proposed by the present invention；
Fig. 4 is that a kind of agitating paddle section of sulfonated graphene preparation ultrasonic mixing device proposed by the present invention is illustrated
Figure.
In figure：1- charging baskets, 2- supersonic generators, 3- agitating rollers, 4- planes of refraction, 5- sun gears, 6- planetary gears, 7- teeth
Circle, 8- agitating paddles, 9- stirring motors, 10- charging apertures, 11- discharging openings.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.
Reference picture 1-4, a kind of sulfonated graphene preparation ultrasonic mixing device, including charging basket 1, supersonic generator 2
With agitating roller 3, the charging basket 1 is cylindrical barrel structure, and the inwall of the charging basket 1 is provided with four mounting grooves, the ultrasound
Wave producer 2 shares four and is embedded in respectively in mounting groove, other areas on the inwall of the charging basket 1 in addition to mounting groove
The surface in domain is continuous fold plane 4, and the agitating roller 3 is arranged on inside charging basket 1, and the bottom of the agitating roller 3, which is fixed, to be connected
Sun gear 5 is connect, the outer surface of the sun gear 5 is rotatablely connected four planetary gears 6, and the outside of planetary gear 6 is socketed with gear ring 7, institute
State gear ring 7 to fix with charging basket 1, the planetary gear 6 is socketed in the top of agitating paddle 8, and the outer surface of the agitating paddle 8 is continuous
Fold plane 4.
The bottom of the agitating roller 3 is fixedly connected through the upper surface of charging basket 1 with the output end of stirring motor 9, described to stir
Mix motor 9 and be fixed on the upper end of charging basket 1, the angle folding of the fold plane 4 on the inwall of charging basket 1 and the fold plane 4 outside agitating paddle 8
It it is 120 °, the upper surface of the charging basket 1 is provided with charging aperture 10, and the bottom side of charging basket 1 is provided with discharging opening 11.
Operation principle：After mixed liquor enters charging basket 1, supersonic generator 2 sends ultrasonic wave, and ultrasonic wave is in charging basket 1
Refraction back and forth is carried out on the plane of refraction of wall and the plane of refraction of agitating paddle 8, the ammonium sulfate in mixed liquor and graphene oxide are entered
Row dispersion mixing, wherein, agitating paddle 8 around agitating roller 3 while revolving round the sun, additionally it is possible to rotation, adds ultrasonic wave refraction
Probability, improve mixed effect.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (4)
1. a kind of sulfonated graphene preparation ultrasonic mixing device, including charging basket (1), supersonic generator (2) and agitating roller
(3), it is characterised in that：The charging basket (1) is cylindrical barrel structure, and the inwall of the charging basket (1) is provided with four mounting grooves,
The supersonic generator (2) shares four and is embedded in respectively in mounting groove, except mounting groove on the inwall of the charging basket (1)
Outside the surface in other regions be continuous fold plane (4), it is internal that the agitating roller (3) is arranged on charging basket (1), described to stir
The bottom for mixing roller (3) is fixedly connected with sun gear (5), and the outer surface of the sun gear (5) is rotatablely connected four planetary gears (6), OK
The outside of star-wheel (6) is socketed with gear ring (7), and the gear ring (7) is fixed with charging basket (1), and the planetary gear (6) is socketed in agitating paddle
(8) top, the outer surface of the agitating paddle (8) is continuous fold plane (4).
A kind of 2. sulfonated graphene preparation ultrasonic mixing device according to claim 1, it is characterised in that：It is described to stir
The bottom for mixing roller (3) is fixedly connected through the upper surface of charging basket (1) with the output end of stirring motor (9), the stirring motor (9)
It is fixed on charging basket (1) upper end.
A kind of 3. sulfonated graphene preparation ultrasonic mixing device according to claim 1, it is characterised in that：The material
The angle folding of fold plane (4) and the fold plane (4) of agitating paddle (8) outside on bucket (1) inwall is 120 °.
A kind of 4. sulfonated graphene preparation ultrasonic mixing device according to claim 1, it is characterised in that：The material
The upper surface of bucket (1) is provided with charging aperture (10), and the bottom side of charging basket (1) is provided with discharging opening (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720813139.7U CN206881639U (en) | 2017-07-06 | 2017-07-06 | A kind of sulfonated graphene preparation ultrasonic mixing device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720813139.7U CN206881639U (en) | 2017-07-06 | 2017-07-06 | A kind of sulfonated graphene preparation ultrasonic mixing device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206881639U true CN206881639U (en) | 2018-01-16 |
Family
ID=61297663
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720813139.7U Expired - Fee Related CN206881639U (en) | 2017-07-06 | 2017-07-06 | A kind of sulfonated graphene preparation ultrasonic mixing device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206881639U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108816461A (en) * | 2018-04-08 | 2018-11-16 | 江苏匠心信息科技有限公司 | A kind of graphene finished product grinding device |
-
2017
- 2017-07-06 CN CN201720813139.7U patent/CN206881639U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108816461A (en) * | 2018-04-08 | 2018-11-16 | 江苏匠心信息科技有限公司 | A kind of graphene finished product grinding device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180116 Termination date: 20180706 |