CN206853153U - A kind of toluene condensate collection device - Google Patents

A kind of toluene condensate collection device Download PDF

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Publication number
CN206853153U
CN206853153U CN201720429243.6U CN201720429243U CN206853153U CN 206853153 U CN206853153 U CN 206853153U CN 201720429243 U CN201720429243 U CN 201720429243U CN 206853153 U CN206853153 U CN 206853153U
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China
Prior art keywords
pipe
layer
condenser
condenser pipe
cotton
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CN201720429243.6U
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Inventor
徐小亮
曾凡波
徐华
程胜利
李宗荣
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Zhejiang Taizhou Lianchuang Environmental Protection Technology Co., Ltd.
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Zhejiang Taizhou Lian Environmental Protection Technology Co Ltd
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Abstract

The utility model discloses a kind of toluene condensate collection device, it is good to aim to provide a kind of condensation effect, collecting effect is good, safe toluene condensate collection device, its drip irrigation device is a kind of toluene condensate collection device, including distillation still, condenser and collecting box, the distillation still includes escape pipe, condenser includes cold water pipe and the condenser pipe being placed in cold water pipe, condenser pipe is connected with escape pipe by dissipating air cavity, dissipate the internal diameter of air cavity is increased by one end to the one end being connected with condenser pipe being connected with escape pipe in gradual, condenser pipe is more and connected with scattered air cavity, condenser pipe is in the shape of a spiral, mozzle and adsorption layer are provided with collecting box, mozzle one end is connected with condenser pipe by liquid collecting cavity, the mozzle other end is placed on below adsorption layer through absorption, the utility model is applied to technical field of chemical.

Description

A kind of toluene condensate collection device
Technical field
A kind of technical field of chemical is the utility model is related to, more specifically, it relates to which a kind of condensation of toluene is collected Device.
Background technology
Toluene is needed to carry out condensation collection when passing through distilation, but existing condensing unit is generally difficult in steam Toluene total condensation, condensation effect is insufficient, and the toluene remained in gas can be remained in collecting box with gaseous state, under collecting effect Drop, and the gaseous state toluene remained can form explosive mixture with air, influence security.
Utility model content
In view of the deficienciess of the prior art, the purpose of this utility model is to provide, a kind of condensation effect is good, collects effect Good, the safe toluene condensate collection device of fruit.
To achieve the above object, the utility model provides following technical scheme:A kind of toluene condensate collection device, including Distillation still, condenser and collecting box, it is characterized in that:The distillation still includes escape pipe, and condenser includes cold water pipe and is placed in cold Condenser pipe in water pipe, condenser pipe and escape pipe connects by dissipating air cavity, and the internal diameter of scattered air cavity is by one end for being connected with escape pipe To one end for be connected with condenser pipe in gradually increase, condenser pipe is more and is connected with scattered air cavity, condenser pipe in the shape of a spiral, Mozzle and adsorption layer are provided with collecting box, mozzle one end is connected with condenser pipe by liquid collecting cavity, and the mozzle other end passes through Absorption is placed on below adsorption layer.
By using above-mentioned technical proposal, during pipe condensed through steam stream caused by distillation, pass through the cooling in cold water pipe Water is cooled down, and steam is turned into liquid from gaseous state, and toluene can be layered with water after cooling, cold in order to improve so as to be collected Solidifying effect, more and diameter is as far as possible small as far as possible for the quantity of condenser pipe, can increase the contact area of condenser pipe and cooling water, improve cold Solidifying effect, because condenser pipe and escape pipe connects by dissipating air cavity, the internal diameter of scattered air cavity by one end for being connected with escape pipe extremely with It is easy to steam to disperse in gradually increase, reduces vapour concentration, steam is dispersed into each condenser pipe in one end of condenser pipe connection It is interior, condensation effect is improved, condenser pipe in the shape of a spiral, further improves cooling water to the cooling effect of steam, condensed first Benzene is flowed into collecting box by mozzle, and the steam remained in mozzle can be adsorbed layer and be adsorbed, if the toluene in collecting box Volatilization, can also be adsorbed layer and be adsorbed, and so as to prevent toluene from forming explosive mixture with air, improve security.
The utility model is further arranged to:The condenser is by close to one end of distillation still to one end of close collecting box Set in tilting down, cold water pipe includes cooling water inlet and cooling water outlet, and cooling water inlet is placed in the lowest part of cold water pipe, and cold water goes out Mouth is placed in the highest point of cold water pipe.
By using above-mentioned technical proposal, cooling water flows into from the lowest part of cold water pipe, then from the highest point of cold water pipe Outflow, cooling water can be made to carry out condenser pipe sufficiently cool.
The utility model is further arranged to:The adsorption layer includes filter and scrim layer, and scrim layer includes cotton-spinning layer It is provided with and lives and carbon fiber layer, carbon fiber layer, cotton-spinning layer and filter overlap successively from top to bottom, between cotton-spinning layer and carbon fiber layer Property charcoal particle.
By using above-mentioned technical proposal, carbon fiber layer, cotton-spinning layer and filter are both secured in collecting box, and cotton-spinning layer can To be adsorbed to the moisture in entrained steam, activated carbon granule can adsorb to the toluene in entrained steam, carbon fiber Layer can be adsorbed further to the toluene in entrained steam, and so as to improve adsorption effect, filter plays barriering effect, makes Most of entrained steam is trapped on filter, so as to be back to collecting box bottom.
The utility model is further arranged to:The filter opening aperture of the filter is by close to the side of cotton-spinning layer to remote cotton The side of tissue layer is in be gradually reduced.
By using above-mentioned technical proposal, when scrim layer is to vapor sorption saturation, the meeting shape globule, the globule can pass through The filter opening of filter plate is back to the bottom of collecting box, because the aperture of filter is by close to the side of cotton-spinning layer to remote cotton-spinning layer Side is in being gradually reduced, i.e. the aperture of filter opening is gradually reduced from top to bottom, i.e. perforated area of the filter close to cotton-spinning layer side More than the perforated area that filter deviates from cotton-spinning layer side, the small side of perforated area can increase the barriering effect to steam, The big side of perforated area is easy to the globule to flow back, and is easily clumped together when the globule flows through filter opening, accelerates backflow.
Brief description of the drawings
Fig. 1 is a kind of structural representation of toluene condensate collection device embodiment of the utility model.
Fig. 2 is the structural representation of adsorption layer in a kind of toluene condensate collection device embodiment of the utility model.
Reference is in figure, 1- distillation stills, 2- condensers, 3- collecting boxs, 4- escape pipes, 5- cold water pipes, 6- condenser pipes, 7- dissipates air cavity, 8- mozzles, 9- adsorption layers, 10- liquid collecting cavities, 11- cooling water inlets, 12- cooling water outlets, 20- filters, 21- cottons Tissue layer, 22- carbon fiber layers, 23- activated carbon granules.
Embodiment
A kind of condensate collection device embodiment of the utility model is described further referring to figs. 1 to Fig. 2.
A kind of toluene condensate collection device, including distillation still 1, condenser 2 and collecting box 3, it is characterized in that:The distillation still 1 includes escape pipe 4, and condenser 2 includes cold water pipe 5 and the condenser pipe 6 being placed in cold water pipe 5, and condenser pipe 6 passes through with escape pipe 4 Dissipate air cavity 7 to connect, the internal diameter for dissipating air cavity 7 is increased by one end to the one end being connected with condenser pipe 6 being connected with escape pipe 4 in gradual Add, condenser pipe 6 is more and connected with scattered air cavity 7, and condenser pipe 6 is provided with mozzle 8 and inhaled in the shape of a spiral, in collecting box 3 Attached layer 9, the one end of mozzle 8 are connected with condenser pipe 6 by liquid collecting cavity 10, and the other end of mozzle 8 is placed in adsorption layer through adsorption layer 9 9 lower sections.
By using above-mentioned technical proposal, during pipe 6 condensed through steam stream caused by distillation, by cold in cold water pipe 5 But water is cooled down, and steam is turned into liquid from gaseous state, and toluene can be layered with water after cooling, so as to be collected, in order to improve Condensation effect, more and diameter is as far as possible small as far as possible for the quantity of condenser pipe 6, can increase the contact area of condenser pipe 6 and cooling water, carry High condensation effect, because condenser pipe 6 and escape pipe 4 connect by dissipating air cavity 7, the internal diameter of air cavity 7 is dissipated by being connected with escape pipe 4 It is easy to steam to disperse in gradually increase, reduces vapour concentration, be dispersed into steam in one end to one end being connected with condenser pipe 6 In each condenser pipe 6, condensation effect is improved, condenser pipe 6 in the shape of a spiral, further improves cooling effect of the cooling water to steam, Condensed toluene is flowed into collecting box 3 by mozzle 8, and the steam remained in mozzle 8 can be adsorbed layer 9 and be adsorbed, if Toluene volatilization in collecting box 3, can also be adsorbed layer 9 and be adsorbed, so as to prevent toluene from forming explosive mixture with air, be carried High security.
The utility model is further arranged to:The condenser 2 is by close to one end of distillation still 1 to close collecting box 3 One end is in setting is tilted down, and cold water pipe 5 includes cooling water inlet 11 and cooling water outlet 12, and cooling water inlet 11 is placed in cold water pipe 5 Lowest part, cooling water outlet 12 are placed in the highest point of cold water pipe 5
By using above-mentioned technical proposal, cooling water flows into from the lowest part of cold water pipe 5, then from the highest of cold water pipe 5 Place's outflow, can make cooling water carry out condenser pipe 6 sufficiently cool.
The utility model is further arranged to:The adsorption layer 9 includes filter 20 and scrim layer, and scrim layer is knitted including cotton Layer 21 and carbon fiber layer 22, carbon fiber layer 22, cotton-spinning layer 21 and filter 20 overlap successively from top to bottom, and cotton-spinning layer 21 and carbon are fine Activated carbon granule 23 is provided between dimension layer 22.
By using above-mentioned technical proposal, carbon fiber layer 22, cotton-spinning layer 21 and filter 20 are both secured in collecting box 3, Cotton-spinning layer 21 can be adsorbed to the moisture in entrained steam, and activated carbon granule 23 can be carried out to the toluene in entrained steam Absorption, carbon fiber layer 22 can be adsorbed further to the toluene in entrained steam, so as to improve adsorption effect, filter 20 Barriering effect is played, most of entrained steam is trapped on filter 20, so as to be back to the bottom of collecting box 3.
The utility model is further arranged to:The filter opening aperture of the filter 20 by close to the side of cotton-spinning layer 21 to remote Side from cotton-spinning layer 21 is in be gradually reduced.
By using above-mentioned technical proposal, when scrim layer is to vapor sorption saturation, the meeting shape globule, the globule can pass through The filter opening of filter plate 20 is back to the bottom of collecting box 3, due to filter 20 aperture by close to the side of cotton-spinning layer 21 to remote The side of cotton-spinning layer 21 is in being gradually reduced, i.e. the aperture of filter opening is gradually reduced from top to bottom, i.e., filter 20 is close to cotton-spinning layer 21 The perforated area of side is more than the perforated area that filter 20 deviates from the side of cotton-spinning layer 21, and the small side of perforated area can increase To the barriering effect of steam, the big side of perforated area is easy to the globule to flow back, and is easily clumped together when the globule flows through filter opening, Accelerate backflow.
Preferred embodiment of the present utility model is the foregoing is only, not limiting the utility model, the skill of this area Art personnel carry out common variations and alternatives in the range of technical solutions of the utility model should all be included in guarantor of the present utility model In the range of shield.

Claims (4)

1. a kind of toluene condensate collection device, including distillation still, condenser and collecting box, it is characterized in that:The distillation still includes Escape pipe, condenser include cold water pipe and the condenser pipe being placed in cold water pipe, and condenser pipe is connected with escape pipe by dissipating air cavity, is dissipated The internal diameter of air cavity is for more and equal in gradually increase, condenser pipe by one end that the one end being connected with escape pipe is extremely connected with condenser pipe Connected with scattered air cavity, condenser pipe in the shape of a spiral, is provided with mozzle and adsorption layer, mozzle one end leads to condenser pipe in collecting box Liquid collecting cavity connection is crossed, the mozzle other end is placed on below adsorption layer through absorption.
2. a kind of toluene condensate collection device according to claim 1, it is characterized in that:The condenser is by close to distillation still One end to close to one end of collecting box, in tilting down setting, cold water pipe includes cooling water inlet and cooling water outlet, cooling water inlet The lowest part of cold water pipe is placed in, cooling water outlet is placed in the highest point of cold water pipe.
3. a kind of toluene condensate collection device according to claim 1, it is characterized in that:The adsorption layer include filter and Scrim layer, scrim layer include cotton-spinning layer and carbon fiber layer, and carbon fiber layer, cotton-spinning layer and filter overlap successively from top to bottom, cotton Activated carbon granule is provided between tissue layer and carbon fiber layer.
4. a kind of toluene condensate collection device according to claim 3, it is characterized in that:The filter opening aperture of the filter by It is in be gradually reduced close to the side of cotton-spinning layer to the side of remote cotton-spinning layer.
CN201720429243.6U 2017-04-22 2017-04-22 A kind of toluene condensate collection device Active CN206853153U (en)

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CN201720429243.6U CN206853153U (en) 2017-04-22 2017-04-22 A kind of toluene condensate collection device

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Application Number Priority Date Filing Date Title
CN201720429243.6U CN206853153U (en) 2017-04-22 2017-04-22 A kind of toluene condensate collection device

Publications (1)

Publication Number Publication Date
CN206853153U true CN206853153U (en) 2018-01-09

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112321419A (en) * 2020-11-10 2021-02-05 安徽海顺化工有限公司 Separation and drying process for preparing intermediate of 2-4- (chlorphenyl) -3-methylbutyryl chloride
CN118491131A (en) * 2024-07-16 2024-08-16 烟台丰鲁精细化工有限责任公司 Benzene liquid separation and collection device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112321419A (en) * 2020-11-10 2021-02-05 安徽海顺化工有限公司 Separation and drying process for preparing intermediate of 2-4- (chlorphenyl) -3-methylbutyryl chloride
CN118491131A (en) * 2024-07-16 2024-08-16 烟台丰鲁精细化工有限责任公司 Benzene liquid separation and collection device

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Address after: 317000 Taizhou City, Zhejiang Province, chemical raw material base Lin Hai Park

Patentee after: Zhejiang Taizhou Lianchuang Environmental Protection Technology Co., Ltd.

Address before: 317000 Taizhou City, Zhejiang Province, Zhejiang province chemical raw material base Lin Hai Park

Patentee before: Zhejiang Taizhou LIAN Environmental Protection Technology Co., Ltd.

CP03 Change of name, title or address