CN206828476U - continuous high-efficient fractional distillation device - Google Patents
continuous high-efficient fractional distillation device Download PDFInfo
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- CN206828476U CN206828476U CN201720704803.4U CN201720704803U CN206828476U CN 206828476 U CN206828476 U CN 206828476U CN 201720704803 U CN201720704803 U CN 201720704803U CN 206828476 U CN206828476 U CN 206828476U
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Abstract
The application is related to a kind of grape wine distillation equipment, more particularly to a kind of continuous high-efficient fractional distillation device；It includes destilling tower, main condenser device, thermal source, low-temperature receiver, grape water pot and at least fractional distillation equipment of one-level；Fractional distillation equipment per one-level includes distillation case, fractional condensing unit, finished product storage tank；Distillation case is provided with the classification charging aperture for being easy to wine liquid body to enter, is easy to the classification gas outlet that wine steam is discharged, the classification liquid outlet for being easy to wine liquid body to discharge.Due to implementation above-mentioned technical proposal, karusen is removed raffinate by raffinate discharge pipe in the application；The relatively low wine steam of concentration again by distillation case at different levels, obtain purity from high to low, quality, by classification wine steam more at least and the grape water without alcoholic strength, avoid continuous still, aromatic substance from losing by fractional condensing unit by excellent to secondary, fragrant containing substance；Whole technique is continuous, sustainable a large amount of productions, can also directly obtain high, medium and low former wine and grape water.
Description
Technical field
The application is related to a kind of grape wine distillation equipment, more particularly to a kind of continuous high-efficient fractional distillation device.
Background technology
The distillation technique of grape wine is mainly two kinds both at home and abroad at present：Tower distillation and kettle formula；Tower distillation is whole
Still-process is continuous, can successively obtain the higher grape wine steam of alcoholic strength, be characterized in continuous still, yield
Height, but obtained Spirit is single, it is impossible to it is classified.Alcoholic solution is needed to distill repeatedly in kettle formula, and alcohol is can obtain per kettle
Grape wine, can be classified, be characterized in batch distillation, yield poorly by the different Spirit of concentration, but its remain it is very rich
Rich aromatic substance, suitable for brewageing the grape wine of high-quality.There is presently no a kind of distillation equipment that can combine the two advantage.
The content of the invention
The purpose of the application be to propose it is a kind of can continuous, high yield production high-quality wine spirit, grape can be preserved
Aromatic substance, removal harmful substance, the continuous high-efficient fractional distillation device that wine spirit is classified inside wine.
What the application was realized in：Continuous high-efficient fractional distillation equipment, it include destilling tower, main condenser device, thermal source,
Low-temperature receiver, grape water pot and at least fractional distillation equipment of one-level；Fractional distillation equipment per one-level is cold including distillation case, classification
Solidifying device, finished product storage tank；Distillation case is provided with the classification charging aperture for being easy to wine liquid body to enter, is easy to the classification of wine steam discharge to go out
Gas port, the classification liquid outlet for being easy to wine liquid body to discharge, main condenser device are provided with the main condenser charging aperture for being easy to wine steam to enter
With the main condenser discharging opening for being easy to the wine liquid body discharge after cooling down, fractional condensing unit is provided with the classification for being easy to wine steam to enter
Condensation charging aperture and the fractional condensaion discharging opening for being easy to the wine liquid body discharge after cooling；Classification gas outlet per one-level on distillation case
It is connected by pipeline with the fractional condensaion charging aperture on corresponding fractional condensing unit, the fractional condensaion on fractional condensing unit goes out
Material mouth is connected by pipeline with corresponding finished product storage tank；Karusen inlet pipe and raffinate discharge pipe, destilling tower are installed on destilling tower
Top is connected by pipeline with main condenser charging aperture, and main condenser discharging opening is connected by pipeline with the classification charging aperture of the first order,
Classification liquid outlet is connected with the classification charging aperture or grape water pot of next stage；Thermal source is by pipeline respectively with destilling tower, per one-level
Distillation case be connected；Low-temperature receiver is connected by fractional condensing unit of the pipeline respectively with main condenser device, per one-level.
Further, distilling case includes being sequentially fixed at upper box, flange and lower box together from top to bottom；Lower box
The top of side is provided with high-temperature steam import, and the bottom of lower box opposite side exports provided with high-temperature condensation water, high-temperature steam import,
High-temperature condensation water outlet is connected with thermal source respectively；Lower box bottom is provided with classification charging aperture and is connected with more through lower box
Heat exchanger tube, the upper port of heat exchanger tube communicate with upper box；The bottom of upper box is provided with classification liquid outlet, and the top of upper box is provided with
It is classified gas outlet；Upper box is built-in with least one layer of float valve, or/and, at least one layer of bubble cap tray.
Further, in addition to the reboiler that is connected between thermal source and destilling tower, by two-way between reboiler and thermal source
Pipeline is connected, and is connected between reboiler and destilling tower by two-way pipeline.
Further, be sequentially provided with the pipeline between main condenser discharging opening and the classification charging aperture of the first order temporary storage tank,
Reflux pump.
Further, in addition to finished product condensing unit, finished product condensing unit are provided with the finished product condensation for being easy to wine liquid body to enter
Charging aperture and the finished product condensation discharging opening for being easy to the wine liquid body discharge after cooling；Fractional condensaion discharging opening is cold with finished product by pipeline
Solidifying charging aperture is connected, and finished product condensation discharging opening is connected with finished pot；Finished product condensing unit is connected between low-temperature receiver by two-way pipeline.
Due to implementation above-mentioned technical proposal, karusen obtains the relatively low wine steam of concentration by destilling tower and led in the application
Raffinate discharge pipe is crossed to remove raffinate；The relatively low wine steam of concentration again by distillation case at different levels, obtain purity from high to low, product
Matter, by classification wine steam more at least and the grape water without alcoholic strength, passes through fractional condensing unit by excellent to secondary, fragrant containing substance
Avoid continuous still, aromatic substance loss；Whole technique is continuous, sustainable a large amount of productions, can also directly obtain high, medium and low
Former wine and grape water, can arbitrarily be allocated after storage, raw materials used to be all from grape in itself, safe and non-toxic, allotment is blent
The wine spirit mouthfeel obtained afterwards is naturally, best in quality.
Brief description of the drawings：The concrete structure of the application is provided by following drawings and examples：
Fig. 1 is the structural representation of the embodiment of the present application 1；
Fig. 2 is the structural representation for distilling case.
Legend：1. destilling tower, 2. main condenser devices, 3. thermals source, 4. low-temperature receivers, 5. grape water pots, 6. distillation casees, 601. top boxs
Body, 602. lower boxes, 603. high-temperature steam imports, the outlet of 604. high-temperature condensation waters, 605. heat exchanger tubes, 606. float valves, 607. methods
Orchid, 7. fractional condensing units, 8. finished product storage tanks, 9. classification charging apertures, 10. classification gas outlets, 11. classification liquid outlets, 12. masters are cold
Solidifying charging aperture, 13. main condenser discharging openings, 14. fractional condensaion charging apertures, 15. fractional condensaion discharging openings, 16. karusen inlet pipes,
17. raffinate discharge pipe, 18. reboilers, 19. temporary storage tanks, 20. reflux pumps, 21. finished product condensing units, the condensation charging of 22. finished products
Mouthful, 23. finished products condensation discharging opening.
Embodiment：
The application is not limited by following embodiments, can be determined specifically with actual conditions according to the technical scheme of the application
Embodiment.
As shown in Figure 1, 2, continuous high-efficient fractional distillation equipment include destilling tower 1, main condenser device 2, thermal source 3, low-temperature receiver 4,
The fractional distillation equipment of grape water pot 5 and at least one-level；Fractional distillation equipment per one-level includes distillation case 6, fractional condensaion
Device 7, finished product storage tank 8；Distillation case 6 is provided with the classification charging aperture 9 for being easy to wine liquid body to enter, the classification for being easy to wine steam to discharge
Gas outlet 10, the classification liquid outlet 11 for being easy to wine liquid body to discharge, main condenser device 2 are provided with the main condenser for being easy to wine steam to enter
Charging aperture 12 and the main condenser discharging opening 13 for being easy to the wine liquid body discharge after cooling, fractional condensing unit 7, which is provided with, is easy to wine to steam
The fractional condensaion charging aperture 14 that vapour enters and the fractional condensaion discharging opening 15 for being easy to the wine liquid body discharge after cooling down；Distilled per one-level
Classification gas outlet 10 on case 6 is connected by pipeline with the fractional condensaion charging aperture 14 on corresponding fractional condensing unit 7, classification
Fractional condensaion discharging opening 15 on condensing unit 7 is connected by pipeline with corresponding storage tank 8；Karusen is installed on destilling tower 1
Inlet pipe 16 and raffinate discharge pipe 17, the top of destilling tower 1 are connected by pipeline with main condenser charging aperture 12, and main condenser discharging opening 13 is logical
Cross pipeline with the classification charging aperture 9 of the first order to be connected, the classification charging aperture 9 or grape water pot 5 of classification liquid outlet 11 and next stage
It is connected；Thermal source 3 is connected by distillation case 6 of the pipeline respectively with destilling tower 1, per one-level；Low-temperature receiver 4 by pipeline respectively with main condenser
Device 2, the fractional condensing unit 7 per one-level are connected.
As shown in Fig. 2 distillation case 6 includes being sequentially fixed at upper box 601, flange 607 and nowel together from top to bottom
Body 602；The top of the side of lower box 602 is provided with high-temperature steam import 603, and the bottom of the opposite side of lower box 602 is cold provided with high temperature
Condensate outlet 604, high-temperature steam import 603, high-temperature condensation water outlet 604 are connected with thermal source 3 respectively；The bottom of lower box 602 is set
There is classification charging aperture 9 and be connected with the more heat exchanger tubes 605 for running through lower box 602, the upper port and upper box of heat exchanger tube 605
601 communicate；The bottom of upper box 601 is provided with classification liquid outlet 11, and the top of upper box is provided with classification gas outlet 10；In upper box
At least one layer of float valve 606 is equipped with, or/and, at least one layer of bubble cap tray.During work, wine liquid body enters lower box from classification charging aperture 9
In 602, the generation distillation of upper box 601 is entered under the effect of heat exchanger tube 605, is changed into the high gas of alcoholic strength from classification outlet
Mouth 10 escapes, and the low liquid of alcoholic strength flows out from classification liquid outlet 11.
As shown in figure 1, continuous high-efficient fractional distillation equipment also includes the reboiler being connected between thermal source 3 and destilling tower 1
18, it is connected between reboiler 18 and thermal source 3 by two-way pipeline, is connected between reboiler 18 and destilling tower 1 by two-way pipeline.Boil again
Device 18 is by device described in the patent No. " 201220738371.6 ", and purpose is efficiently to utilize heat energy；In this application, it is high
Warm steam need to be required to heat to destilling tower 1, distillation case 6 at different levels, so can more save the energy.
As shown in figure 1, sequentially it is provided with pipeline between main condenser discharging opening 13 and the classification charging aperture 9 of the first order temporary
Tank 19, reflux pump 20.
As shown in figure 1, continuous high-efficient fractional distillation equipment also includes finished product condensing unit 21, finished product condensing unit 21 is provided with
It is easy to the finished product condensation charging aperture 22 that wine liquid body enters and the finished product condensation discharging opening 23 for being easy to the wine liquid body after cooling to discharge；Point
Level condensation discharging opening 15 condenses charging aperture 22 with finished product by pipeline and is connected, and finished product condensation discharging opening 23 is connected with finished pot；Into
It is connected between product condensing unit 21 and low-temperature receiver 4 by two-way pipeline.
The continuous high-efficient fractional distillation technique processed using the application：The first step, karusen are sent into destilling tower 1 and carried out
Distillation, the column bottom temperature of destilling tower 1 are 75 DEG C to 110 DEG C, and according to the Type Control steam pressure of tower still and fermentation
Wine with dregs flow is remaining in destilling tower 1 to obtain alcohol concentration as 20%vol to 35%vol wine steam and deliver to main condenser device 2
A raffinate part returns to reboiler 18 and produces steam, and a part is discharged by raffinate discharge pipe 17；Second step, in above-mentioned steps
The wine steam arrived is former wine before 40 DEG C to 60 DEG C of classification through the condensation temperature of main condenser device 2；3rd step, gained in second step
Former wine passes sequentially through fractional distillation equipment at different levels before classification, obtain purity from high to low, quality steamed by excellent to secondary classification wine
Vapour and the grape water without alcoholic strength.
Former wine before classification obtained by second step is sent into the distillation case 6 of the first order, in the high-temperature steam effect that thermal source 3 is sent out
Under, one-level wine steam and one-level wine liquid body are obtained, one-level wine steam is sent into the first order by the classification gas outlet 10 of the first order
Fractional condensing unit 7 cool down after obtain temperature 25 DEG C to 35 DEG C alcohol concentration 75%vol to 85%vol highly former wine simultaneously
Storage, one-level wine liquid body are sent into the distillation case 6 of the second level by the classification liquid outlet 11 of the first order；One-level wine liquid body is in thermal source 3
Under the high-temperature steam effect of submitting, two level wine steam and two level wine liquid body are obtained, two level wine steam is gone out by the classification of the second level
Gas port 10 be sent into the second level fractional condensing unit 7 cool down after obtain temperature 25 DEG C to 35 DEG C of alcohol concentration in 35%vol extremely
75%vol moderate former wine is simultaneously stored, and two level wine liquid body is sent into the distillation case 6 of the third level by the classification liquid outlet 11 of the second level；
The distillation case 6 of the third level obtains three-level wine steam and grape water, three-level wine steam under the high-temperature steam effect that thermal source 3 is sent out
Temperature is obtained at 25 DEG C to 35 DEG C after the cooling of fractional condensing unit 7 of the third level is sent into by the classification gas outlet 10 of the third level
Alcohol concentration 10%vol to 35%vol low former wine and store, grape water is sent into Portugal by the classification liquid outlet 11 of the third level
Grape water pot 5 is stored.
Allocated with highly former wine, moderate former wine, low former wine and the grape water after storage ageing, appointed without addition
What distilled water or pure water, reach the purpose of anhydrous allotment；It is raw materials used to be all from grape in itself, safe and non-toxic, minuent fractionation
Wine former wine composition is naturally pollution-free, and the grape wine mouthfeel obtained after being blent with height fractionation wine former wine allotment is natural and increases wind
Taste, it is best in quality, it is uneven that the grape wine quality level finally brewageed caused by water quality difference will not be produced.
Grape fermentation wine with dregs is distilled by the application device, shown in obtained tables of data 1（Due to grape variety, production
The difference of ground, weather, maturity and fermented bacterium technique, may cause data to be deviated）.
It can be seen from the data analysis of table 1：Acted on by fractional distillation equipment, high degree remains esters virtue in wine
Studies of The Aromatic Substances, the harmful substances such as acetic acid, enanthic acid, octanoic acid are reduced, improve the quality of wine.Simultaneously respectively obtain highly former wine, in
Former wine, the former wine of three kinds of qualities of low former wine are spent, wherein aromatic substance is held up in highly former wine, and harmful substance is less, wine
Smart concentration highest；The reservation of moderate former wine aromatic substance is more, and harmful substance is less, and alcohol concentration is medium；Low former wine aromatic substance
Quality guarantee is stayed less, and harmful substance is minimum, and alcohol concentration is minimum.
Highly former wine, moderate former wine, low former wine and the grape water obtained with the application is allocated, and is made respectively
50vol and 30vol wine, it is as shown in table 2 to make formula.It can be seen that can using four kinds of products obtained by the application according to table 2
Directly to allocate the high, medium and low wine of the various number of degrees；Simplify technique, and it is raw materials used be all from grape in itself, it is safe and non-toxic,
Mouthfeel is natural.
Above technical characteristic constitutes embodiments herein, and it has stronger adaptability and implementation result, can basis
The inessential technical characteristic of increase and decrease is actually needed, to meet the needs of different situations.
Table 1
Table 2
Claims (8)
- A kind of 1. continuous high-efficient fractional distillation device, it is characterised in that：Including destilling tower, main condenser device, thermal source, low-temperature receiver, Portugal The fractional distillation equipment of grape water pot and at least one-level；Per one-level fractional distillation equipment include distillation case, fractional condensing unit, Finished product storage tank；Distillation case is provided with the classification charging aperture for being easy to wine liquid body to enter, is easy to the classification gas outlet, just of wine steam discharge In the classification liquid outlet of wine liquid body discharge, main condenser device is provided with the main condenser charging aperture for being easy to wine steam to enter and is easy to cold But the main condenser discharging opening of the wine liquid body discharge after, fractional condensing unit are provided with the fractional condensaion charging for being easy to wine steam to enter Mouth and the fractional condensaion discharging opening for being easy to the wine liquid body discharge after cooling；Classification gas outlet per one-level on distillation case passes through pipeline It is connected with the fractional condensaion charging aperture on corresponding fractional condensing unit, the fractional condensaion discharging opening on fractional condensing unit passes through Pipeline is connected with corresponding finished product storage tank；Karusen inlet pipe and raffinate discharge pipe are installed on destilling tower, passed through at the top of destilling tower Pipeline is connected with main condenser charging aperture, and main condenser discharging opening is connected by pipeline with the classification charging aperture of the first order, is classified out liquid Mouth is connected with the classification charging aperture or grape water pot of next stage；Thermal source by pipeline respectively with destilling tower, per one-level distillation case It is connected；Low-temperature receiver is connected by fractional condensing unit of the pipeline respectively with main condenser device, per one-level.
- 2. continuous high-efficient fractional distillation device according to claim 1, it is characterised in that：Distill case include from top to bottom according to The secondary upper box being fixed together, flange and lower box；The top of lower box side is provided with high-temperature steam import, and lower box is another The bottom of side exports provided with high-temperature condensation water, and high-temperature steam import, high-temperature condensation water outlet are connected with thermal source respectively；Lower box bottom Portion is provided with classification charging aperture and is connected with the more heat exchanger tubes for running through lower box, and the upper port of heat exchanger tube communicates with upper box；On The bottom of casing is provided with classification liquid outlet, and the top of upper box is provided with classification gas outlet；Upper box is built-in with least one layer of float valve, Or/and at least one layer of bubble cap tray.
- 3. continuous high-efficient fractional distillation device according to claim 1 or 2, it is characterised in that：Also include being connected to thermal source Reboiler between destilling tower, it is connected between reboiler and thermal source by two-way pipeline, by two-way between reboiler and destilling tower Pipeline is connected.
- 4. continuous high-efficient fractional distillation device according to claim 1 or 2, it is characterised in that：Main condenser discharging opening and Temporary storage tank, reflux pump are sequentially installed on pipeline between the classification charging aperture of one-level.
- 5. continuous high-efficient fractional distillation device according to claim 3, it is characterised in that：Main condenser discharging opening and the first order Classification charging aperture between pipeline on temporary storage tank, reflux pump are sequentially installed.
- 6. continuous high-efficient fractional distillation device according to claim 1 or 2, it is characterised in that：Also include finished product condensation dress Put, finished product condensing unit be provided be easy to wine liquid body enter finished product condensation charging aperture and be easy to cooling after wine liquid body discharge into Product condense discharging opening；Fractional condensaion discharging opening condenses charging aperture with finished product by pipeline and is connected, finished product condensation discharging opening and finished product Tank is connected；Finished product condensing unit is connected between low-temperature receiver by two-way pipeline.
- 7. continuous high-efficient fractional distillation device according to claim 3, it is characterised in that：Also include finished product condensing unit, Finished product condensing unit is provided with the finished product condensation charging aperture for being easy to wine liquid body to enter and is easy to the finished product of the wine liquid body discharge after cooling Condense discharging opening；Fractional condensaion discharging opening condenses charging aperture with finished product by pipeline and is connected, finished product condensation discharging opening and finished pot It is connected；Finished product condensing unit is connected between low-temperature receiver by two-way pipeline.
- 8. continuous high-efficient fractional distillation device according to claim 4, it is characterised in that：Also include finished product condensing unit, Finished product condensing unit is provided with the finished product condensation charging aperture for being easy to wine liquid body to enter and is easy to the finished product of the wine liquid body discharge after cooling Condense discharging opening；Fractional condensaion discharging opening condenses charging aperture with finished product by pipeline and is connected, finished product condensation discharging opening and finished pot It is connected；Finished product condensing unit is connected between low-temperature receiver by two-way pipeline.
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| CN201720704803.4U CN206828476U (en) | 2017-06-16 | 2017-06-16 | continuous high-efficient fractional distillation device |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108165440A (en) * | 2018-02-08 | 2018-06-15 | 平南县科力酿酒机械制造有限公司 | Distillation brewing equipment |
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2017
- 2017-06-16 CN CN201720704803.4U patent/CN206828476U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108165440A (en) * | 2018-02-08 | 2018-06-15 | 平南县科力酿酒机械制造有限公司 | Distillation brewing equipment |
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