A kind of device of novel dried recovery of acetic acid sodium
Technical field
Sodium acetate recovery technology field is the utility model is related to, specially a kind of device of novel dried recovery of acetic acid sodium.
Background technology
China's industrialization produces a large amount of industrial wastewaters in building, and has low concentration in the industrial wastewater of part and discards sodium acetate
Solution, sodium acetate are a kind of crystalline solid of colorless and odorless, in atmosphere can be flammable by weathering.It is soluble in water, ethanol is slightly soluble in,
Insoluble in ether.The crystallization water is lost at 123 DEG C.But the taste for having acetic acid of usual wet-method.Hydrolyzed in water.In alkali
Property, esterifying agent and photographic chemical, medicine as organic synthesis, printing and dyeing mordant, buffer, chemical reagent, meat anticorrosion,
Many aspects such as pigment, tanning.Available for producing various chemical products, such as furylacrylic acid, acetate and monoxone.
In the device of traditional dried recovered sodium acetate, sodium acetate is easily deposited in mother liquor tank, is unfavorable for sodium acetate
Recycle, the rate of recovery of sodium acetate is relatively low, easily causes waste, and function is single.
Utility model content
The purpose of this utility model is to provide a kind of device of novel dried recovery of acetic acid sodium, to solve above-mentioned background skill
The sodium acetate proposed in art is easily deposited in mother liquor tank, is unfavorable for the recycling of sodium acetate, and the rate of recovery of sodium acetate is relatively low,
Waste is easily caused, the problem of function is single.
To achieve the above object, the utility model provides following technical scheme:A kind of dress of novel dried recovery of acetic acid sodium
Put, including sodium acetate mother liquor tank, stirring motor, circulating pump, centrifugal atomizer, drying kettle, temperature sensor, heat exchanger, air
Filter, pressure fan, transparent windows, Blowing stopper, air-introduced machine, one-level retracting device, secondary recovery device, stirring vane, filter
Bag and vibrating motor, the stirring motor are fixedly mounted on the top of sodium acetate mother liquor tank, and sodium acetate mother liquor tank and circulating pump
Between be connected by pipeline, the centrifugal atomizer is located at the top of drying kettle, and passes through pipe between drying kettle and circulating pump
Road is connected, and the temperature sensor is embedded on the inwall of drying kettle, and one end of the pressure fan is connected with air cleaner,
And the other end of pressure fan is connected with heat exchanger, the transparent windows are embedded on the outer wall of drying kettle, and the bottom of drying kettle
Portion is provided with Blowing stopper, and the one-level retracting device is connected to the bottom side of drying kettle, and one-level retracting device returns with two level
It is connected between receiving apparatus by pipeline, is connected between the air-introduced machine and secondary recovery device by pipeline, and the pipeline
The top of secondary recovery device is connected to, the filter bag is located at the inner chamber of secondary recovery device, and the outside both ends of filter bag are all provided with
There is vibrating motor.
Preferably, the bottom of the one-level retracting device and secondary recovery device is respectively connected with Blowing stopper.
Preferably, the side of the heat exchanger is connected with jet chimney, and the opposite side of heat exchanger is connected with condensate pipe
Road.
Preferably, the sodium acetate mother liquor tank generally funnel-shaped structure, and the bottom of sodium acetate mother liquor tank is connected with ball
Valve.
Preferably, the stirring vane is provided with multigroup, and the length of stirring vane diminishes successively from top to bottom.
Preferably, the inner chamber of the one-level retracting device also is provided with filter bag.
Compared with prior art, the beneficial effects of the utility model are:The device of the novel dried recovery of acetic acid sodium is provided with
The stirring vane that length differs, sufficiently the acetic acid mother liquid of sodium of bottom in mother liquor tank can be stirred, mixing effect is good, prevents
Sodium acetate precipitation is advantageous to the follow-up recycling of sodium acetate in tank bottom, provided with multistage retracting device, improves the recovery of sodium acetate
Utilization rate, while the separating effect of sodium acetate and filter bag can be increased in the presence of vibrating motor, the service life of filter bag is improved,
Temperature sensor and transparent windows are inlaid with, can timely grasp the internal temperature and drying regime of drying kettle.
Brief description of the drawings
Fig. 1 is the utility model structure diagram;
Fig. 2 is mplifying structure schematic diagram at the utility model A;
Fig. 3 is the utility model secondary recovery device internal structure schematic diagram;
Fig. 4 is Tthe utility model system schematic process flow diagram.
In figure:1st, sodium acetate mother liquor tank, 2, stirring motor, 3, circulating pump, 4, centrifugal atomizer, 5, drying kettle, 6, temperature
Sensor, 7, heat exchanger, 8, air cleaner, 9, pressure fan, 10, transparent windows, 11, Blowing stopper, 12, air-introduced machine, 13, one
Level retracting device, 14, secondary recovery device, 15, stirring vane, 16, filter bag, 17, vibrating motor.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belong to the scope of the utility model protection.
Fig. 1-2-3-4 are referred to, the utility model provides a kind of technical scheme:A kind of dress of novel dried recovery of acetic acid sodium
Put, including sodium acetate mother liquor tank 1, stirring motor 2, circulating pump 3, centrifugal atomizer 4, drying kettle 5, temperature sensor 6, heat exchanger
7th, air cleaner 8, pressure fan 9, transparent windows 10, Blowing stopper 11, air-introduced machine 12, one-level retracting device 13, secondary recovery
Device 14, stirring vane 15, filter bag 16 and vibrating motor 17, stirring motor 2 are fixedly mounted on the top of sodium acetate mother liquor tank 1,
And be connected between sodium acetate mother liquor tank 1 and circulating pump 3 by pipeline, centrifugal atomizer 4 is located at the top of drying kettle 5, and dry
It is connected between dry kettle 5 and circulating pump 3 by pipeline, temperature sensor 6 is embedded on the inwall of drying kettle 5, temperature sensor 6
Model PT100, the temperature inside drying kettle 5 can be detected, so as to preferably be slapped to the temperature inside drying kettle 5
Control, one end of pressure fan 9 is connected with air cleaner 8, and the other end of pressure fan 9 is connected with heat exchanger 7, transparent windows 10
It is embedded on the outer wall of drying kettle 5, and the bottom of drying kettle 5 is provided with Blowing stopper 11, one-level retracting device 13 is connected to drying
The bottom side of kettle 5, and be connected between one-level retracting device 13 and secondary recovery device 14 by pipeline, air-introduced machine 12 and two
It is connected between level retracting device 14 by pipeline, and the pipeline is connected to the top of secondary recovery device 14, the filter bag 16
The inner chamber of secondary recovery device 14 is located at, and the outside both ends of filter bag 16 are equipped with vibrating motor 17.
In above-described embodiment, specifically, the bottom of one-level retracting device 13 and secondary recovery device 14 is all connected with relevant wind
Machine 11, Blowing stopper 11 are also discharger, and one-level retracting device 13 and the sodium acetate of the bottom of secondary recovery device 14 can be unloaded
Material.
In above-described embodiment, specifically, the side of heat exchanger 7 is connected with jet chimney, and the opposite side connection of heat exchanger 7
There is condensing water conduit, delivered a vapor to by jet chimney in heat exchanger 7, so as to entering by the cold wind inside heat exchanger 7
Row heating, while steam coagulation flows out into condensed water from pipeline.
In above-described embodiment, specifically, the generally funnel-shaped structure of sodium acetate mother liquor tank 1, and the bottom of sodium acetate mother liquor tank 1
Portion is connected with ball valve, is advantageous to the cleaning inside Dichlorodiphenyl Acetate mother liquid of sodium tank 1, and the waste liquid after cleaning is flowed out by the ball valve of bottom.
In above-described embodiment, specifically, stirring vane 15 is provided with multigroup, and the length of stirring vane 15 is from top to bottom successively
Diminish, can sufficiently the acetic acid mother liquid of sodium of bottom is stirred in Dichlorodiphenyl Acetate mother liquid of sodium tank 1, mixing effect is good, prevents sodium acetate
Tank bottom is deposited in, is advantageous to the follow-up recycling of sodium acetate.
, can sufficient Dichlorodiphenyl Acetate sodium specifically, the inner chamber of one-level retracting device 13 also is provided with filter bag 16 in above-described embodiment
Recycled, improve the recovery utilization rate of sodium acetate.
Operation principle:When using the device of the novel dried recovery of acetic acid sodium, need first to whole novel dried recovery
The device of sodium acetate has the understanding in a structure, can more easily be used, and starts stirring motor 2, drives length
Also the acetic acid mother liquid of sodium inside the Dichlorodiphenyl Acetate mother liquid of sodium tank 1 of stirring vane 15 to differ is stirred, can sufficiently Dichlorodiphenyl Acetate sodium it is female
The acetic acid mother liquid of sodium of bottom is stirred in flow container 1, prevents that then acetic acid mother liquid of sodium is in circulating pump 3 in tank bottom for sodium acetate precipitation
Conveying under, and uniformly sprayed in the presence of centrifugal atomizer 4 from the top of drying kettle 5, and exchanged heat by heat exchanger 7
It is dried under hot blast effect afterwards, is slipped to the bottom of drying kettle 5 and is drawn off in the presence of Blowing stopper 11, in drying kettle 5
The wind in portion flows out by one-level retracting device 13 with secondary recovery device 14 successively under the gravitation of air-introduced machine 12, is reclaimed in one-level
Device 13 is separated air with sodium acetate with the filtering of the filter bag 16 inside secondary recovery device 14, inside filter bag 16
Sodium acetate is drawn off under the vibration of vibrating motor 17 by the Blowing stopper 11 of bottom.
In summary, general principle, principal character and advantage of the present utility model has been shown and described above.The industry
Technical staff it should be appreciated that the utility model is not restricted to the described embodiments, described in above-described embodiment and specification only
It is to illustrate principle of the present utility model, on the premise of the spirit and scope of the utility model is not departed from, the utility model also has
Various changes and modifications, these changes and improvements are both fallen within claimed the scope of the utility model.The requires of the utility model
Protection domain is defined by appended claims and its effect thing.