CN206746032U - A kind of cumyl peroxide crystallization apparatus - Google Patents

A kind of cumyl peroxide crystallization apparatus Download PDF

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Publication number
CN206746032U
CN206746032U CN201720602597.6U CN201720602597U CN206746032U CN 206746032 U CN206746032 U CN 206746032U CN 201720602597 U CN201720602597 U CN 201720602597U CN 206746032 U CN206746032 U CN 206746032U
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CN
China
Prior art keywords
rotating disk
base
cumyl peroxide
bottle
fixedly installed
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Expired - Fee Related
Application number
CN201720602597.6U
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Chinese (zh)
Inventor
顾健
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TAICANG PLASTIC ADDITIVES FACTORY CO Ltd
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TAICANG PLASTIC ADDITIVES FACTORY CO Ltd
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Priority to CN201720602597.6U priority Critical patent/CN206746032U/en
Application granted granted Critical
Publication of CN206746032U publication Critical patent/CN206746032U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of cumyl peroxide crystallization apparatus, including base and the gate stand for being fixedly mounted on base exterior upper surface, raise-lower hydraulic bar is fixedly installed vertically downward in the middle part of the crossbeam of gate stand, the lower end of raise-lower hydraulic bar is provided with the refrigeration cover of upside down funnel shape structure, it is adhesively fixed on refrigeration cover inwall and is provided with heat insulation inner wall, the external upper of base is fixedly installed ring seat, rotating disk is provided with the center of ring seat and on base, crystallization bottle is provided with rotating disk, thermal insulating seat is provided between ring seat and rotating disk in annulus, the surface of heat insulation inner wall and thermal insulating seat, which is rabbeted, evaporation tube, the inside of base is fixedly installed refrigeration system, centrifuge motor and hydraulic pump.This kind of cumyl peroxide crystallization apparatus crystalline rate is high, time saving and energy saving without repeatedly being crystallized, and increases processing safety.

Description

A kind of cumyl peroxide crystallization apparatus
Technical field
A kind of chemical industry equipment is the utility model is related to, specially a kind of cumyl peroxide crystallization apparatus.
Background technology
Cumyl peroxide produces obtained concentrate, it is necessary to carry out low temperature crystallization after centralized collection, is purified, Existing crystallizer generally use cooling stands still for crystals processing, less efficient, and crystallization content is less, it is necessary to repeatedly be tied Crystalline substance, thus it is time-consuming, and also cumyl peroxide and its raw material are respectively provided with toxicity, add the wind that workers ' health is encroached on Danger.
To solve the above problems, therefore it is proposed that a kind of cumyl peroxide crystallization apparatus.
Utility model content
The technical problems to be solved in the utility model is the defects of overcoming prior art, there is provided a kind of cumyl peroxide Crystallization apparatus, in order to solve the above-mentioned technical problem, the utility model provide following technical scheme:
A kind of cumyl peroxide crystallization apparatus of the utility model, including base and it is fixedly mounted on base exterior upper table The gate stand in face, the crossbeam middle part of the gate stand are fixedly installed raise-lower hydraulic bar, the raise-lower hydraulic vertically downward The lower end of bar is provided with the refrigeration cover of upside down funnel shape structure, is adhesively fixed on the refrigeration cover inwall and is provided with heat insulation inner wall, The external upper of the base is fixedly installed ring seat, is provided with rotating disk at the center of the ring seat and on base, institute State and crystallization bottle is provided with rotating disk, and the cover that freezes, crystallization bottle and rotating disk axis overlap, ring-type is empty between the ring seat and rotating disk In be provided with thermal insulating seat, the surface of the heat insulation inner wall and thermal insulating seat, which is rabbeted, evaporation tube, and the inside of the base is fixed It is provided with refrigeration system, centrifugation motor and hydraulic pump.
As a kind of preferred embodiment of the present utility model, the bottom integration of the crystallization bottle is fixedly installed block set With multiple inserting columns vertically downward, and inserting column is distributed on inside block set, and the crystallization bottle is socketed on rotating disk by block set, And the upper surface of rotating disk corresponds to the position of inserting column and is provided with spliced eye.
As a kind of preferred embodiment of the present utility model, the inner surface of the heat insulation inner wall correspondingly crystallizes the bottleneck of bottle Place position is fixedly installed firm bearing, and the firm bearing is socketed in the bottleneck of crystallization bottle, and the inner ring face of firm bearing It is provided with rubber buffer packing ring.
As a kind of preferred embodiment of the present utility model, the inwall lower end of the refrigeration cover and positioned at heat insulation inner wall Lower section is provided with lasso, and the refrigeration cover is socketed in ring seat outer wall by lasso, and is set between lasso and ring seat contact surface There is sealing gasket.
As a kind of preferred embodiment of the present utility model, the evaporation tube connects with refrigeration system, the centrifugation electricity The output shaft of machine connects the lower end of rotating disk by deceleration device, and the raise-lower hydraulic bar connects hydraulic pump by hydraulic tube.
The beneficial effect that the utility model is reached is:Utilized while being cooled to concentrate and centrifuge motor driven Crystallize bottle high-speed rotation, to crystal carry out centrifugal treating, so accelerate crystalline rate and less crystal fine grain from The lower separative efficiency assembled, be easy to improve follow-up separation process of heart effect, this kind of crystallization apparatus crystalline rate is high, more without carrying out Secondary crystallization, it is time saving and energy saving, increase processing safety.
Brief description of the drawings
Accompanying drawing is used for providing further understanding to of the present utility model, and a part for constitution instruction, with this practicality New embodiment is used to explain the utility model together, does not form to limitation of the present utility model.In the accompanying drawings:
Fig. 1 is a kind of general assembly cross section structure schematic diagram of cumyl peroxide crystallization apparatus;
Fig. 2 is schematic enlarged-scale view at a kind of A of cumyl peroxide crystallization apparatus;
Fig. 3 is schematic enlarged-scale view at a kind of B of cumyl peroxide crystallization apparatus;
Fig. 4 is schematic enlarged-scale view at a kind of C of cumyl peroxide crystallization apparatus;
Fig. 5 is a kind of turntable structure top view of cumyl peroxide crystallization apparatus.
In figure:1- bases;2- gate stands;3- raise-lower hydraulic bars;4- refrigeration covers;5- crystallizes bottle;6- heat insulation inner walls;7- systems Cooling system;8- centrifuges motor;9- hydraulic pumps;10- thermal insulating seats;11- evaporation tubes;12- consolidates bearing;13- block sets;14- grafting Post;15- rotating disks;16- lassos;17- ring seats;18- spliced eyes.
Embodiment
Preferred embodiment of the present utility model is illustrated below in conjunction with accompanying drawing, it will be appreciated that described herein excellent Select embodiment to be merely to illustrate and explain the utility model, be not used to limit the utility model.
Embodiment 1
As Figure 1-5, a kind of cumyl peroxide crystallization apparatus, including base 1 and be fixedly mounted on outside base 1 The gate stand 2 of upper surface, the crossbeam middle part of gate stand 2 are fixedly installed raise-lower hydraulic bar 3, raise-lower hydraulic bar vertically downward 3 lower end is provided with the refrigeration cover 4 of upside down funnel shape structure, is adhesively fixed on refrigeration 4 inwalls of cover and is provided with heat insulation inner wall 6, bottom The external upper of seat 1 is fixedly installed ring seat 17, and rotating disk 15, rotating disk are provided with the center of ring seat 17 and on base 1 Crystallization bottle 5 is provided with 15, and the cover 4 that freezes, crystallization bottle 5 and the axis of rotating disk 15 overlap, ring-type between ring seat 17 and rotating disk 15 It is provided with thermal insulating seat 10 in space, the surface of heat insulation inner wall 6 and thermal insulating seat 10, which is rabbeted, evaporation tube 11, and the inside of base 1 is consolidated Surely refrigeration system 7, centrifugation motor 8 and hydraulic pump 9, heat insulation inner wall 6 and thermal insulating seat 10 is provided with to be made of insulation material, Refrigeration system is using the common refrigeration plant in market.
In the present embodiment, the bottom integration of crystallization bottle 5 is fixedly installed block set 13 and multiple inserting columns vertically downward 14, and inserting column 14 is distributed on inside block set 13, crystallization bottle 5 is socketed on rotating disk 15 by block set 13, and the upper table of rotating disk 15 The position that face corresponds to inserting column 14 is provided with spliced eye 18, and the bottleneck position that the inner surface of heat insulation inner wall 6 correspondingly crystallizes bottle 5 is consolidated Surely firm bearing 12 is provided with, firm bearing 12 is socketed in the bottleneck of crystallization bottle 5, and the inner ring face of firm bearing 12 is set There is rubber buffer packing ring, firm bearing 12 is used for keeping crystallization bottle 5 to keep stability, rubber buffer while high-speed rotation Circle prevents that crystallize bottle 5 is destroyed by external force, and refrigeration covers 4 inwall lower end and the lower section of heat insulation inner wall 6 is provided with lasso 16, Refrigeration cover 4 is socketed in the outer wall of ring seat 17 by lasso 16, and is provided with sealing gasket between lasso 16 and the contact surface of ring seat 17, covers The space sealing that circle 16 and ring seat 17 will be freezed between cover 4 and base 1, is easy to refrigerating thermal-insulation, evaporation tube 11 connects with refrigeration system 7 Logical, the output shaft for centrifuging motor 8 connects the lower end of rotating disk 15 by deceleration device, and raise-lower hydraulic bar 3 connects liquid by hydraulic tube Press pump 9.
Principle and advantage of the present utility model:This kind of cumyl peroxide crystallization apparatus, crystallization bottle 5 is passed through into its bottom Block set 13 be fastened on rotating disk 15, while inserting column 14 is plugged in spliced eye 18, and cumyl peroxide concentrate is noted Enter to crystallize inside bottle 5, and good seal, raise-lower hydraulic bar 3 will freeze 4 seal closures of cover on the outside of crystallization bottle 5, and form confined space, Refrigeration system 7 works to cool to crystallization bottle 5, and the energization work of centrifugation motor 8 drives rotating disk 15 to rotate, so as to drive crystallization bottle 5 high Speed rotates, and after certain time, centrifuges motor 8 and refrigeration system 7 is stopped, raise-lower hydraulic bar 3 drives refrigeration cover 4 to move up, and takes Lower crystallization bottle 5 carries out subsequent processing processing, and this kind of cumyl peroxide crystallization apparatus concentrates to cumyl peroxide Using the drive crystallization high-speed rotation of bottle 5 of motor 8 is centrifuged while liquid is cooled, centrifugal treating is carried out to crystal, so added Fast crystalline rate and less crystal fine grain is assembled under the action of the centrifugal, it is easy to improve crystalline rate and changes and later separation work The separative efficiency of skill, it is time saving and energy saving without repeatedly being crystallized, increase processing safety.
Finally it should be noted that:Preferred embodiment of the present utility model is the foregoing is only, is not limited to this Utility model, although the utility model is described in detail with reference to the foregoing embodiments, for those skilled in the art For, it can still modify to the technical scheme described in foregoing embodiments, or to which part technical characteristic Carry out equivalent substitution.All any modification, equivalent substitution and improvements within the spirit and principles of the utility model, made etc., It should be included within the scope of protection of the utility model.

Claims (5)

1. a kind of cumyl peroxide crystallization apparatus, including base (1) and the door for being fixedly mounted on base (1) external upper Type stand (2), it is characterised in that:Raise-lower hydraulic bar is fixedly installed vertically downward in the middle part of the crossbeam of the gate stand (2) (3), the lower end of the raise-lower hydraulic bar (3) is provided with the refrigeration cover (4) of upside down funnel shape structure, described refrigeration cover (4) inwall On be adhesively fixed and be provided with heat insulation inner wall (6), the external upper of the base (1) is fixedly installed ring seat (17), the ring Rotating disk (15) is provided with the center of seat (17) and on base (1), crystallization bottle (5) is provided with the rotating disk (15), and Refrigeration cover (4), crystallization bottle (5) and rotating disk (15) axis overlap, between the ring seat (17) and rotating disk (15) in annulus It is provided with thermal insulating seat (10), the surface of the heat insulation inner wall (6) and thermal insulating seat (10), which is rabbeted, evaporation tube (11), the base (1) inside is fixedly installed refrigeration system (7), centrifugation motor (8) and hydraulic pump (9).
2. cumyl peroxide crystallization apparatus as claimed in claim 1, it is characterised in that:The bottom of the crystallization bottle (5) Integration is fixedly installed block set (13) and multiple inserting columns (14) vertically downward, and inserting column (14) is distributed on block set (13) Inside, the crystallization bottle (5) is socketed on rotating disk (15) by block set (13), and the upper surface of rotating disk (15) corresponds to inserting column (14) position is provided with spliced eye (18).
3. cumyl peroxide crystallization apparatus as claimed in claim 1, it is characterised in that:The heat insulation inner wall (6) it is interior The bottleneck position that surface correspondingly crystallizes bottle (5) is fixedly installed firm bearing (12), and the firm bearing (12) is socketed in knot The bottleneck of brilliant bottle (5), and the inner ring face of firm bearing (12) is provided with rubber buffer packing ring.
4. cumyl peroxide crystallization apparatus as claimed in claim 1, it is characterised in that:The inwall of the refrigeration cover (4) Lower end and lasso (16) is provided with below the heat insulation inner wall (6), the refrigeration cover (4) is socketed in ring seat by lasso (16) (17) outer wall, and it is provided with sealing gasket between lasso (16) and ring seat (17) contact surface.
5. cumyl peroxide crystallization apparatus as claimed in claim 1, it is characterised in that:The evaporation tube (11) and refrigeration System (7) connects, and the output shaft of the centrifugation motor (8) connects the lower end of rotating disk (15), the lifting liquid by deceleration device Depression bar (3) connects hydraulic pump (9) by hydraulic tube.
CN201720602597.6U 2017-05-26 2017-05-26 A kind of cumyl peroxide crystallization apparatus Expired - Fee Related CN206746032U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720602597.6U CN206746032U (en) 2017-05-26 2017-05-26 A kind of cumyl peroxide crystallization apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720602597.6U CN206746032U (en) 2017-05-26 2017-05-26 A kind of cumyl peroxide crystallization apparatus

Publications (1)

Publication Number Publication Date
CN206746032U true CN206746032U (en) 2017-12-15

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720602597.6U Expired - Fee Related CN206746032U (en) 2017-05-26 2017-05-26 A kind of cumyl peroxide crystallization apparatus

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110052075A (en) * 2019-06-05 2019-07-26 太仓塑料助剂厂有限公司 The separation method and system of cumyl peroxide

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110052075A (en) * 2019-06-05 2019-07-26 太仓塑料助剂厂有限公司 The separation method and system of cumyl peroxide

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171215

Termination date: 20200526