CN206736052U - A kind of integrated treatment reactor of sludge wet oxidation - Google Patents

A kind of integrated treatment reactor of sludge wet oxidation Download PDF

Info

Publication number
CN206736052U
CN206736052U CN201720451939.9U CN201720451939U CN206736052U CN 206736052 U CN206736052 U CN 206736052U CN 201720451939 U CN201720451939 U CN 201720451939U CN 206736052 U CN206736052 U CN 206736052U
Authority
CN
China
Prior art keywords
sludge
reactor
gas
zoneofoxidation
guide shell
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201720451939.9U
Other languages
Chinese (zh)
Inventor
杨欢
陈阳
覃小刚
房慧
文路
王焕
孙登科
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dongfang Boiler Group Co Ltd
Original Assignee
Dongfang Boiler Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dongfang Boiler Group Co Ltd filed Critical Dongfang Boiler Group Co Ltd
Priority to CN201720451939.9U priority Critical patent/CN206736052U/en
Application granted granted Critical
Publication of CN206736052U publication Critical patent/CN206736052U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Treatment Of Sludge (AREA)

Abstract

The utility model discloses the integrated treatment reactor of sludge wet oxidation, reactor includes pyrohydrolysis area and zoneofoxidation and the outside bag of reactor is provided with heat-preserving heating jacket, and the bottom that agitator and pyrohydrolysis area are provided with pyrohydrolysis area is provided with slag-drip opening;Guide shell is set in zoneofoxidation, and short transverse of the guide shell along zoneofoxidation is set and the top of guide shell has extension mouth;It is provided with the side wall of zoneofoxidation at the top of sludge import, product exit and gas access and zoneofoxidation and is provided with gas vent, sludge import is opened in the lower section of the extension mouth of guide shell, gas access is opened in the lower section of sludge import and positioned at the bottom of zoneofoxidation, product exit is opened in the top of the extension mouth of guide shell, gas access and the first gas distributor being arranged between guide shell and the side wall of zoneofoxidation connect, and sludge entrance is provided with sludge disperser.

Description

A kind of integrated treatment reactor of sludge wet oxidation
Technical field
The technical field of Treatment of Sludge is the utility model is related to, more particularly, is related to the one of a kind of sludge wet oxidation Body treatment reactor.
Background technology
Sludge wet oxidation is the another Treatment of Sludge mode after burning, landfill, anaerobic fermentation, aerobic compost, is utilized Gaseous oxidant under high temperature, high pressure in sludge organic matter carry out " wet combustion " with reach sludge reduction, it is innoxious, Stabilized purpose.
Existing Wet Oxidation Process all contains two critical process steps substantially:1) preprocessing process of sludge, city (viscosity of aqueous about 80%) is big, low without mobility, mass-and heat-transfer efficiency, directly handles for the particularly municipal dewatered sludge of political affairs sludge There is very big difficulty, all first sludge can be pre-processed typically before wet oxidation, change the character of dewatered sludge, reduce and glue Degree, increase mobility, this process is the pyrohydrolysis of sludge by the way of;2) oxidation of pyrohydrolysis sludge, it is dirty in pyrohydrolysis Sludge is further processed at high temperature under high pressure using oxygen/air on the basis of mud.
In the prior art, Chinese patent literature CN104341082A is entered using high-temperature steam in hydrolytic reaction pot to sludge Input high-temperature oxydation tower after row pyrohydrolysis to be aoxidized, Chinese patent literature CN102786190A is being pre-processed using the liquid of heat Input oxidation reactor is further handled after pyrohydrolysis is carried out to primary sludge in device.But at such sludge wet oxidation Two main devices have been comprised at least in reason flow:Pyrohydrolysis reactor (or preatreating reactors) and wet oxidation reactor, Reaction system is numerous and diverse, floor space is high, economy is low.
Existing to be related to most of reactor in sludge wet oxidation patent and use semi-batch tank reactor, such as China is specially Sharp document CN201981109U, Chinese patent literature CN105776794A.Sludge enters reactor from entrance, at high temperature under high pressure Maintain sludge outlet discharge from below after certain residence time.But such reactor mass-transfer efficiency is low, stirring is uneven very Hot-spot is easily caused, the mode of operation of semi-batch is also more troublesome.Meanwhile the wet oxidation process of sludge is a heat release Reaction, can produce the gaseous product of HTHP after oxidation, existing sludge wet-type oxidation technology is directed to this portion gas all only The heat in waste gas is make use of, but is not in fact in time for the oxygen of reaction in the gas of reactor discharge containing some still Gas.
The content of the invention
In order to solve technical problem present in prior art, the purpose of this utility model is to provide one kind and has merged sludge Pyrohydrolysis and oxidizing process and ensure abundant mass transfer and reaction sludge wet oxidation integrated treatment reactor.
The utility model provides a kind of integrated treatment reactor of sludge wet oxidation, and the reactor includes being located at The outside bag of the pyrohydrolysis area of reactor lower part and the zoneofoxidation positioned at reactor middle and upper part and reactor is provided with Heat preservation Set, wherein,
The bottom that agitator and pyrohydrolysis area are provided with the pyrohydrolysis area is provided with slag-drip opening;
Guide shell is set in the zoneofoxidation, short transverse setting and guide shell of the guide shell along zoneofoxidation Top has extension mouth;Sludge import, product exit and gas access and zoneofoxidation are provided with the side wall of the zoneofoxidation Top is provided with gas vent, and the sludge import is opened in the lower section of the extension mouth of the guide shell, and the gas access is opened It is located at the lower section of sludge import and is opened in the extension mouth of the guide shell positioned at the bottom of zoneofoxidation, the product exit Top, wherein, the gas access and the first gas distributor being arranged between the guide shell and the side wall of zoneofoxidation connect Connect, the sludge entrance is provided with sludge disperser.
According to one embodiment of the integrated treatment reactor of the utility model sludge wet oxidation, the pyrohydrolysis area In agitator be magnetic stirrer, the rotary shaft of the magnetic stirrer is not directly connected to be driven with the output shaft of motor;Institute The quantity for stating slag-drip opening is at least one.
According to one embodiment of the integrated treatment reactor of the utility model sludge wet oxidation, the Heat preservation The heating medium of set is electricity, oily or steam, and when using oil or steam as heating medium, the Heat preservation, which is put, to be also set up There are medium inlet and media outlet.
According to one embodiment of the integrated treatment reactor of the utility model sludge wet oxidation, in reactor start-up Initial period reactor is heated using the heat-preserving heating jacket, after stable reaction stop heating, wherein, reactor On be additionally provided with temperature measuring unit and pressure measuring unit.
According to one embodiment of the integrated treatment reactor of the utility model sludge wet oxidation, the gas access The gaseous oxidant being passed through is oxygen and/or air, and the sludge that the sludge import is passed through is the dirt that water content is 80~90% Mud;Reaction temperature in the reactor is 150~350 DEG C, and pressure is 2~20MPa.
According to one embodiment of the integrated treatment reactor of the utility model sludge wet oxidation, the zoneofoxidation Top has the gas compartment, and reacted waste gas enters after the gas compartment by gas vent outflow reactor, wherein, one Portion is back in reactor after pressurizeing again, another part waste gas be used for preheat fresh sludge or gaseous oxidant or Discharged after directly carrying out vent gas treatment.
According to one embodiment of the integrated treatment reactor of the utility model sludge wet oxidation, the zoneofoxidation Circulating air entrance is additionally provided with side wall, the circulating air entrance is connected with by one by external gas circuit with the gas vent Waste gas is divided to be back in reactor, wherein, the circulating air entrance is opened in the lower section of sludge import and in the upper of gas access Side, the circulating air entrance and the second gas distributor being arranged between the guide shell and the side wall of zoneofoxidation connect.
Another aspect of the present utility model provides a kind of integral treatment method of sludge wet oxidation, using above-mentioned dirt The integrated treatment reactor of mud wet oxidation carries out the integrated treatment of sludge wet-type oxidation degradation, the dirt after being handled Mud.
The utility model incorporates sludge pyrohydrolysis and two processes of sludge wet oxidation in sludge wet oxidation process, Realize that sludge wet oxidation is handled in same reactor, be effectively improved the economy of sludge wet oxidation equipment, design It is reasonable and workable;The utility model reduces the limit value to feed sludge water content, from the dewatered sludge without mobility (80% water content), which arrives, has the sludge (90% water content) of mobility applicable, is directly fed without pre-processing;Instead Answer and unreacted oxygen is included in the waste gas of device out, waste gas is reentered in reactor by extraneous gas circulation, improved The residence time of gas in the reactor, sludge degradation efficiency is improved, also improve the utilization rate of oxygen.
Brief description of the drawings
Fig. 1 shows the integrated treatment reactor of the sludge wet oxidation according to the utility model exemplary embodiment Structural representation.
Fig. 2 shows the structural representation of sludge disperser.
Description of reference numerals:
1- reactors, 2- pyrohydrolysis area, 3- zoneofoxidations, 4- agitators, 5- slag-drip openings, 6- guide shells, 7- extension mouths, 8- are dirty Mud import, 9- product exits, 10- gas accesses, 11- gas vents, 12- circulating air entrance, 13- gas circulators, 14- first Gas distributor, 15- second gas distributors.
Embodiment
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive Feature and/or step beyond, can combine in any way.
Any feature disclosed in this specification, unless specifically stated otherwise, can be equivalent by other or with similar purpose Alternative features are replaced.I.e., unless specifically stated otherwise, each feature is an example in a series of equivalent or similar characteristics .
The utility model provides a kind of reactor for being integrated with sludge hot hydrolysis-oxidation process, and reactor is divided into hot water Xie Qu and zoneofoxidation, zoneofoxidation using having compared with circular response form in the up-flow of high mass transfer efficiency, react heel row in form The waste gas gone out by be again introduced into reactor improve oxygen residence time, taken into account economy, reaction efficiency and The many aspects such as treatment effect.
The structure to the integrated treatment reactor of the utility model sludge wet oxidation and principle are carried out detailed below Explanation.
Fig. 1 shows the integrated treatment reactor of the sludge wet oxidation according to the utility model exemplary embodiment Structural representation.
It is as shown in figure 1, anti-according to exemplary embodiment of the present utility model, the integrated treatment of the sludge wet oxidation Device is answered to include positioned at the outer of the pyrohydrolysis area 2 of the bottom of reactor 1 and zoneofoxidation 3 positioned at the middle and upper part of reactor 1 and reactor 1 Portion's bag is provided with heat-preserving heating jacket (not shown).Wherein, the pyrohydrolysis area 2 of bottom is used for the pyrohydrolysis for realizing sludge, and zoneofoxidation 3 is used In the oxidative degradation for realizing pyrohydrolysis sludge, heat-preserving heating jacket then realizes the heating and insulation effect to reactor.
Specifically, agitator 4 is provided with pyrohydrolysis area 2 and the bottom in pyrohydrolysis area 2 is provided with slag-drip opening 5.Hot water Solution area 2 is located at the bottom of reactor, then when reactor works, sludge can directly sink to bottom and in high temperature after entering reactor Hydrolyzed in the pyrohydrolysis area 2 of high pressure, the sludge after hydrolysis turns into the slurry condition that particle diameter is small, mobility is high, thus, it is possible to upper Zoneofoxidation under the drive of portion's current into top carries out oxidative degradation.
Preferably, the agitator 4 in pyrohydrolysis area 2 uses magnetic stirrer, and the rotary shaft of magnetic stirrer not with The output shaft of motor is directly connected to be driven, and solves the problems, such as mechanical agitator and reactor bearing sealing failure and leakage, agitator 4 Lasting stirring action sludge can be made uniformly to heat, avoid the situation of hot-spot.The slag-drip opening energy of the bottom of pyrohydrolysis area 2 Enough periodically discharge proportion it is bigger do not allow solid, such as bulk sandstone, the quantity of slag-drip opening 5 is preferably at least one.
The heat-preserving heating jacket for being heated to reactor is provided with outside reactor 1, the heating medium of heat-preserving heating jacket can With using electricity, oil or steam, when using oil or steam as heating medium when, Heat preservation put be additionally provided with medium inlet and Media outlet.And, it is only necessary to reactor 1 is heated using heat-preserving heating jacket in the initial period that reactor 1 starts, it is dirty Mud starts liberated heat after reacting and is enough the normal operation for maintaining whole reactor, can stop heating after stable reaction. For the ease of the temperature and pressure situation in detection reactor 1, temperature measuring unit and pressure measuring unit are additionally provided with (not on reactor 1 Show).
Also, guide shell 6 is provided with zoneofoxidation 3, short transverse of the guide shell 6 along zoneofoxidation 3 is set and water conservancy diversion The top of cylinder 6 has extension mouth 7;Sludge import 8, product exit 9 and gas access 10 and oxygen are provided with the side wall of zoneofoxidation 3 The top for changing area 3 is provided with gas vent 9, and sludge import 8 is opened in the lower section of the extension mouth 7 of guide shell 6, and gas access 10 is opened It is located at the lower section of sludge import 8 and is opened in the upper of the extension mouth 7 of guide shell 6 positioned at the bottom of zoneofoxidation 3, product exit 9 Side, gas access 10 and the first gas distributor 14 being arranged between the side wall of guide shell 6 and zoneofoxidation 3 connect, and sludge enters Sludge disperser is provided with mouth 8.Wherein, first gas distributor 14 is in fact that ring is located at outside guide shell 6 and can led Equably realize that gas sprays and is distributed, the gas vent court of first gas distributor 15 between the side wall of flow cartridge 6 and zoneofoxidation 3 Upper setting.Fig. 2 shows the structural representation of sludge disperser, as shown in Fig. 2 sludge disperser is AND DEWATERING FOR ORIFICE STRUCTURE form, greatly Block sludge enters reactor after sludge disperser is dispersed into fritter, is advantageous to effective progress of subsequent treatment.In addition, in order to The extraction of product is convenient for, product exit 9 is preferably provided in the opposite side of sludge import.
Wherein, the gaseous oxidant that gas access 10 is passed through is oxygen and/or air, preferably oxygen;Sludge import 8 is logical The sludge entered is the sludge that water content is 80~90%, and reactor of the present utility model reduces the limit to feed sludge water content System, it is applicable to the sludge (90% is aqueous) with mobility from the dewatered sludge (80% is aqueous) without mobility, without pre- Processing is directly fed;The mud that product exit 9 is used for after continuous extraction, the liquid level in maintenance reaction device;Gas goes out Mouth 11 is then used to discharge the waste gas after sludge reaction.Preferably, the reaction temperature in the utility model reactor 1 is 150~350 DEG C, pressure is 2~20MPa.
Zoneofoxidation 3 is actually up-flow inner circulation structure, and the gaseous oxidant (air/oxygen) after over pressurizeed passes through Gas access 10 and first gas distributor 14 enter zoneofoxidation 3, drive the pyrohydrolysis mud in bed to flow up, and form gas Liquid solid three-phase fluid.When three-phase fluid reach guide shell 6 extension mouth 7 height when, gas kept because the small buoyancy of density is big to Upper flowing enters in extension mouth 7 and inside guide shell 6 up to gas vent 11, liquid and sludge bulky grain turn over greatly stream because of density Guide shell 6 is flowed downward out, the exterior space reentered between guide shell 6 and zoneofoxidation side wall, is continued under the drive of air-flow Flow up, form the self-loopa process that a complete cycle cake maintains whole reaction system.Mud granule is in guide shell 6 Section does not circulate outside, adds residence time of the sludge in zoneofoxidation 3, the organic matter in sludge obtain fully degraded and everywhere Sludge after reason.It follows that the set location of above-mentioned each mouth of reactor is closely related and non-with overall structure and technique Often important, can it directly determine that can reaction be normally carried out and circulate and normally maintain.
After air and/or oxygen enter reactor 1 by gas access 10, transported upwards in reactor in a manner of bubbling Move and drive mud to be circulated in reactor 1.By controlling gas flow to form a large amount of minute bubbles, minute bubbles in zoneofoxidation 3 Specific surface area is larger, it is possible to increase the mass-transfer efficiency of gas-liquid-solid three-phase.Reacted waste gas (including unreacted air, oxygen, Vapor and the gas of reaction generation) leave reaction zone from ullage and discharge.Wherein, the top of zoneofoxidation 3 also has gas Body space, reacted waste gas enters after the gas compartment passes through the outflow reactor 1. of gas vent 11 again by foam removal
Preferably, in order to effectively utilize reacted waste gas, a part of waste gas is after the grade of gas circulator 13 is pressurizeed again It is recycled back in reactor 1, another part waste gas is used to preheat fresh sludge or gaseous oxidant or directly carries out tail gas Discharged after processing, improve the utilization rate of oxygen.
Accordingly, circulating air entrance 12 is additionally provided with the side wall of zoneofoxidation 3, circulating air entrance 12 passes through external gas circuit It is connected with gas vent 11 so that a part of waste gas is back in reactor 1, wherein, circulating air entrance 12 is opened in sludge import 8 lower section and in the top of gas access 10, circulating air entrance 12 and is arranged between the side wall of guide shell 6 and zoneofoxidation 3 Second gas distributor 15 connects.Similarly, second gas distributor 15 is in fact and ring is located at outside guide shell 6 and can Equably realize that gas sprays and divided between the side wall of guide shell 6 and zoneofoxidation 3 and in the top of first gas distributor 14 Cloth, the gas vent of second gas distributor 16 are set upward, improve the residence time of gas in the reactor, and further carry High sludge degradation efficiency and oxygen utilization rate.
The defects of for sludge wet oxidation processing equipment in the prior art, the utility model proposes a kind of highly integrated Reactor, merged the pyrohydrolysis and oxidizing process of sludge, practicality is higher;Also, reactor of the present utility model is actual On be circulation flow reactor in a kind of up-flow, sludge circulates in reactor ensure that its residence time, and reactor Interior bubble specific surface area is larger, and alternate contact is good and mass-transfer efficiency is high;In addition, the utility model by reacted waste gas circulation again It is secondary to be passed through in reactor, the residence time of gaseous oxidant in the reactor can be increased, improve the utilization rate of oxygen, economy On be greatly improved.To sum up, the utility model proposes rational solution for prior art, try hard in economy and Preferred plan is found on treatment effeciency, can be applied in the future in Practical Project.
When the integrated treatment reactor using above-mentioned sludge wet oxidation carries out the integration of sludge wet-type oxidation degradation During processing, it may comprise steps of:
A, first the gas oxidation for being forced into predetermined pressure is made by more than liquid level lifting control to the product exit in reactor Agent enters uniform bubbling in the zoneofoxidation of reactor by gas access and first gas distributor, while opens heat-preserving heating jacket Temperature in reactor is heated to predetermined temperature;
B, it is passed through after sludge is disperseed by the sludge disperser of sludge import in reactor, sludge sinks to reactor lower part Pyrohydrolysis area and in the presence of agitator mix, hydrolyze become sludge slurry;The sludge slurry the top in pyrohydrolysis area with Current enter zoneofoxidation and by circulating and the gaseous oxidant haptoreaction and releasing in the up-flow inside and outside guide shell Substantial amounts of reaction heat, stop heating after question response is stable;
C, the bulk sandstone of deposition is intermittently discharged from slag-drip opening, after recycling the reaction flowed out by gas vent Waste gas, the sludge after product exit extraction, until complete sludge wet-type oxidation degradation processing, wherein, sludge is taken out Output is highly controlled with the normal level of liquid being able to maintain that in reactor.
During reaction, it is back to after preferably a part of waste gas is pressurizeed again in reactor, by another part Waste gas is used to preheat fresh sludge or gaseous oxidant or discharged after directly carrying out vent gas treatment.
With reference to specific embodiment, the utility model is described in further detail.
Integrated treatment reactor shown in Fig. 1 is used for sludge oxidative degradation, needed liquid level first before reactor start-up It is promoted to more than product exit.Enter by air and/or oxygen pressing to 5MPa and from gas access and first gas distributor Uniform bubbling is carried out in the zoneofoxidation of reactor, drives current to be circulated in inside reactor when bubble moves upwards.
The start-up temperature of the heating mantle maintenance reaction device of reactor external insulation is at 250 DEG C.Heat medium can use electricity, Oil or steam, when using oil or steam, medium inlet and outlet are correspondingly set on muff.Reactor heating only needs Carried out within a period of time that device has just started, liberated heat is enough to maintain the normal of whole reactor after sludge starts reaction Operation.
The sludge that water content is 80~90% is disperseed to be passed through from the sludge disperser of sludge import, sludge sinks to bottom Pyrohydrolysis area simultaneously starts to mix in the presence of magnetic stirrer, hydrolyzed, and sludge character changes, by not having consolidating for mobility Body is changed into the slurry with certain fluidity, then enters zoneofoxidation and air and/or oxygen with current at the top in pyrohydrolysis area Gas haptoreaction simultaneously releases substantial amounts of reaction heat.Temperature measuring unit is set on reactor to monitor the temperature in reactor as 250 DEG C, Stop external heat after stable reaction, the reaction heat maintenance reaction released using reaction is carried out.
Reacted mud is extracted out from product exit, and extracted amount is to maintain normal level of liquid to be highly controlled.Mud with Gas flows up between guide shell and zoneofoxidation side wall, and when reaching expansion open height, heavier mud granule ploughs under water conservancy diversion Cylinder inside and from guide shell bottom outflow reenter circulation.Slurries gas content outside guide shell is high, density is low and to Upper flowing;Slurries gas content inside guide shell is low, density is high and moves downward, and maintains the self-loopa of whole reaction system Journey.Cyclic process adds residence time of the sludge in zoneofoxidation, and the organic matter in sludge obtains fully degraded.Reacting Cheng Zhong, the bulk sandstone for being deposited on bottom is intermittently discharged from the slag-drip opening of reactor bottom.
Reacted waste gas (including unreacted air, oxygen, vapor and gas of reaction generation) flows upwards out liquid Face enters the gas compartment with reactor top, passes through gas vent outflow reactor after the demister of top.A part is useless Gas is forced into slightly above system pressure and returns to reactor, another part from recyclegas entrance again under gas circulation pumping action Waste gas enters downstream and can pass through heat exchanger and is used to preheat fresh sludge or oxidant, can also be directly over vent gas treatment dress Postpone discharge.
In summary, integrated treatment reactor of the present utility model incorporates sludge hot water in sludge wet oxidation process Solution and two processes of sludge wet oxidation, realize that sludge wet oxidation is handled in same reactor, be effectively improved dirt The economy of mud wet oxidation equipment, it is reasonable in design and workable;The utility model is reduced to feed sludge water content Limit value, from the dewatered sludge (80% water content) without mobility to mobility sludge (90% water content) It is applicable, is directly fed without pre-processing;Unreacted oxygen is included in the waste gas that reactor comes out, waste gas passes through extraneous gas Circulation is reentered in reactor, is improved the residence time of gas in the reactor, is improved sludge degradation efficiency, also improve The utilization rate of oxygen.
The utility model is not limited to foregoing embodiment.The utility model expands to any in this specification The new feature of middle disclosure or any new combination, and disclose any new method or process the step of or any new group Close.

Claims (7)

1. a kind of integrated treatment reactor of sludge wet oxidation, it is characterised in that the reactor includes being located at reactor The outside bag of the pyrohydrolysis area of bottom and the zoneofoxidation positioned at reactor middle and upper part and reactor is provided with heat-preserving heating jacket, its In,
The bottom that agitator and pyrohydrolysis area are provided with the pyrohydrolysis area is provided with slag-drip opening;
Guide shell is set in the zoneofoxidation, and short transverse of the guide shell along zoneofoxidation is set and the top of guide shell With extension mouth;Sludge import, product exit and gas access and the top of zoneofoxidation are provided with the side wall of the zoneofoxidation Gas vent is provided with, the sludge import is opened in the lower section of the extension mouth of the guide shell, and the gas access is opened in The lower section of sludge import and the bottom for being located at zoneofoxidation, the product exit are opened in the upper of the extension mouth of the guide shell Side, wherein, the gas access and the first gas distributor being arranged between the guide shell and the side wall of zoneofoxidation connect, The sludge entrance is provided with sludge disperser.
2. the integrated treatment reactor of sludge wet oxidation according to claim 1, it is characterised in that the pyrohydrolysis area In agitator be magnetic stirrer, the rotary shaft of the magnetic stirrer is not directly connected to be driven with the output shaft of motor;Institute The quantity for stating slag-drip opening is at least one.
3. the integrated treatment reactor of sludge wet oxidation according to claim 1, it is characterised in that the Heat preservation The heating medium of set is electricity, oily or steam, and when using oil or steam as heating medium, the Heat preservation, which is put, to be also set up There are medium inlet and media outlet.
4. the integrated treatment reactor of sludge wet oxidation according to claim 1, it is characterised in that in reactor start-up Initial period reactor is heated using the heat-preserving heating jacket, after stable reaction stop heating, wherein, reactor On be additionally provided with temperature measuring unit and pressure measuring unit.
5. the integrated treatment reactor of sludge wet oxidation according to claim 1, it is characterised in that the gas access The gaseous oxidant being passed through is oxygen and/or air, and the sludge that the sludge import is passed through is the dirt that water content is 80~90% Mud;Reaction temperature in the reactor is 150~350 DEG C, and pressure is 2~20MPa.
6. the integrated treatment reactor of sludge wet oxidation according to claim 1, it is characterised in that the zoneofoxidation Top has the gas compartment, and reacted waste gas enters after the gas compartment by gas vent outflow reactor, wherein, one Portion is back in reactor after pressurizeing again, another part waste gas be used for preheat fresh sludge or gaseous oxidant or Discharged after directly carrying out vent gas treatment.
7. the integrated treatment reactor of sludge wet oxidation according to claim 6, it is characterised in that the zoneofoxidation Circulating air entrance is additionally provided with side wall, the circulating air entrance is connected with by one by external gas circuit with the gas vent Waste gas is divided to be back in reactor, wherein, the circulating air entrance is opened in the lower section of sludge import and in the upper of gas access Side, the circulating air entrance and the second gas distributor being arranged between the guide shell and the side wall of zoneofoxidation connect.
CN201720451939.9U 2017-04-27 2017-04-27 A kind of integrated treatment reactor of sludge wet oxidation Active CN206736052U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720451939.9U CN206736052U (en) 2017-04-27 2017-04-27 A kind of integrated treatment reactor of sludge wet oxidation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720451939.9U CN206736052U (en) 2017-04-27 2017-04-27 A kind of integrated treatment reactor of sludge wet oxidation

Publications (1)

Publication Number Publication Date
CN206736052U true CN206736052U (en) 2017-12-12

Family

ID=60562179

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720451939.9U Active CN206736052U (en) 2017-04-27 2017-04-27 A kind of integrated treatment reactor of sludge wet oxidation

Country Status (1)

Country Link
CN (1) CN206736052U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106904806A (en) * 2017-04-27 2017-06-30 东方电气集团东方锅炉股份有限公司 The integrated treatment reactor and processing method of a kind of sludge wet oxidation
CN110510839A (en) * 2018-05-21 2019-11-29 中国石油化工股份有限公司 Remaining biochemical sludge decrement treatment system and processing method
CN111468064A (en) * 2019-01-24 2020-07-31 中国石化工程建设有限公司 Reactor for preparing alkyl peroxide and application thereof
CN111492042A (en) * 2017-12-21 2020-08-04 C-绿色科技公司 Comprising hydrothermal carbonising of sludge recycled from the wet oxidation section

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106904806A (en) * 2017-04-27 2017-06-30 东方电气集团东方锅炉股份有限公司 The integrated treatment reactor and processing method of a kind of sludge wet oxidation
CN111492042A (en) * 2017-12-21 2020-08-04 C-绿色科技公司 Comprising hydrothermal carbonising of sludge recycled from the wet oxidation section
CN111492042B (en) * 2017-12-21 2022-04-15 C-绿色科技公司 Comprising hydrothermal carbonising of sludge recycled from the wet oxidation section
CN110510839A (en) * 2018-05-21 2019-11-29 中国石油化工股份有限公司 Remaining biochemical sludge decrement treatment system and processing method
CN110510839B (en) * 2018-05-21 2021-08-06 中国石油化工股份有限公司 Excess biochemical sludge reduction treatment system and treatment method
CN111468064A (en) * 2019-01-24 2020-07-31 中国石化工程建设有限公司 Reactor for preparing alkyl peroxide and application thereof

Similar Documents

Publication Publication Date Title
CN206736052U (en) A kind of integrated treatment reactor of sludge wet oxidation
CN106904806A (en) The integrated treatment reactor and processing method of a kind of sludge wet oxidation
CN105085338B (en) The production method and device of DMDS
CN104211018A (en) Method and device for recovering high-purity sulfur from sulfur foam
CN106315885A (en) System and method for simultaneously performing circulation utilization on sewage, sludge and domestic garbage
CN105561893B (en) A kind of grease collar oxidation reaction apparatus
CN206279063U (en) Oil-bearing sludge treatment equipment
CN205270320U (en) Kitchen garbage total matter deoiling system
CN105907481B (en) Alternating is used in series the reaction unit of high pressure vapor methanol production biodiesel
CN101792447A (en) Process and device for preparing urotropine by using gas phase method
JPH0438476B2 (en)
CN109945711A (en) A kind of exothermic method and apparatus of chemical heat accumulation-
CN105692951B (en) The waste water iron-carbon reduction processing method and its device that a kind of iron cement recycles
CN214781454U (en) Sludge treatment system
CN205061839U (en) Mud deoiling system
CN107473440A (en) A kind of device for improving ozone utilization rate in multistage ozone air-float technique
CN206652499U (en) A kind of self-suction mixing reactor
CN209507875U (en) A kind of ammonia nitrogen wastewater treatment device
CN206368160U (en) A kind of material heating of biogas slurry anaerobic reactor and outer circulation mixing arrangement
CN207727066U (en) A kind of organic waste materials fermentation drying system
CN109749853A (en) A kind of device by soap stock continuous production acidification oil and by-product sodium sulfate crystal
CN207227237U (en) A kind of high temeperature chemistry anaerobic system
CN218359150U (en) Reaction device for preparing succinic anhydride through maleic anhydride hydrogenation
CN101869818B (en) Method and device for reducing internal pressure of terephthalic acid make-up tank
CN210560330U (en) Device for continuously producing acidified oil and byproduct sodium sulfate crystals from soapstock

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant