CN206730561U - A kind of chemical industry crystallizer - Google Patents

A kind of chemical industry crystallizer Download PDF

Info

Publication number
CN206730561U
CN206730561U CN201720602625.4U CN201720602625U CN206730561U CN 206730561 U CN206730561 U CN 206730561U CN 201720602625 U CN201720602625 U CN 201720602625U CN 206730561 U CN206730561 U CN 206730561U
Authority
CN
China
Prior art keywords
shell
shower nozzle
crystallizer
nozzle
fixedly connected
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720602625.4U
Other languages
Chinese (zh)
Inventor
张圣燕
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Binzhou University
Original Assignee
Binzhou University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Binzhou University filed Critical Binzhou University
Priority to CN201720602625.4U priority Critical patent/CN206730561U/en
Application granted granted Critical
Publication of CN206730561U publication Critical patent/CN206730561U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A kind of chemical industry crystallizer of the utility model, including toroidal nozzle, shower nozzle and stirrer paddle;The perpendicular floor is fixedly welded on the outside of shell, and is fixedly connected with X-type floor and cross rib plate between two groups of perpendicular floors;The crystallization outlet is fixedly connected on the bottom of shell, and indirect steam outlet is welded with the top of shell;Control valve is connected with the fresh water pipeline, and the end of fresh water pipeline is welded with toroidal nozzle;Multigroup shower nozzle has been fixedly connected with inside and outside the bottom of the toroidal nozzle;The drain cylinder is fixedly connected among the inner side of inner casing.The setting of the utility model thermal insulation board, avoid the temperature of shell too high, prevent internal heat to be lost in, the setting of the utility model floor, improve the intensity of crystallizer housing, the setting of the utility model toroidal nozzle and shower nozzle, be advantageous to clean inside crystallizer, preferably different product is crystallized.

Description

A kind of chemical industry crystallizer
Technical field
It the utility model is related to crystallizer, technical field of chemical, more particularly to a kind of chemical industry crystallizer.
Background technology
In chemical field, conventional crystallizer to carry out crystallization and purification to product.The operation principle of crystallizer is, in stream The product solution of body state is cooled down so that product solution is in hypersaturated state, so as to crystallize, then again by residue Solution discharge, so as to the high purity product after being crystallized.By the method for crystallization, can remove some distillating methods can not The impurity of removal.Such as when the boiling point of impurity and the close boiling point of product, can not just be made a return journey the removal of impurity by the method for distillation, Impurity can now be separated with product by the method for crystallization, deimpurity purpose is gone to realize.
The present inventor has found that existing chemical crystallization device can not be timely to crystallization after use terminates in use Cleaned inside device, easily mixed when being crystallized to other products, reduce the purity of product, steam is used in crystallization process The higher easily scald staff of outside wall temperature of crystallizer.
Then, inventor in view of this, adhere to the relevant industries for many years it is abundant design and develop and the experience of actual fabrication, Improvement is studied for existing structure and missing, there is provided a kind of novel chemical crystallizer, is had more more to reach The purpose of practical value.
The content of the invention
The purpose of this utility model is to provide a kind of chemical industry crystallizer, made with solve to propose in above-mentioned background technology Timely crystallizer inside can not be cleaned with after end, easily mix when being crystallized to other products, reduce product Purity, in crystallization process using steam crystallizer outside wall temperature it is higher easily scald staff the problem of.
The purpose and effect of the utility model chemical industry crystallizer, are reached by technological means in detail below:
A kind of chemical industry crystallizer, it is characterised in that:Described chemical industry is included with crystallizer:
Shell, perpendicular floor, X-type floor, cross rib plate, material inlet, steam inlet, crystallization outlet, indirect steam export, are clear Waterpipe, control valve, motor, deceleration device, thermal insulation board, inner casing, toroidal nozzle, shower nozzle, drain cylinder and stirrer paddle;
The perpendicular floor is fixedly welded on the outside of shell, and is fixedly connected with X-type floor and horizontal stroke between two groups of perpendicular floors Floor;The material inlet is separately mounted to the outside lower end of shell, and the lower end of material inlet is provided with steam inlet;
The crystallization outlet is fixedly connected on the bottom of shell, and indirect steam outlet is welded with the top of shell;It is described Control valve is connected with fresh water pipeline, and the end of fresh water pipeline is welded with toroidal nozzle;In the bottom of the toroidal nozzle Outer both sides have been fixedly connected with multigroup shower nozzle;
The motor is fixedly mounted on one end of deceleration device, and is connected between deceleration device and stirrer paddle by rotating shaft Connect;The drain cylinder is fixedly connected among the inner side of inner casing, and stirrer paddle is located at the inner side of drain cylinder.
Further, the shell, thermal insulation board and shell collectively constitute the shell structure of crystallizer, and thermal insulation board is located at shell Between inner casing.
Further, it is in 60 ° of angles between the shower nozzle and horizontal direction.
Further, the shower nozzle is using toroidal nozzle center to be circular arranged in a ring.
Further, the shower nozzle is collectively constituted by outer shower nozzle and interior shower nozzle, the outer shower nozzle downwardly inner casing, and interior Shower nozzle downwardly drain cylinder.
With existing structure in comparison, the utility model has the following advantages that:
1. the setting of the utility model thermal insulation board, there is good effect of heat insulation, avoid crystallizer shell during use Temperature it is too high, while can prevent inside heat loss.
2. the utility model erects the setting of floor, X-type floor and cross rib plate, the intensity of crystallizer housing is improved, is avoided Crystallizer casing rupture when crystallizer internal pressure is excessive.
3. the setting of the utility model toroidal nozzle and shower nozzle, be advantageous to after crystallization has ended carry out clearly crystallizer inside Wash, preferably to be crystallized to different product, avoid two kinds of product mixes, improve the purity of product.
Brief description of the drawings
Fig. 1 is the utility model structure diagram;
Fig. 2 is the utility model internal structure schematic diagram;
Fig. 3 is the utility model toroidal nozzle dimensional structure diagram;
Fig. 4 is the utility model annular Peng's pipe positive structure schematic.
In figure:1st, shell, 2, perpendicular floor, 3, X-type floor, 4, cross rib plate, 5, material inlet, 6, steam inlet, 7, crystallization Outlet, 8, indirect steam outlet, 9, fresh water pipeline, 10, control valve, 11, motor, 12, deceleration device, 13, thermal insulation board, 14, Inner casing, 15, toroidal nozzle, 16, shower nozzle, 17, drain cylinder, 18, stirrer paddle.
Embodiment
Below, embodiment of the present utility model is will be explained in, the example is shown in the accompanying drawings and the description below.Although will The utility model is described with reference to exemplary embodiment, it is to be understood that the description does not really want the utility model to be limited to this to show The embodiment of example property.On the contrary, the utility model will not only cover the exemplary embodiment, but also cover various replacements, Change, equivalent and other embodiment, it can be included in spirit of the present utility model and the model that appended claims are limited In enclosing.
Such as accompanying drawing 1 to accompanying drawing 4, a kind of chemical industry crystallizer, include:
Shell 1, perpendicular floor 2, X-type floor 3, cross rib plate 4, material inlet 5, steam inlet 6, crystallization outlet 7, indirect steam Outlet 8, fresh water pipeline 9, control valve 10, motor 11, deceleration device 12, thermal insulation board 13, inner casing 14, toroidal nozzle 15, shower nozzle 16th, drain cylinder 17 and stirrer paddle 18;
Perpendicular floor 2 is fixedly welded on the outside of shell 1, and is fixedly connected with X-type floor 3 and horizontal stroke between two groups of perpendicular floors 2 Floor 4;Material inlet 5 is separately mounted to the outside lower end of shell 1, and the lower end of material inlet 5 is provided with steam inlet 6;
Crystallization outlet 7 is fixedly connected on the bottom of shell 1, and the top of shell 1 is welded with indirect steam outlet;Water pipe Control valve 10 is connected with road 9, and the end of fresh water pipeline 9 is welded with toroidal nozzle 15;Inside and outside the bottom of toroidal nozzle 15 Both sides have been fixedly connected with multigroup shower nozzle;
Motor 11 is fixedly mounted on one end of deceleration device 12, and passes through rotating shaft between deceleration device 12 and stirrer paddle 18 It is connected;Drain cylinder 17 is fixedly connected among the inner side of inner casing 14, and stirrer paddle 18 is located at the inner side of drain cylinder 17.
Shell 1, thermal insulation board 13 and shell 14 collectively constitute the shell structure of crystallizer, and thermal insulation board 13 be located at shell 1 with it is interior Between shell 14, thermal insulation board 13 is synthesized by the composite of glass fiber material and high-fire resistance, has preferable heat resistance and resistance to Tide, pyroconductivity is low, and high temperature resistant is up to 300 degree, at high temperature with excellent bending strength;
It is in 60 ° of angles between shower nozzle 16 and horizontal direction;
Shower nozzle 16 is easy to clear water to be uniformly sprayed at by shower nozzle 16 using the center of toroidal nozzle 15 to be circular arranged in a ring The inner side of crystallizer;
Shower nozzle 16 is collectively constituted by outer shower nozzle and interior shower nozzle, outer shower nozzle downwardly inner casing 4, and interior shower nozzle is downwardly toward guide Fluid cylinder 17, it is easy to after crystallization has ended clean the inner side of crystallizer inner casing 4 and guide shell 17.
The operation principle of the present embodiment:
Hot saturation feed liquid is added to inside crystallizer by material inlet 5 first, and flows into guide shell bottom, is then passed through Controlling switch starts motor 11, and so as to drive stirrer paddle 18 slowly to be rotated by deceleration device 12, stirrer paddle 18 will Solution delivers to liquid level along drain cylinder 17, and is crystallized in the presence of steam, and crystal is in crystalliser feet by crystallizing outlet 7 Outflow, crystallizer is using end opening controlling valve door 10 so that the inside clear water of fresh water pipeline 9 is transported into toroidal nozzle 15 and led to Cross shower nozzle 16 to spray, so as to clean crystallizer inwall and the inner side of drain cylinder 17, preferably to enter different product Row crystallization, avoids two kinds of product mixes, improves the purity of product, and in practical application experiment, the design is relative to market ability Domain other products, the performance higher than its 90% or so.
It should be noted that the standardized element that uses of the utility model can commercially, shaped piece according to Specification and accompanying drawing record can carry out customized, and the specific connected mode of each part is using ripe in the prior art Bolt, rivet, the conventional meanses such as welding, machinery, part and equipment are using in the prior art, conventional model, inventor It will not be described in detail herein.
In summary, although the utility model is described in detail with reference to the foregoing embodiments, for this area For technical staff, it can still modify to the technical scheme described in foregoing embodiments, or to which part Technical characteristic carries out equivalent substitution, all within the spirit and principles of the utility model, any modification for being made, equivalent substitution, Improve etc., it should be included within the scope of protection of the utility model.

Claims (1)

  1. A kind of 1. chemical industry crystallizer, it is characterised in that:Described chemical industry is included with crystallizer:
    Shell, perpendicular floor, X-type floor, cross rib plate, material inlet, steam inlet, crystallization outlet, indirect steam outlet, water pipe Road, control valve, motor, deceleration device, thermal insulation board, inner casing, toroidal nozzle, shower nozzle, drain cylinder and stirrer paddle;
    The perpendicular floor is fixedly welded on the outside of shell, and is fixedly connected with X-type floor and cross rib plate between two groups of perpendicular floors; The material inlet is separately mounted to the outside lower end of shell, and the lower end of material inlet is provided with steam inlet;
    The crystallization outlet is fixedly connected on the bottom of shell, and indirect steam outlet is welded with the top of shell;The clear water Control valve is connected with pipeline, and the end of fresh water pipeline is welded with toroidal nozzle;Two inside and outside the bottom of the toroidal nozzle Side has been fixedly connected with multigroup shower nozzle;
    The motor is fixedly mounted on one end of deceleration device, and is connected between deceleration device and stirrer paddle by rotating shaft;
    The drain cylinder is fixedly connected among the inner side of inner casing, and stirrer paddle is located at the inner side of drain cylinder, the shell, every Hot plate collectively constitutes the shell structure of crystallizer with shell, and thermal insulation board is located between shell and inner casing, the shower nozzle and level side Be in 60 ° of angles between, the shower nozzle using toroidal nozzle center to be circular arranged in a ring, the shower nozzle by outer shower nozzle with it is interior Shower nozzle collectively constitutes, the outer shower nozzle downwardly inner casing, and interior shower nozzle downwardly drain cylinder.
CN201720602625.4U 2017-05-27 2017-05-27 A kind of chemical industry crystallizer Expired - Fee Related CN206730561U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720602625.4U CN206730561U (en) 2017-05-27 2017-05-27 A kind of chemical industry crystallizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720602625.4U CN206730561U (en) 2017-05-27 2017-05-27 A kind of chemical industry crystallizer

Publications (1)

Publication Number Publication Date
CN206730561U true CN206730561U (en) 2017-12-12

Family

ID=60568596

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720602625.4U Expired - Fee Related CN206730561U (en) 2017-05-27 2017-05-27 A kind of chemical industry crystallizer

Country Status (1)

Country Link
CN (1) CN206730561U (en)

Similar Documents

Publication Publication Date Title
CN104174260B (en) A kind of absorption column of gas and using method thereof
CN206730561U (en) A kind of chemical industry crystallizer
CN101333268B (en) Reactor for EPS
CN203315784U (en) Scraper crystallization separator
CN209575820U (en) A kind of high-efficiency and energy-saving type trehalose crystallization apparatus
CN107008029A (en) A kind of chemical industry crystallizer
CN206083330U (en) Reaction kettle for petrochemical engineering
CN107469576A (en) Industrial waste gas removes objectionable impurities device
CN109092238A (en) A kind of industrial chemicals production reaction unit with cooling effect
CN205850835U (en) A kind of reactor
CN205340185U (en) Continuous crystallization equipment of multistage high vacuum insulation flash distillation
CN208553201U (en) A kind of crystallizer for ion-exchange-resin process synthesis of bisphenol A
CN204768670U (en) Water -reducing agent reation kettle
CN209138632U (en) A kind of device for reactor cycles cooling
CN104771928B (en) A kind of crystallize still for preparing trimethyl acetone acid
CN207121549U (en) Diethyl toluene diamine produces pre-processing device
CN209155160U (en) A kind of rectifying column raw material separator
CN101538192A (en) Enyl phenol refining plant and method thereof
CN205413024U (en) Control by temperature change formula high efficiency reation kettle
CN205252603U (en) Edulcoration distillation plant
CN211026302U (en) Lifting device for polyester resin reaction kettle
CN207951442U (en) A kind of mixing plant producing ferric trichloride
CN210045654U (en) A crystallization rinsing spray set for preparing high-purity β -aminopropionic acid
CN209155170U (en) A kind of rapid crystallization equipment of potassium fluotitanate
CN209679548U (en) A kind of stirring-type crystallization kettle

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171212

Termination date: 20180527

CF01 Termination of patent right due to non-payment of annual fee