CN206660867U - A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser - Google Patents

A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser Download PDF

Info

Publication number
CN206660867U
CN206660867U CN201720119724.7U CN201720119724U CN206660867U CN 206660867 U CN206660867 U CN 206660867U CN 201720119724 U CN201720119724 U CN 201720119724U CN 206660867 U CN206660867 U CN 206660867U
Authority
CN
China
Prior art keywords
acid mist
condenser
acid
tube
type graphite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720119724.7U
Other languages
Chinese (zh)
Inventor
殷朋飞
刘中文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Hanxin Graphite Equipment Technology Co Ltd
Original Assignee
Qingdao Hanxin Graphite Equipment Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Hanxin Graphite Equipment Technology Co Ltd filed Critical Qingdao Hanxin Graphite Equipment Technology Co Ltd
Priority to CN201720119724.7U priority Critical patent/CN206660867U/en
Application granted granted Critical
Publication of CN206660867U publication Critical patent/CN206660867U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model provides a kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser, including with acid mist conveyance conduit, acid mist scrubbing tower, scrubbing tower spray pump, running water valve, ventilation blower.One big specification tube-type graphite acid mist condenser, acid mist condenser collecting tank, acid mist condensate liquid delivery pump are provided with acid mist conveyance conduit.Acid mist condenser is big specification tube-type graphite heat exchanger, by upper cover plate, upper cover, fixed tube sheet, housing, deflection plate, Graphtic heat exchanging pipe, floating tubesheet, low head, lower cover, gas access, gas vent, evacuation port, drain, cooling water inlet, coolant outlet are formed.The characteristics of the utility model is:Fine corrosion resistance, heat transfer coefficient is high, dilute acid recycle rate is high, service life length, not only realize the recycling to HCL gases, also reduce the water consumption of scrubbing tower simultaneously and reduce the treating capacity of acid-bearing wastewater, production cost is saved, and the load of acid mist purifying tower is greatly reduced, make the acid mist for being discharged into air that national standard be fully achieved.

Description

A kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser returns Receive purifier
Technical field
The utility model provides a kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser and returned Receive purifier.
Background technology
Cold-rolling pickling production line in China's has hundreds of at present, but in the sector, either continuous pickling, plug-type Pickling lines, its technique are all that acid solution first is heated into technological temperature to carry out recycle stream dynamic formula pickling by circulating pump again. During this, substantial amounts of HCL gases will evaporate with vapor from hydrochloric acid so as to produce substantial amounts of acid mist, hydrochloric acid Loss and the purified treatment of acid mist also just turn into two hang-ups of puzzlement pickling manufacturer.
Present most of manufacturers take carries out washing absorption using the mode of acid mist scrubbing tower to acid mist, after absorption Acid solution is directly discharged to water treatment station, had so not only wasted acid solution and water resource simultaneously but also needs processing is largely useless containing diluted acid Water, the production cost of Shi Ge pickling producer increase.It was verified that acid mist only by being difficult after acid mist scrubbing tower progress washing absorption Reach discharging standards, very big pollution is caused to environment.According to practical application experience in recent years, we have devised one Increase a set of tube-type graphite acid mist condenser before being enclosed on the acid mist reclaiming clean device that conventional manufacturer uses.
The content of the invention
The purpose of this utility model is to provide a kind of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser Acid mist reclaiming clean device, it is related to a kind of big specification tube-type graphite acid mist condenser in conventional acid mist purifying retracting device In application.
The purpose of this utility model is realized by following technical proposals.
A kind of cold-rolling pickling line acid mist recovery provided with big specification tube-type graphite acid mist condenser of the present utility model is net Makeup is put, including tube-type graphite condenser, the acid mist scrubbing tower being connected with acid mist conveyance conduit, with this acid mist scrubbing tower In, the scrubbing tower spray pump that is connected of top, be connected with the bottom of this acid mist scrubbing tower and tube-type graphite condenser dilute Hydrochloric acid tank, running water valve, with the ventilation blower and emptying pipeline being connected at the top of this acid mist scrubbing tower, it is characterised in that Described acid mist conveyance conduit is provided with a tube-type graphite acid mist condenser, and this tube-type graphite acid mist condenser bottom is set There is gas-liquid separator, the acid mist condensate outlet of this gas-liquid separator is connected with a watery hydrochloric acid storage tank, this watery hydrochloric acid storage tank Bottom sides be connected with an acid mist condensate liquid delivery pump, this acid mist condensate liquid delivery pump is connected by pipeline with complex acid tank Connect, the gas vent of this gas-liquid separator is connected with the bottom of described acid mist scrubbing tower.
Described big specification tube-type graphite acid mist condenser is Tube Heat Exchanger, by a housing, is located at this Some heat exchanger tubes, deflection plates in housing, it is located at the fixed tube sheet of this shell one end, the envelope being connected with this fixed tube sheet Head, the gas access being connected with this end socket, it is located at the floating tubesheet of this housing other end, the envelope being connected with this floating tubesheet Head, the gas vent being connected with this end socket, the drain at described fixed tube sheet on the upside of described housing is located at, if Cooling water inlet on the downside of described housing at described fixed tube sheet, it is located on the upside of described housing close to described Coolant outlet at floating tubesheet, it is located at the discharging hole on the downside of described housing at described floating tubesheet and is formed.
Housing made of all carbon steel materials of described housing.
Some described heat exchanger tubes are some heat exchanger tubes made of pure graphite material.
Described fixed tube sheet is fixed tube sheet made of pure graphite material.
Described floating tubesheet is floating tubesheet made of pure graphite material.
Described two end sockets being connected with fixed tube sheet, floating tubesheet are two envelopes made of pure graphite material Head.
The described end socket being connected with floating tubesheet is gas-liquid separator.
Described scrubbing tower spray pump is provided with two scrubbing tower spray pumps in parallel for switching switch, this two scrubbing towers Spray pump is fluoroplastics centrifugal pump.
Described ventilation blower is two corrosion-resistant air-introduced machines in parallel provided with switching switch.
A kind of cold-rolling pickling line acid mist recovery provided with big specification tube-type graphite acid mist condenser of the present utility model is net Disguising the course of work put is:Caused acid mist is extracted out from the mist exhausting port on descaling bath cell body in acid cleaning process, through conveyance conduit Into acid mist reclaiming clean device, reclaiming clean device is made up of condenser and scrubbing tower, and the acid mist with certain temperature is through cold Droplet is formed after condenser condensation, then the gas-liquid separator by condenser carries out gas-liquid separation and is collected into acid solution dilute In hydrochloric acid tank, the acid strength that gets off being collected 16% or so, can directly carry out pickling, most acid mist has been during this Get off to be formed condensation acid through being collected, remaining fraction acid mist carries out washing absorption by scrubbing tower again after condensed recovery. Scrubbing tower is the absorption pattern using two layers of filler and the vaporific comprehensive spray of two sections of umbrella-type, will be circulated by scrubbing tower circulating pump Water delivers to shower and acid mist is absorbed, and after recirculated water reaches finite concentration in scrubbing tower, watery hydrochloric acid is delivered to by pipeline Storage tank, then new recirculated water is supplemented into tower.Gas after scrubbing tower absorbs extracts that to deliver to cigarette chimney straight out through acid fog blower fan Connect and be emitted into air.
The utility model has the advantages that:Due to acid mist be in process of production hydrochloric acid through being heated at high temperature and circulating when produce It is raw, so the characteristics of using HCL gases and vapor cryogenic condensation, first make most acid mist cold before scrubbing tower is entered Congeal into liquid and carry out gas-liquid separation, acid solution is collected, then the scrubbed tower washing absorption of remaining fraction acid mist is most After be discharged into air.The present apparatus not only realizes the recovery to HCL gases, serves the effect of energy efficiency, and drops significantly The low load of acid mist scrubbing tower, makes to be discharged into the acid mist in air and national standard is fully achieved, environment protecting is obvious.
It is of the present utility model it is a kind of provided with big specification tube-type graphite acid mist condenser be graphite tubular heat exchanger, tube sheet, Heat exchanger tube and end socket are made up of pure graphite material, and the part such as housing is that carbon steel material is made through internal and external anti-corrosive.
Major advantage of the present utility model has:
(1)Graphite material corrosion resistance and good, there is good decay resistance and chemical stability, especially anti-chlorine ion With fluorine ion function admirable.
(2)Graphite material good heat conductivity, thermal conductivity factor is big, is only second to copper and aluminium, is 2.5 times of carbon steel, and the 5 of stainless steel Times, it is a kind of material for preferably making heat transmission equipment.
(3)Graphite material is non-toxic, and pollution-free, inside and outside wall is smooth, medium non-scaling, not wall built-up, and fluid resistance is small.
(4)Graphite material linear expansion coefficient is small, heatproof, pressure-resistant function admirable.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the structural representation of condenser of the present utility model.
Embodiment
Illustrate specific embodiment of the present utility model below in conjunction with the accompanying drawings.
A kind of cold-rolling pickling line acid mist recovery provided with big specification tube-type graphite acid mist condenser of the present utility model is net Makeup is put, including the acid mist condenser 2 being connected with acid mist conveyance conduit 1, and gas-liquid separation is provided with this bottom of acid mist condenser 2 Device 3, the watery hydrochloric acid storage tank 4 being connected with gas-liquid separator 3, the gas vent of this gas-liquid separator 3 and the bottom of acid mist scrubbing tower 6 Portion is connected, with this acid mist scrubbing tower 6, the scrubbing tower spray pump 4 that top is connected, with this acid mist scrubbing tower 6 and condensation Watery hydrochloric acid storage tank 3 that the bottom of device 2 is connected, running water valve 5, the acid mist wind being connected with the top of this acid mist scrubbing tower 6 Machine 7 and pipeline 8.
Described big specification tube-type graphite acid mist condenser 2 is Tube Heat Exchanger, by a housing 3, is located at Some heat exchanger tubes 4 in this housing 3, it is located at the fixed tube sheet 2 of this one end of housing 3, the end socket being connected with this fixed tube sheet 2 1, gas access is provided with this phase of end socket 1, is located at the floating tubesheet 6 of this other end of housing 3, is connected with this floating tubesheet 6 End socket 7, it is gas-liquid separator with this end socket 7, provided with condensate outlet and gas vent, it is close is located at the described upside of housing 3 Drain at described fixed tube sheet 2, it is located at cooling water of the described downside of housing 3 at described fixed tube sheet 2 and enters Mouthful, coolant outlet of the described upside of housing 3 at described floating tubesheet 6 is located at, the described downside of housing 3 is located at and leans on Discharging hole at nearly described floating tubesheet 6 is formed.
Housing made of described 3 all carbon steel materials of housing.
Some described heat exchanger tubes 4 are some heat exchanger tubes made of pure graphite material.
Described fixed tube sheet 2 is fixed tube sheet made of pure graphite material.
Described floating tubesheet 6 is floating tubesheet made of pure graphite material.
Described two end sockets 1,7 being connected with fixed tube sheet 2, floating tubesheet 6 are two made of pure graphite material Individual end socket.
Described end socket 7 is gas-liquid separator.
Described scrubbing tower spray pump 4 is two scrubbing tower spray pumps in parallel provided with switching switch, and this two are washed Tower spray pump is fluoroplastics centrifugal pump.
Described ventilation blower 7 is two ventilation blowers in parallel provided with switching switch.

Claims (6)

1. a kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser, including with acid Tube-type graphite condenser that mist conveyance conduit is connected, acid mist scrubbing tower, with this acid mist scrubbing tower, top is connected Scrubbing tower spray pump, watery hydrochloric acid storage tank, the running water being connected with the bottom of this acid mist scrubbing tower and tube-type graphite condenser Valve, with the ventilation blower being connected at the top of this acid mist scrubbing tower, it is characterised in that be provided with described acid mist conveyance conduit One tube-type graphite acid mist condenser, this tube-type graphite acid mist condenser bottom are provided with gas-liquid separator, this gas-liquid separation The acid mist condensate outlet of device is connected with a watery hydrochloric acid storage tank, and the bottom sides of this watery hydrochloric acid storage tank condense with an acid mist Liquid delivery pump is connected, and this acid mist condensate liquid delivery pump is connected by pipeline with complex acid tank, and the gas of this gas-liquid separator goes out Mouth is connected with the bottom of described acid mist scrubbing tower.
2. a kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser according to claim 1 returns Receive purifier, it is characterised in that described big specification tube-type graphite acid mist condenser is Tube Heat Exchanger, by one Individual housing, some heat exchanger tubes being located in this housing, is located at the fixed tube sheet of this shell one end, is connected with this fixed tube sheet End socket, the gas access being connected with this end socket, be located at the floating tubesheet of this housing other end, be connected with this floating tubesheet End socket, the gas vent being connected with this end socket, be located at the emptying at described fixed tube sheet on the upside of described housing Mouthful, the cooling water inlet at described fixed tube sheet on the downside of described housing is located at, is located at close on the upside of described housing Coolant outlet at described floating tubesheet, it is located at the discharging hole institute at described floating tubesheet on the downside of described housing Composition.
3. a kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser according to claim 2 returns Receive purifier, it is characterised in that some described heat exchanger tubes are some heat exchanger tubes made of pure graphite material.
4. a kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser according to claim 2 returns Receive purifier, it is characterised in that described fixed tube sheet is fixed tube sheet made of pure graphite material.
5. a kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser according to claim 2 returns Receive purifier, it is characterised in that described floating tubesheet is floating tubesheet made of pure graphite material.
6. a kind of cold-rolling pickling line acid mist provided with big specification tube-type graphite acid mist condenser according to claim 2 returns Receive purifier, it is characterised in that two end sockets being connected with fixed tube sheet, floating tubesheet are pure graphite material Manufactured two end sockets.
CN201720119724.7U 2017-02-09 2017-02-09 A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser Expired - Fee Related CN206660867U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720119724.7U CN206660867U (en) 2017-02-09 2017-02-09 A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720119724.7U CN206660867U (en) 2017-02-09 2017-02-09 A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser

Publications (1)

Publication Number Publication Date
CN206660867U true CN206660867U (en) 2017-11-24

Family

ID=60378168

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720119724.7U Expired - Fee Related CN206660867U (en) 2017-02-09 2017-02-09 A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser

Country Status (1)

Country Link
CN (1) CN206660867U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109529522A (en) * 2018-12-16 2019-03-29 唐钢美锦(唐山)煤化工有限公司 A kind of ammonia still diffused gas purification process technique
CN110772823A (en) * 2019-10-09 2020-02-11 中盐安徽红四方股份有限公司 Light component removal tower feeding equipment for DMC refining
CN111235586A (en) * 2020-02-28 2020-06-05 马鞍山钢铁股份有限公司 Low acid consumption environment-friendly pickling acid mist pumping and discharging system

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109529522A (en) * 2018-12-16 2019-03-29 唐钢美锦(唐山)煤化工有限公司 A kind of ammonia still diffused gas purification process technique
CN110772823A (en) * 2019-10-09 2020-02-11 中盐安徽红四方股份有限公司 Light component removal tower feeding equipment for DMC refining
CN111235586A (en) * 2020-02-28 2020-06-05 马鞍山钢铁股份有限公司 Low acid consumption environment-friendly pickling acid mist pumping and discharging system

Similar Documents

Publication Publication Date Title
CN108465368A (en) Desulfurization and dedusting disappears white device for deep cleaning
CN206660867U (en) A kind of acid mist recycling purifier of cold-rolling pickling line provided with big specification tube-type graphite acid mist condenser
CN101261058B (en) Evaporation condenser applying harmonica-shaped tube
CN201470140U (en) Acid mist recycling purifier of cold-rolling pickling line with acid mist condenser
CN107400076A (en) A kind of NMP in working procedure of coating lithium ion cell recovery essence steams purifying plant
CN102674491B (en) Seawater desalination device
CN205774224U (en) A kind of NMP in working procedure of coating lithium ion cell reclaims essence and steams purifying plant
CN103277854B (en) Evaporative cooling dehumidification air conditioner unit with waste heat recovery used for air compressor
CN201081559Y (en) Integrated fume cleaning and waste heat recovery device
CN103112836B (en) Method for recycling phosphoric acid in tail gas generated in process of producing activated carbon by phosphoric acid process and utilizing afterheat of tail gas
CN208504437U (en) A kind of dedusting of boiler smoke disappears white waste heat recovering energy conserving emission-reducing system
CN113720049B (en) Evaporative condenser for energy tower heat pump system
CN210198133U (en) Cooling device for sulfuric acid purification
CN210773522U (en) Concurrent flow type evaporative condenser
CN111457672A (en) Method and device for condensing crude chloroethylene
CN203798185U (en) Novel shell and tube evaporative condenser
CN209242713U (en) A kind of high-efficiency energy-saving evaporator
CN212747066U (en) Thick chloroethylene device of condensation
CN207266818U (en) Desulfuration absorbing tower enclosed cyclone condensing dehumidifier
CN207307549U (en) A kind of vacuum drying oven organic gas cools down retracting device
CN107976105A (en) Multi-functional filler and evaporator, condenser and reactor containing multi-functional filler
CN206424596U (en) A kind of high salt organic waste water low-temperature evaporation crystallization apparatus
CN202688001U (en) Acid mist condensing water-saving system of reaction kettle for polymeric aluminum production
CN109443032A (en) A kind of evaporative condenser
CN210448600U (en) NMP waste gas recovery device

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171124

Termination date: 20180209

CF01 Termination of patent right due to non-payment of annual fee