CN206638624U - A kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system - Google Patents
A kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system Download PDFInfo
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- CN206638624U CN206638624U CN201720357269.4U CN201720357269U CN206638624U CN 206638624 U CN206638624 U CN 206638624U CN 201720357269 U CN201720357269 U CN 201720357269U CN 206638624 U CN206638624 U CN 206638624U
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- constant temperature
- electrode material
- detection device
- temperature liquid
- workspace
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Abstract
The utility model provides a kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system, and belonging to electrode material for super capacitor electro-chemical test instrument field wherein electrode material Thermostatic detection device includes device case；Device case has Packed constant temperature runner, and hull outside forms the workspace for accommodating electrolyte, and workspace includes opening；Device case also includes constant temperature liquid entrance and constant temperature liquid exports, and constant temperature liquid entrance is arranged on one end of opening remote on the outside of device case, and is connected with constant temperature liquid pipe, and the outlet of constant temperature liquid is arranged on close to one end of opening on the outside of device case, and is connected with constant temperature liquid pipe.When electrode material Thermostatic detection device is placed into plane, the constant temperature liquid energy from bottom to top flowed provides more stable constant temperature effect.And electrode material Thermostatic detection device carries out system perfecting on this basis, stable thermal environment can be provided for the electro-chemical test of the higher material of heat sensitivity.
Description
Technical field
Electrode material for super capacitor electro-chemical test instrument field is the utility model is related to, in particular to one kind
Electrode material Thermostatic detection device and electrode material Constant Temperature Detection system.
Background technology
The general heat sensitivity of electrode material for super capacitor is higher, can all influence his electrification under fine temperature change
Often temperature control is relatively difficult when learning performance, and carrying out electrochemistry experiment to it, and exclusively carries out heat without existing equipment
The electro-chemical test of the higher electrode material for super capacitor of susceptibility.
Utility model content
The utility model provides a kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system, it is intended to solves
Certainly above mentioned problem existing for electrode material Thermostatic detection device and electrode material Constant Temperature Detection system in the prior art.
What the utility model was realized in：
A kind of electrode material Thermostatic detection device, it includes device case；
Described device housing has Packed constant temperature runner, and the hull outside forms the work for accommodating electrolyte
Area, the workspace include opening；
Described device housing also includes constant temperature liquid entrance and constant temperature liquid exports, and the constant temperature liquid entrance is arranged on described device
One end of the remote opening of hull outside, and connected with the constant temperature liquid pipe, the constant temperature liquid outlet is arranged on described device shell
External side connects close to one end of the opening, and with the constant temperature liquid pipe.
In the utility model preferred embodiment, the workspace is cylinder shape groove.
In the utility model preferred embodiment, described device housing wall thickness 1-2mm.
In the utility model preferred embodiment, the electrode material Thermostatic detection device also includes lid, the lid
Body includes being placed in the choking portion of the workspace and seals the covering part of the opening.
In the utility model preferred embodiment, the lid is provided with axial electrode hole.
In the utility model preferred embodiment, the described one end of electrode material Thermostatic detection device away from the opening
It is provided with flat.
A kind of electrode material Constant Temperature Detection system, it includes thermostat water bath, booster pump and above-mentioned electrode material constant temperature
Detection means；
The thermostat water bath exports including tank, in the tank outlet and the electrode material Thermostatic detection device
Constant temperature liquid entrance is connected, and the constant temperature liquid outlet in the electrode material Thermostatic detection device is connected with the entrance of the booster pump,
The outlet of the booster pump is connected with the tank.
In the utility model preferred embodiment, connected between the tank outlet and the constant temperature liquid entrance with the first flexible pipe
Connect.
It is soft with second between the entrance of the constant temperature liquid outlet and the booster pump in the utility model preferred embodiment
Pipe connects.
In the utility model preferred embodiment, the tank exit is provided with stop valve.
The beneficial effects of the utility model are：Pass through electrode material Thermostatic detection device provided by the utility model and electrode
Material Constant Temperature Detection system, stable temperature conditionss can be provided for the test of electrode material for super capacitor so that thermal sensitivity
Electrode material for super capacitor accurate chemical property result can be obtained in the present apparatus.
Brief description of the drawings
, below will be to required in embodiment in order to illustrate more clearly of the technical scheme of the utility model embodiment
The accompanying drawing used is briefly described, it will be appreciated that and the following drawings illustrate only some embodiments of the present utility model, therefore not
The restriction to scope is should be considered as, for those of ordinary skill in the art, on the premise of not paying creative work,
Other related accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the structural representation at the first visual angle of the electrode material Thermostatic detection device that the utility model embodiment provides
Figure；
Fig. 2 be the utility model embodiment provide electrode material Thermostatic detection device without lid when the second visual angle
Structural representation；
Fig. 3 is the structural representation at the 3rd visual angle of the electrode material Thermostatic detection device that the utility model embodiment provides
Figure；
Fig. 4 is the structural representation for the electrode material Constant Temperature Detection system that the utility model embodiment provides.
Icon：001- electrode material Constant Temperature Detection systems；002- electrode material Thermostatic detection devices；010- device cases；
100- inner casings；110- first is flat；190- sides shell；200- shells；210- second is flat；300- workspaces；310- is open；400-
Constant temperature runner；410- constant temperature liquid entrances；430- constant temperature liquid exports；500- lids；510- choking portions；530- covering parts；600- is permanent
Warm water bath；610- tanks export；The flexible pipes of 630- first；650- stop valves；700- booster pumps；The flexible pipes of 710- second.
Embodiment
To make the purpose, technical scheme and advantage of the utility model embodiment clearer, below in conjunction with this practicality
Accompanying drawing in new embodiment, the technical scheme in the utility model embodiment is clearly and completely described, shown
So, described embodiment is a part of embodiment of the utility model, rather than whole embodiments.Based on this practicality
Embodiment in new, those of ordinary skill in the art are obtained every other under the premise of creative work is not made
Embodiment, belong to the scope of the utility model protection.Therefore, the implementation of the present utility model to providing in the accompanying drawings below
The detailed description of mode is not intended to limit claimed the scope of the utility model, but is merely representative of of the present utility model
Selected embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not making creative labor
The every other embodiment obtained under the premise of dynamic, belong to the scope of the utility model protection.
In description of the present utility model, it is to be understood that the term of indicating position or position relationship is based on accompanying drawing
Shown orientation or position relationship, it is for only for ease of description the utility model and simplifies description, rather than indicates or imply institute
The equipment or element of finger must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that to this reality
With new limitation.
In the utility model, unless otherwise clearly defined and limited, term " installation ", " connected ", " connection ", " Gu
It is fixed " etc. term should be interpreted broadly, for example, it may be fixedly connected or be detachably connected, or integrally；Can be
Mechanically connect or electrically connect；Can be joined directly together, can also be indirectly connected by intermediary, can be two
The connection of element internal or the interaction relationship of two elements.For the ordinary skill in the art, can basis
Concrete condition understands concrete meaning of the above-mentioned term in the utility model.
In the utility model, unless otherwise clearly defined and limited, fisrt feature is on or below second feature
Can directly it be contacted including the first and second features, it is not directly to contact but pass through it that can also include the first and second features
Between other characterisation contact.Moreover, fisrt feature is on second feature, top and above include fisrt feature the
Directly over two features and oblique upper, or be merely representative of fisrt feature level height and be higher than second feature.Fisrt feature is special second
Under sign, lower section and fisrt feature included below are immediately below second feature and obliquely downward, or are merely representative of fisrt feature level
Highly it is less than second feature.
Embodiment one
A kind of electrode material Thermostatic detection device 002 is present embodiments provided, referring to Fig. 1, this electrode material constant temperature
Detection means 002 includes device case 010.
Fig. 1 and Fig. 2 are referred to, device case 010 includes inner casing 100 and shell 200 in the present embodiment, and inner casing 100 is
Cylindrical shell, and including first flat 110, be internally formed workspace 300 in inner casing 100, electricity can be accommodated in workspace 300
Solve liquid and carry out electrode material Constant Temperature Detection experiment.Shell 200 is the cylindrical shell that diameter of section is more than the diameter of section of inner casing 100
Body, shell 200 radially wraps up inner casing 100, and with second flat 210, second flat 210 is parallel with first flat 110.Pass through
Second flat 210 can be positioned over electrode material Thermostatic detection device 002 in plane.
The section radius of inner casing 100 are 20mm in the utility model, and the section radius of shell 200 are 30mm, inner casing 100
The constant temperature runner that spacing is uniformly 5mm is formed with the center overlapping of axles of shell 200, between the side wall of inner casing 100 and the side wall of shell 200
400。
Device case 010 also includes sealing inner casing 100 and shell 200 to form the side shell 190 of constant temperature runner 400.Constant temperature
Runner 400 wraps up wall and the bottom surface of whole inner casing 100.By that can be work toward isothermal liquid is passed through in constant temperature runner 400
Area 300 provides stationary temperature so that can carry out the experiment of constant temperature in workspace 300.
Workspace 300 has opening 310, adds electrolyte from opening 310, can also be inserted from opening 310 to electrode, reference
Electrode and working electrode, so as to the electro-chemical test to carrying out two electrode systems or three-electrode system in workspace 300.
Referring to Fig. 1, Fig. 2 and Fig. 3, constant temperature liquid entrance 410 is provided with the one end of the side wall of shell 200 away from opening 310,
One end of opening 310 is provided with constant temperature liquid outlet 430 in the side wall of shell 200.When electrode material Thermostatic detection device 002
Second flat 210 when placing in the plane, is passed through constant temperature liquid by constant temperature liquid entrance 410, it is permanent to pass through the outflow of constant temperature liquid outlet 430
Warm liquid, due to constant temperature liquid entrance 410 less than constant temperature liquid outlet 430, increased resident time of the constant temperature liquid in constant temperature runner 400,
Help to keep constant temperature in workspace 300.
In the present embodiment, constant temperature liquid entrance 410 and constant temperature liquid outlet 430 are diameter 5mm circular port, and past remote
The direction extension of axial line.
In the present embodiment, inner casing 100 and shell 200 are made by heat resistant glass, and wherein the wall thickness of inner casing 100 is 1mm,
Heat resistant glass can ensure to work long hours, and relatively thin wall thickness is while proof strength, can strengthen constant temperature runner 400 with
Heat exchange between workspace 300.
Electrode material Thermostatic detection device 002 also includes lid 500, and lid 500 includes choking portion 510 and covering part 530,
Choking portion 510 is the cylinder that diameter of section is less than the diameter of section of workspace 300.Choking portion 510 has less thickness, can be with
While fixed lid 500, liquid level of electrolyte is not contacted.Covering part 530 is that diameter of section is more than the diameter of section of workspace 300
Cylinder.Covering part 530 has relatively large thickness, can cover opening 310 by covering part 530, and be insertion
The electrode of lid 500 plays a part of guiding.
Axial electrode hole is provided with lid 500, with power pole insert workspace 300, carry out two electrode tests or
Three electrode tests.
The application method of electrode material Thermostatic detection device 002 provided by the utility model is：Added in workspace 300
Electrolyte, lid 500 is covered, electrode is inserted from the electrode hole on lid 500, adjust the spacing between each electrode to reach examination
Requirement is tested, constant temperature liquid is arranged at the place higher than electrode material Thermostatic detection device 002, perseverance is passed through from constant temperature liquid entrance 410
Warm liquid, constant temperature liquid at the uniform velocity enters constant temperature runner 400 by Action of Gravity Field, then is taken over from constant temperature liquid outlet 430 and constant temperature liquid is led to
Go out, enter the stabilization of trip temperature to workspace 300 by constant temperature liquid, so that Electrochemical results are accurate.
In the utility model, the radius of inner casing 100 can be not only 20mm, or other, the radius of shell 200
Can be not only 30, or other, as long as wrapping up inner casing 100 by shell 200 to form constant temperature runner 400.It is interior
The wall thickness of shell 100 can be not only 1mm, or the arbitrary value between 1mm-2mm, can so ensure electrode material constant temperature
The temperature adjustment of requirement of experiment is provided up while 002 stability of detection means for workspace 300.
Can be electrode material for super capacitor by electrode material Thermostatic detection device 002 provided by the utility model
Test stable temperature conditionss are provided so that the electrode material for super capacitor of thermal sensitivity can obtain accurately in the present apparatus
Chemical property result.
Embodiment two
A kind of electrode material Constant Temperature Detection system 001 is present embodiments provided, referring to Fig. 4, this electrode material constant temperature
Detecting system 001 includes electrode material Thermostatic detection device 002, thermostat water bath 600 and booster pump 700.
Include tank outlet 610 in thermostat water bath 600, thermostat water bath 600 can be that electrode material Constant Temperature Detection fills
02 offer constant temperature liquid is provided.
And booster pump 700 can receive the constant temperature liquid discharged from electrode material Thermostatic detection device 002 and be back to again
In thermostat water bath 600.
Fig. 1, Fig. 2 and Fig. 3 are referred to, wherein electrode material Thermostatic detection device 002 includes device case 010.In this reality
To apply in example, device case 010 includes inner casing 100 and shell 200, and inner casing 100 is cylindrical shell, and including first flat 110,
Workspace 300 is internally formed in inner casing 100, electrolyte can be accommodated in workspace 300 and carries out electrode material Constant Temperature Detection experiment.
Shell 200 is the cylindrical shell that diameter of section is more than the diameter of section of inner casing 100, and shell 200 radially wraps up inner casing 100, and has
Have second flat 210, second flat 210 is parallel with first flat 110.Electrode material constant temperature can be examined by second flat 210
Device 002 is surveyed to be positioned in plane.
The section radius of inner casing 100 are 20mm in the utility model, and the section radius of shell 200 are 30mm, inner casing 100
The constant temperature runner that spacing is uniformly 5mm is formed with the center overlapping of axles of shell 200, between the side wall of inner casing 100 and the side wall of shell 200
400。
Device case 010 also includes sealing inner casing 100 and shell 200 to form the side shell 190 of constant temperature runner 400.Constant temperature
Runner 400 wraps up wall and the bottom surface of whole inner casing 100.By that can be work toward isothermal liquid is passed through in constant temperature runner 400
Area 300 provides stationary temperature so that can carry out the experiment of constant temperature in workspace 300.
Workspace 300 has opening 310, adds electrolyte from opening 310, can also be inserted from opening 310 to electrode, reference
Electrode and working electrode, so as to the electro-chemical test to carrying out two electrode systems or three-electrode system in workspace 300.
The one end of the side wall of shell 200 away from opening 310 is provided with constant temperature liquid entrance 410, leaned in the side wall of shell 200
One end of nearly opening 310 is provided with constant temperature liquid outlet 430.Second flat 210 when electrode material Thermostatic detection device 002 places
When in the plane, constant temperature liquid is passed through by constant temperature liquid entrance 410, by the outflow constant temperature liquid of constant temperature liquid outlet 430, due to constant temperature liquid
Entrance 410 increased resident time of the constant temperature liquid in constant temperature runner 400, contributes to workspace 300 less than constant temperature liquid outlet 430
Interior holding constant temperature.
In the present embodiment, constant temperature liquid entrance 410 and constant temperature liquid outlet 430 are diameter 5mm circular port, and past remote
The direction extension of axial line.
In the present embodiment, inner casing 100 and shell 200 are made by heat resistant glass, and wherein the wall thickness of inner casing 100 is 1mm,
Heat resistant glass can ensure to work long hours, and relatively thin wall thickness is while proof strength, can strengthen constant temperature runner 400 with
Heat exchange between workspace 300.
Electrode material Thermostatic detection device 002 also includes lid 500, and lid 500 includes choking portion 510 and covering part 530,
Choking portion 510 is the cylinder that diameter of section is less than the diameter of section of workspace 300.Choking portion 510 has less thickness, can be with
While fixed lid 500, liquid level of electrolyte is not contacted.Covering part 530 is that diameter of section is more than the diameter of section of workspace 300
Cylinder.Covering part 530 has relatively large thickness, can cover opening 310 by covering part 530, and be insertion
The electrode of lid 500 plays a part of guiding.
Axial electrode hole is provided with lid 500, with power pole insert workspace 300, carry out two electrode tests or
Three electrode tests.
Thermostat water bath 600 includes tank outlet 610, is provided with tank outlet 610 for controlling water bath stream
The stop valve 650 of amount, connected between stop valve 650 and constant temperature liquid entrance 410 by the first flexible pipe 630, the connected mode of flexible pipe
The test result in the vibration effect electrode material Thermostatic detection device 002 of thermostat water bath 600 can be prevented.
Connected between the entrance of constant temperature liquid outlet 430 and booster pump 700 by the second flexible pipe 710, the connected mode of flexible pipe can
To prevent the test result in the vibration effect electrode material Thermostatic detection device 002 of booster pump 700.
When being tested, thermostat water bath 600 is positioned over the place higher than electrode material Thermostatic detection device 002, permanent
Constant temperature liquid in warm water bath 600 can be uniformly flowed into electrode material Thermostatic detection device 002 by gravity.And booster pump 700
Supercharging lifting liquid level is carried out, the constant temperature liquid that electrode material Thermostatic detection device 002 flows out is imported into thermostat water bath 600 again
It is interior.
The application method of electrode material Thermostatic detection device 002 provided by the utility model is：Added in workspace 300
Electrolyte, lid 500 is covered, electrode is inserted from the electrode hole on lid 500, adjust the spacing between each electrode to reach examination
Requirement is tested, thermostat water bath 600 is arranged at the place higher than electrode material Thermostatic detection device 002, opens stop valve 650,
So that constant temperature liquid flows into from constant temperature liquid entrance 410, constant temperature liquid at the uniform velocity enters constant temperature runner 400 by Action of Gravity Field, then from constant temperature
Liquid outlet 430, which is taken over, causes constant temperature liquid pass-out, enters the stabilization of trip temperature to workspace 300 by constant temperature liquid, so that electrochemical
It is accurate to learn test result.After terminating experiment, booster pump 700 is closed, closes stop valve 650.
In the utility model, the radius of inner casing 100 can be not only 20mm, or other, the radius of shell 200
Can be not only 30, or other, as long as wrapping up inner casing 100 by shell 200 to form constant temperature runner 400.It is interior
The wall thickness of shell 100 can be not only 1mm, or the arbitrary value between 1mm-2mm, can so ensure electrode material constant temperature
The temperature adjustment of requirement of experiment is provided up while 002 stability of detection means for workspace 300.
The utility model also includes a kind of electrode material Constant Temperature Detection method, and it uses electrode material Constant Temperature Detection system
001, comprise the following steps：
A. constant temperature liquid is added into thermostat water bath 600, thermostat water bath 600 is opened, to constant temperature liquid temperature adjustment；
B. thermostat water bath 600 is positioned over the plane higher than electrode material Thermostatic detection device 002；
C. booster pump 700 is opened so that thermostat water bath 600, electrode material Thermostatic detection device 002 and booster pump 700
Form constant temperature liquid stream loop；
D. electrolyte is added into the workspace 300 of electrode material Thermostatic detection device 002, stood to test temperature；
E. lid 500 is covered, insertion electrode carries out electrochemical measurement.
Can be electrode material for super capacitor by electrode material Thermostatic detection device 002 provided by the utility model
Test stable temperature conditionss are provided so that the electrode material for super capacitor of thermal sensitivity can obtain accurately in the present apparatus
Chemical property result.
Claims (10)
1. a kind of electrode material Thermostatic detection device, it is characterised in that including device case；
Described device housing has Packed constant temperature runner, and the hull outside forms the workspace for accommodating electrolyte, institute
Stating workspace includes opening；
Described device housing also includes constant temperature liquid entrance and constant temperature liquid exports, and the constant temperature liquid entrance is arranged on described device housing
One end of the remote opening in outside, and connected with the constant temperature liquid pipe, the constant temperature liquid outlet is arranged on outside described device housing
Side connects close to one end of the opening, and with the constant temperature liquid pipe.
2. electrode material Thermostatic detection device according to claim 1, it is characterised in that the workspace is recessed for cylinder
Groove.
3. electrode material Thermostatic detection device according to claim 1, it is characterised in that described device housing wall thickness 1-
2mm。
4. electrode material Thermostatic detection device according to claim 2, it is characterised in that the electrode material Constant Temperature Detection
Device also includes lid, and the lid includes being placed in the choking portion of the workspace and seals the covering part of the opening.
5. electrode material Thermostatic detection device according to claim 4, it is characterised in that the lid is provided with axial
Electrode hole.
6. electrode material Thermostatic detection device according to claim 1, it is characterised in that the electrode material Constant Temperature Detection
The one end of device away from the opening is provided with flat.
7. a kind of electrode material Constant Temperature Detection system, it is characterised in that including thermostat water bath, booster pump and claim 1-6
Electrode material Thermostatic detection device described in any one；
The thermostat water bath exports including tank, the tank outlet and the constant temperature in the electrode material Thermostatic detection device
Liquid entrance is connected, and the constant temperature liquid outlet in the electrode material Thermostatic detection device is connected with the entrance of the booster pump, described
The outlet of booster pump is connected with the tank.
8. electrode material Constant Temperature Detection system according to claim 7, it is characterised in that the tank outlet and the perseverance
Connected between warm liquid entrance with the first flexible pipe.
9. electrode material Constant Temperature Detection system according to claim 7, it is characterised in that constant temperature liquid outlet with it is described
Connected between the entrance of booster pump with the second flexible pipe.
10. electrode material Constant Temperature Detection system according to claim 8, it is characterised in that the tank exit is set
There is stop valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720357269.4U CN206638624U (en) | 2017-04-06 | 2017-04-06 | A kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720357269.4U CN206638624U (en) | 2017-04-06 | 2017-04-06 | A kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system |
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| Publication Number | Publication Date |
|---|---|
| CN206638624U true CN206638624U (en) | 2017-11-14 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720357269.4U Expired - Fee Related CN206638624U (en) | 2017-04-06 | 2017-04-06 | A kind of electrode material Thermostatic detection device and electrode material Constant Temperature Detection system |
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| Country | Link |
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| CN (1) | CN206638624U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107045009A (en) * | 2017-04-06 | 2017-08-15 | 盐城工学院 | A kind of electrode material Thermostatic detection device, electrode material Constant Temperature Detection system and electrode material Constant Temperature Detection method |
-
2017
- 2017-04-06 CN CN201720357269.4U patent/CN206638624U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107045009A (en) * | 2017-04-06 | 2017-08-15 | 盐城工学院 | A kind of electrode material Thermostatic detection device, electrode material Constant Temperature Detection system and electrode material Constant Temperature Detection method |
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