CN206635036U - A kind of Purification of Carbon Nanotubes device - Google Patents
A kind of Purification of Carbon Nanotubes device Download PDFInfo
- Publication number
- CN206635036U CN206635036U CN201720133273.2U CN201720133273U CN206635036U CN 206635036 U CN206635036 U CN 206635036U CN 201720133273 U CN201720133273 U CN 201720133273U CN 206635036 U CN206635036 U CN 206635036U
- Authority
- CN
- China
- Prior art keywords
- container
- washing drying
- purification
- reactor
- pipeline
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000746 purification Methods 0.000 title claims abstract description 21
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 239000002041 carbon nanotube Substances 0.000 title claims abstract description 13
- 229910021393 carbon nanotube Inorganic materials 0.000 title claims abstract description 13
- 238000005406 washing Methods 0.000 claims abstract description 30
- 238000001035 drying Methods 0.000 claims abstract description 28
- 238000007599 discharging Methods 0.000 claims abstract description 15
- 239000002699 waste material Substances 0.000 claims abstract description 11
- 239000012530 fluid Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000003860 storage Methods 0.000 claims abstract description 9
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims abstract description 7
- 239000007789 gas Substances 0.000 claims description 7
- 238000005070 sampling Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 5
- 230000007246 mechanism Effects 0.000 claims description 4
- 238000002242 deionisation method Methods 0.000 claims description 2
- 239000002912 waste gas Substances 0.000 claims description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 3
- 239000002071 nanotube Substances 0.000 description 3
- 238000005554 pickling Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000001241 arc-discharge method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004523 catalytic cracking Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Carbon And Carbon Compounds (AREA)
Abstract
The utility model discloses a kind of Purification of Carbon Nanotubes device, including reactor, washing drying container, waste fluid container, deionized water storage container and drier to place container；Reactor includes first charging aperture and the first discharging opening, reactor has agitating shaft, paddle and motor, washing drying container includes second charging aperture and the second discharging opening, first discharging opening connects the second charging aperture, first discharge outlet has the first valve, second discharging opening connects waste fluid container by waste-solution line, has the second valve on waste-solution line；Deionized water storage container connects washing drying container by the first pipeline, has the first magnetic valve and liquid pump on the first pipeline, and drier places container and connects washing drying container by the second pipeline, has second solenoid valve on the second pipeline；There is filter screen portion in washing drying container.Purification devices of the present utility model can effectively realize the purifying to CNT.
Description
Technical field
It the utility model is related to new energy field, and in particular to a kind of Purification of Carbon Nanotubes device.
Background technology
CNT is as nano material, and in light weight, hexagonal structure connection is perfect, has many abnormal mechanics, electricity
And chemical property.Especially also there are prominent application, the preparation method of common CNT in field of batteries CNT
There are arc discharge method, laser evaporization method and catalytic cracking solution.But the CNT prepared usually has many impurity,
Need to purify, but existing purifier apparatus species is not also a lot.
Utility model content
Purpose of utility model：A kind of the defects of the utility model is intended to overcome prior art, there is provided Purification of Carbon Nanotubes dress
Put.
Technical scheme：A kind of Purification of Carbon Nanotubes device, including reactor, washing drying container, waste fluid container, deionization
Water storage container and the drier for placing drier place container；The reactor includes first charging aperture and the first discharging
Mouthful, the reactor has the motor of agitating shaft, paddle and the driving agitating shaft, and the washing drying container includes
Second charging aperture and the second discharging opening, first discharging opening connect the second charging aperture, and first discharge outlet has
First valve, second discharging opening connect waste fluid container by waste-solution line, have the second valve on the waste-solution line；Institute
State deionized water storage container and the washing drying container is connected by the first pipeline, there is the first electromagnetism on first pipeline
Valve and liquid pump, the drier place container and connect the washing drying container by the second pipeline, on second pipeline
With second solenoid valve；There is filter screen portion in the washing drying container.
Further, there are multiple first heaters in the reactor.
Further, the washing drying container has multiple secondary heating mechanisms.
Further, the washing drying container has lateral opening and the side door for closing the lateral opening.
Further, the purification devices also include gas sampling unit, and the reactor connects institute by exhaust pipe
State gas sampling unit.
Further, the reactor includes kettle and kettle cover.
Beneficial effect：Purification devices of the present utility model can carry out pickling impurity removal, washing and drying, so as to realize to carbon
The purifying of nanotube.
Brief description of the drawings
Fig. 1 is purification devices schematic diagram.
Embodiment
Reference：11 kettlies；11.1 first heaters；12 kettle covers；13 motors；14 agitating shafts；15 paddles；
16 charging apertures；17 exhaust pipes；18 gas sampling units；19 first valves；31 washing drying containers；31.1 second heating dresses
Put；32 side doors；33 first pipelines；33.1 the first magnetic valve；33.2 liquid pumps；34 deionized water storage containers；35 second pipelines；
35.1 second solenoid valves；36 drier place container；37 filter screen portions；38 waste-solution lines；38.1 the second valve；39 waste fluid containers.
A kind of Purification of Carbon Nanotubes device, including reactor, washing drying container 31, waste fluid container 39, deionized water are deposited
Storage container 34 and the drier for placing drier place container 36；The reactor goes out including first charging aperture 16 and first
Material mouth, the reactor have the motor 13 of agitating shaft 14, paddle 15 and the driving agitating shaft 14, and the washing is dried
Dry container 31 includes second charging aperture and the second discharging opening, and first discharging opening connects the second charging aperture, and described first
Discharge outlet has the first valve 19, and second discharging opening connects waste fluid container 39, the sewer pipe by waste-solution line 38
There is the second valve 38.1 on road 38；The deionized water storage container 34 connects the washing drying by the first pipeline 33 to be held
Device 31, has the first magnetic valve 33.1 and liquid pump 33.2 on first pipeline 33, and the drier is placed container 36 and passed through
Second pipeline 35 connects the washing drying container, has second solenoid valve 35.1 on second pipeline 35；The washing is dried
There is filter screen portion 37 in dry container 31.There are multiple first heaters 11.1 in the reactor 11.The washing drying is held
Device 31 has multiple secondary heating mechanisms 31.1.The washing drying container 31 has lateral opening and for closing the side
The side door 32 of opening.The purification devices also include gas sampling unit 18, and the reactor connects institute by exhaust pipe 17
State gas sampling unit 18.The reactor includes kettle 11 and kettle cover 12.
Purification devices of the present utility model, workflow are as follows：1 pickling, by being put into the carbon with impurity from charging aperture
Nanotube and hydrochloric acid, now the first valve close, paddle is stirred, and first heater is heated, and utilizes hydrochloric acid will
Impurity is reacted away, and the waste gas in acid cleaning process is collected by gas sampling unit；2 washing, pickling opened after terminating the first valve and
Second valve (now second solenoid valve closing), expect in filter screen portion under CNT, waste liquid enters waste fluid container, closes afterwards
First valve, washed by liquid pump to CNT water filling, it is repeated multiple times to be washed, after treating repeatedly washing,
Close the second valve and the first magnetic valve, open second solenoid valve, open secondary heating mechanism, so as to by unnecessary moisture evaporation
Absorbed by drier, so as to realize the drying to CNT.After drying, side door can be opened, takes out carbon after purification
Nanotube.
Although the utility model is illustrated and described with regard to preferred embodiment, those skilled in the art should manage
Solution, without departing from claim limited range of the present utility model, the utility model can be carried out various change and
Modification.
Claims (6)
1. a kind of Purification of Carbon Nanotubes device, it is characterised in that including reactor, washing drying container, waste fluid container, deionization
Water storage container and the drier for placing drier place container；The reactor includes first charging aperture and the first discharging
Mouthful, the reactor has the motor of agitating shaft, paddle and the driving agitating shaft, and the washing drying container includes
Second charging aperture and the second discharging opening, first discharging opening connect the second charging aperture, and first discharge outlet has
First valve, second discharging opening connect waste fluid container by waste-solution line, have the second valve on the waste-solution line；Institute
State deionized water storage container and the washing drying container is connected by the first pipeline, there is the first electromagnetism on first pipeline
Valve and liquid pump, the drier place container and connect the washing drying container by the second pipeline, on second pipeline
With second solenoid valve；There is filter screen portion in the washing drying container.
2. Purification of Carbon Nanotubes device according to claim 1, it is characterised in that have multiple first in the reactor
Heater.
3. Purification of Carbon Nanotubes device according to claim 1, it is characterised in that the washing drying container has multiple
Secondary heating mechanism.
4. Purification of Carbon Nanotubes device according to claim 1, it is characterised in that the washing drying container has side
Opening and the side door for closing the lateral opening.
5. Purification of Carbon Nanotubes device according to claim 1, it is characterised in that the purification devices also include waste gas and received
Collect unit, the reactor connects the gas sampling unit by exhaust pipe.
6. Purification of Carbon Nanotubes device according to claim 1, it is characterised in that the reactor includes kettle and kettle
Lid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720133273.2U CN206635036U (en) | 2017-02-14 | 2017-02-14 | A kind of Purification of Carbon Nanotubes device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720133273.2U CN206635036U (en) | 2017-02-14 | 2017-02-14 | A kind of Purification of Carbon Nanotubes device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206635036U true CN206635036U (en) | 2017-11-14 |
Family
ID=60252183
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720133273.2U Expired - Fee Related CN206635036U (en) | 2017-02-14 | 2017-02-14 | A kind of Purification of Carbon Nanotubes device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206635036U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110090834A (en) * | 2019-04-02 | 2019-08-06 | 南京威安新材料科技有限公司 | The purification devices of medicament-carried nano capsule |
-
2017
- 2017-02-14 CN CN201720133273.2U patent/CN206635036U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110090834A (en) * | 2019-04-02 | 2019-08-06 | 南京威安新材料科技有限公司 | The purification devices of medicament-carried nano capsule |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171114 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |