CN206604216U - Distilling apparatus - Google Patents

Abstract

The utility model discloses a kind of distilling apparatus, including distillation component and condensation liquid collecting component, distilling component includes reaction bulb, rectifying column, still head and thermometer, rectifying column is installed on reaction bulb, still head is installed on rectifying column, the top of still head is installed by thermometer, condensing liquid collecting component includes condenser pipe, Jie Shou ping and the adapter of vacuum tail, condenser pipe is arranged on still head, multiple liquid collecting still heads and multiple adapters are set between condenser pipe and the adapter of vacuum tail, multiple liquid collecting still heads are to be connected in free combination with multiple adapters, a Jie Shou ping is all connected with each liquid collecting still head and vacuum tail adapter.The utility model is simple in construction, the spacing between simple and convenient assembly and safe Jie Shou ping and Jie Shou ping is larger, therefore large volume of Jie Shou ping can be used, more Jie Shou ping can be set simultaneously, so as to once collect more cuts, frequently more changing-over ping need not be received, reduce labor intensity, improve distillation efficiency.

Description

Distilling apparatus

Technical field

The utility model is related to distilling apparatus, more particularly to a kind of can collect the distilling apparatus of a variety of cuts.

Background technology

At present, in chemical experiment, the distilling apparatus of prior art is usually in condenser pipe afterbody when collecting condensate liquid Threeway is connected, three Jie Shou ping are connected by threeway, the collection of different fractions is realized.Due to the spacing between each interface of threeway It is smaller, therefore the size for meeting receipts ping that each interface is connected in threeway is severely limited, and frequently more changing-over is needed when receiving condensate liquid Shou ping, add labor intensity, and Jie Shou ping quantity at most only three, it is impossible to meet the need for receiving more than three kinds cuts Ask.

Utility model content

The technical problems to be solved in the utility model is that the drawbacks described above for prior art is filled there is provided one kind distillation Put, the distilling apparatus is easy to operate, security performance is high, can realize the collection of a variety of cuts, is particularly suitable for use in relatively large or evaporates Divide the distillation compared with multi-product.

In order to realize above-mentioned technical purpose, above-mentioned technique effect is reached, the utility model is achieved through the following technical solutions：

A kind of distilling apparatus, including distillation component and condensation liquid collecting component, the distillation component include reaction bulb, rectifying Installed on post, still head and thermometer, the reaction bulb and the still head, institute are installed on the rectifying column, the rectifying column The thermometer is installed at the top for stating still head, and the condensation liquid collecting component includes condenser pipe, Jie Shou ping and the adapter of vacuum tail, The condenser pipe is arranged on the still head, and multiple liquid collecting still heads are set between the condenser pipe and vacuum tail adapter With multiple adapters, the multiple liquid collecting still head is with the multiple adapter to be connected in free combination, and each liquid collecting is steamed Evaporate and be all connected with a Jie Shou ping in head and vacuum tail adapter.

Further, the lower section of the reaction bulb sets having heaters.

Further, the thermometer is arranged on the top of the still head by rubber stopper.

Further, the liquid collecting still head can arbitrarily rotate.

Its advantage is：

It is simple in construction that the utility model provides a kind of distilling apparatus, simple and convenient assembly and safe, relative to prior art In three meet receipts ping and be arranged in a threeway, cause to connect receipts ping small volumes, need frequently more changing-over to receive ping, the steaming during distillation The Jie Shou ping of distillation unit are separately mounted in liquid collecting still head and the adapter of vacuum tail, spacing between Jie Shou ping and Jie Shou ping compared with Greatly, therefore large volume of Jie Shou ping can be used, while setting multiple liquid collecting still heads, you can to set multiple Jie Shou ping, So as to once collect more cuts, it is not necessary to which frequently ping is received in more changing-over, reduces labor intensity, distillation effect is improved Rate.

Brief description of the drawings

Fig. 1 is the structural representation of the utility model preferred embodiment；

Reference therein is：1-reaction bulb；2-rectifying column；3-still head；4-thermometer；5-condenser pipe； 6-liquid collecting still head；7-adapter；8-vacuum tail is taken over；9-Jie Shou ping.

Embodiment

The technical solution of the utility model is further explained below in conjunction with drawings and examples, but below interior Appearance is not used in restriction protection domain of the present utility model.

Shown in reference picture 1, as a kind of distilling apparatus of preferred embodiment of the present utility model, including component is distilled and cold Aggegation liquid component, distillation component includes installing rectifying column on reaction bulb 1, rectifying column 2, still head 3 and thermometer, reaction bulb 1 2, still head 3 is installed, thermometer 4 is installed at the top of still head 3, and condensation liquid collecting component includes condenser pipe 5, received on rectifying column 2 ping 9 and vacuum tail adapter 8, condenser pipe 5 are arranged on still head 3, and two collection are set between condenser pipe 5 and vacuum tail adapter 8 Liquid still head 6 and two adapters 7, two liquid collecting still heads 6 are connected with two adapters 7 to alternate, and each liquid collecting is steamed Evaporate and a Jie Shou ping 9 is all connected with first 6 and vacuum tail adapter 8.Steam enters in condenser pipe 5 by still head 3 and cooled down during distillation Into liquid distillate, each Jie Shou ping 9 is then flowed into by liquid collecting still head 6 and adapter 7, last vacuum tail adapter 8 and One be arranged in vacuum tail adapter 8, which meets receipts ping 9, can either collect liquid distillate, can be used for sealing whole distillation dress again Put.Jie Shou ping are arranged on liquid collecting still head 6, are connected between two liquid collecting still heads 6 by adapter 7, are increased two collection Spacing between liquid still head 6, therefore large volume of Jie Shou ping 9 can be used.

As one of the present utility model preferably, multiple liquid collecting still heads 6 are set between condenser pipe 5 and vacuum tail adapter 8 With multiple adapters 7, the multiple liquid collecting still head 6 is to be connected in free combination with the multiple adapter 7.Multiple liquid collectings are set Still head 6, you can to set multiple Jie Shou ping 9, so as to once collect more cuts, it is not necessary to frequently change and receive ping, reduces labor intensity, improves distillation efficiency.

As one of the present utility model deformation, the lower section of the reaction bulb sets having heaters, the heating shape of heater Formula can be Electromagnetic Heating, oil bath heating, heating water bath etc..

Preferably, thermometer 4 is arranged on the top of the still head 3 by rubber stopper, and rubber stopper is used to seal still head 3 Top, and rubber stopper facilitates the installation and dismounting of thermometer.

It is highly preferred that liquid collecting still head 6 can arbitrarily rotate, collection still head 6 can drive Jie Shou ping 9 to rotate to random angle Degree conveniently meets receipts ping 9 and put, and avoids the occurrence of some and connect and receive ping 9 and collect the too fast phenomenon of liquid distillate.

It is not new to this practicality although above-mentioned embodiment of the present utility model is described with reference to accompanying drawing The limitation of type protection domain, one of ordinary skill in the art should be understood that on the basis of the technical solution of the utility model, ability Field technique personnel need not pay the various modifications that creative work can make or deform still in protection model of the present utility model In enclosing.

Claims (4)

1. a kind of distilling apparatus, including distillation component and condensation liquid collecting component, it is characterised in that the distillation component includes reaction Installed on bottle, rectifying column, still head and thermometer, the reaction bulb and the steaming is installed on the rectifying column, the rectifying column Head is evaporated, the thermometer is installed at the top of the still head, and the condensation liquid collecting component includes condenser pipe, Jie Shou ping and vacuum Tail is taken over, and the condenser pipe is arranged on the still head, and multiple collection are set between the condenser pipe and vacuum tail adapter Liquid still head and multiple adapters, the multiple liquid collecting still head are to be connected in free combination with the multiple adapter, Mei Gesuo State and be all connected with a Jie Shou ping in liquid collecting still head and vacuum tail adapter.

2. distilling apparatus according to claim 1, it is characterised in that the lower section of the reaction bulb sets having heaters.

3. distilling apparatus according to claim 1, it is characterised in that the thermometer is arranged on described steam by rubber stopper Evaporate the top of head.

4. distilling apparatus according to claim 1, it is characterised in that the liquid collecting still head can arbitrarily rotate.