CN206597541U - A kind of modified chemical reaction device - Google Patents

A kind of modified chemical reaction device Download PDF

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Publication number
CN206597541U
CN206597541U CN201720361265.3U CN201720361265U CN206597541U CN 206597541 U CN206597541 U CN 206597541U CN 201720361265 U CN201720361265 U CN 201720361265U CN 206597541 U CN206597541 U CN 206597541U
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CN
China
Prior art keywords
reactor
kettle cover
pipe
chemical reaction
reaction device
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Expired - Fee Related
Application number
CN201720361265.3U
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Chinese (zh)
Inventor
贺泽峰
明星
李�杰
靳海霞
宋飞飞
袁兴帅
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Individual
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Individual
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Priority to CN201720361265.3U priority Critical patent/CN206597541U/en
Application granted granted Critical
Publication of CN206597541U publication Critical patent/CN206597541U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of modified chemical reaction device, including reactor, be provided with kettle cover at the top of reactor, kettle cover it is cylindrical on be provided with below fixed card slot, each fixed card slot and be each equipped with moving screw;Reactor has interlayer;Two motor are provided with kettle cover and two sets of agitating shafts are configured with;Feed pipe, discharge nozzle, gas-adding pipe, blast pipe and relief tube are provided with reactor;Flush pipe is provided with kettle cover, flush pipe is connected with the spray head being arranged on inside kettle cover, flush pipe access water tank, water tank is connected with high pressure gas holder.Two are provided with reactor of the present utility model turn to different agitating shafts and be staggered and paddle and be disposed with chute, reaction mass mixing can be allowed more uniform;Simultaneous reactions kettle is also configured with condenser and filter, volatile gas can be reclaimed and purification reaction thing.

Description

A kind of modified chemical reaction device
Technical field
The utility model is related to technical field of chemical, and in particular to a kind of modified chemical reaction device.
Background technology
In the traditional chemical process of China, still reaction device is a kind of essential chemical industry equipment, wherein The main reactor including enamel material and stainless steel material.When the reactor is equipped with motor, agitating paddle and some other Just most chemical reaction can be completed after servicing unit.
Usual chemical reaction kettle internal structure is generally that cylinder body adds oval bottom, is widely used in liquid-liquid phase, liquid-solid phase Work hybrid reaction, applicability is preferable and operating flexibility is big.But in actual chemical reaction, such as to carry out Large Copacity liquid-liquid phase or During liquid-solid phase reaction, such reactor there is excessive agitating paddle stress, the temperature of hybrid reaction material and even concentration It is not good, the problems such as a conversion ratio is not high, or even the homogeneity of product quality can be influenceed.Therefore, existing retort is stirred Mix mode and device is optimized and is necessary.
In addition, the reaction unit of prior art is also present, volume is larger to be not easy to carry, and is not suitable for miniaturization scale up test Or experiment.Often turn into intermediate after the completion of being chemically reacted in simultaneous reactions kettle, it is necessary to preservation in pans is passed into, at this During need to use certain mode that pure reaction product is transported in pans.Existing major part is directly to pass through Pipeline is conveyed so that the part debris in reactor is likely to enter in pans, is contaminated it.Therefore design is needed A kind of novel chemical reactor is to solve the above problems.
Utility model content
The purpose of this utility model is to provide a kind of modified chemical reaction device.
For up to above-mentioned purpose, a kind of modified chemical reaction device is provided in one embodiment of the present utility model, its It is characterised by:Including reactor, reactor is fixed on support;Be provided with kettle cover at the top of reactor, kettle cover it is cylindrical on set It is equipped with below some fixed card slots, each fixed card slot and is each equipped with a moving screw being fixed on reactor, activity Screw arrangement has a WING NUTS, by WING NUTS by reactor and kettle cover clamping in moving screw insertion fixed card slot;It is fixed The upper end of neck is provided with a concave station, enters during WING NUTS clamping in concave station;
Reactor, which has, is provided with electric heater unit and filled with conduction oil in interlayer, interlayer;Two are provided with kettle cover Individual motor and it is configured with two sets of agitating shafts;One of a set of agitating shaft of Motor Control is rotated clockwise, another electricity Motivation controls another set of agitating shaft to rotate counterclockwise;Often being provided with set agitating shaft on stirring vane, stirring vane had Stirring vane on chute, and two motor is staggered;
Feed pipe, discharge nozzle, gas-adding pipe, blast pipe and relief tube are provided with reactor;
Loading hopper is provided with charging aperture, discharging opening is configured with filter;Gas-adding pipe is configured with high pressure gas holder, blast pipe Access condenser;
Flush pipe is provided with kettle cover, flush pipe is connected with the spray head being arranged on inside kettle cover, flush pipe access water storage Tank, water tank is connected with high pressure gas holder.
One of prioritization scheme of the present utility model, for the ease of conveying, is provided with universal wheel on support.
One of prioritization scheme of the present utility model, in order to strengthen sealing effectiveness, the upper end of reactor is provided with packing ring Sealing ring is provided with groove, gasket groove.
One of prioritization scheme of the present utility model, for the phase transformation during direct observing response or other feelings Condition, is provided with observation window on reactor.
One of prioritization scheme of the present utility model, in order to be provided with temperature sensor, temperature in the interlayer of reactor The signal of sensor is shown that the temperature sensor is mainly used in monitoring electricity and added by being arranged on the display on reactor surface The working condition of thermal.
One of prioritization scheme of the present utility model, for the ease of control, feed pipe of the present utility model, discharge nozzle, The pipeline connected on gas-adding pipe, blast pipe and relief tube is provided with valve.
One of prioritization scheme of the present utility model, can be in reactor in order to monitor the temperature in course of reaction Temperature sensor is set, and temperature sensor can be arranged on the bottom of reactor or side wall.
In summary, the utility model has advantages below:
Be provided with reactor of the present utility model two turn to different agitating shafts and be staggered paddle and Chute was disposed with, reaction mass mixing can be allowed more uniform;Simultaneous reactions kettle is also configured with condenser and filter, can Volatile gas is reclaimed and purification reaction thing.
Brief description of the drawings
Fig. 1 is the schematic diagram of the utility model one embodiment;
Fig. 2 is the top view of reactor in the utility model one embodiment;
Fig. 3 is the top view of kettle cover in the utility model one embodiment.
Wherein, 1, reactor;2nd, kettle cover;3rd, fixed card slot;4th, moving screw;5th, WING NUTS;6th, concave station;7th, it is electronic Machine;8th, agitating shaft;9th, stirring vane;10th, chute is crossed;11st, feed pipe;12nd, discharge nozzle;13rd, gas-adding pipe;14th, blast pipe;15、 Filter;16th, high pressure gas holder;17th, condenser;18th, flush pipe.
Embodiment
The utility model provides a kind of modified chemical reaction device, including reactor 1, and reactor is fixed on support On;Support is eliminated in Fig. 1.Support can design the height of support according to actual needs, and support can be according to reactor Size and weight selection install fixed form, for example can by the waistline of reactor set a belt type reinforcement Muscle, while the middle part of support sets a hole that reactor bottom can be allowed to enter, and allows reinforcement to be stuck on support, matches somebody with somebody simultaneously Part bolt or buckle is closed to realize fixation.It is preferred that installing universal wheel on support, universal wheel can be with auto lock, can also It is readily transported small-sized reactor.
Kettle cover 2 is provided with the top of reactor, the center section of kettle cover can install the platform of motor with outwardly convex formation, The EDGE CONTACT of most edge and reactor is sealed.Kettle cover it is cylindrical on be provided with some fixed card slots 3, this fixing card What groove was through, a moving screw being fixed on reactor 4 is each equipped with below each fixed card slot, moving screw One end is arranged on reactor and can freely rotated, for example, be arranged on by a removable pin on reactor.Moving screw 4 The other end is configured with WING NUTS 5, and WING NUTS is easy to rotation.In moving screw insertion fixed card slot, then by screwing butterfly Type nut is by reactor and kettle cover clamping;The upper end of fixed card slot is provided with a concave station 6, and concave station is entered during WING NUTS clamping It is interior, WING NUTS or so skidding in use can be avoided;So that reactor and kettle cover connection are closer.In order to further Strengthen sealing, the upper end of reactor, which is provided with gasket groove, gasket groove, is provided with sealing ring.
Observation window is provided with reactor, not shown in figure.Reactor, which also has in interlayer, interlayer, is provided with electrical heating dress Put and filled with conduction oil, the electric wire of electric heater unit can be heated after being connected with supply line to conduction oil so that Reactor temperature is raised.In order to detect the temperature in heating or course of reaction, it is provided with the interlayer of reactor Temperature sensor, the signal of temperature sensor is shown by being arranged on the display on reactor surface;Simultaneously in reactor Temperature sensor is inside provided with, reaction temperature is detected.
Two motor 7 are provided with kettle cover and two sets of agitating shafts 8 are configured with;One of Motor Control is a set of to be stirred Mix axle to rotate clockwise, the another set of agitating shaft of another Motor Control is rotated counterclockwise.Often it is provided with and stirs on set agitating shaft Mixing had chute 10 on blade 9, stirring vane, and the stirring vane on two motor is staggered.This place paddle Piece, which is staggered, can refer to that the stirring vane on two agitating shafts is misaligned in the axial direction, paddle each in the axial direction Two adjacent stirring vanes of piece are the stirring vane on another agitating shaft.
Feed pipe 11, discharge nozzle 12, gas-adding pipe 13, blast pipe 14 and relief tube are provided with reactor, can be distinguished Realize charging, discharging, aerating pressurization, exhaust and pressure release;Connect on feed pipe, discharge nozzle, gas-adding pipe, blast pipe and relief tube The pipeline connect is provided with valve.Further, loading hopper is provided with charging aperture, it is more to be easy in charging such as powder Easily, discharging opening is configured with filter 15, in input pans after can reactant be filtered;Gas-adding pipe is configured with high pressure gas holder 16, be easy to by reactant pass through out of filter by gases at high pressure, blast pipe access condenser 17, can be used for produce it is easy During reaction during volatilization gas.Flush pipe 18 is provided with kettle cover, flush pipe is connected with the spray head being arranged on inside kettle cover, rushed Pipe access water tank is washed, water tank is connected with high pressure gas holder.
Although being described in detail with reference to accompanying drawing to embodiment of the present utility model, it should not be construed as pair The restriction of the protection domain of this patent.In the scope described by claims, those skilled in the art are without creative labor The dynamic various modification and variation that can be made still belong to the protection domain of this patent.

Claims (7)

1. a kind of modified chemical reaction device, it is characterised in that:Including reactor, the reactor is fixed on support;Institute State and kettle cover be provided with the top of reactor, the kettle cover it is cylindrical on be provided with some fixed card slots, each fixed card slot Side is each equipped with a moving screw being fixed on reactor, and moving screw is configured with WING NUTS, and moving screw insertion is solid Determine reactor and kettle cover clamping in neck by WING NUTS;The upper end of the fixed card slot is provided with a concave station, butterfly-type Enter during nut clamping in concave station;
The reactor, which has in interlayer, the interlayer, is provided with electric heater unit and filled with conduction oil;On the kettle cover It is provided with two motor and is configured with two sets of agitating shafts;One of a set of agitating shaft of Motor Control is rotated clockwise, The another set of agitating shaft of another Motor Control is rotated counterclockwise;Often stirring vane, the stirring are provided with set agitating shaft There is the stirring vane on chute, and two motor to be staggered on blade;
Feed pipe, discharge nozzle, gas-adding pipe, blast pipe and relief tube are provided with the reactor;
Loading hopper is provided with the charging aperture, discharging opening is configured with filter;Gas-adding pipe is configured with high pressure gas holder, blast pipe Access condenser;
Flush pipe is provided with the kettle cover, flush pipe is connected with the spray head being arranged on inside kettle cover, the flush pipe access Water tank, the water tank is connected with high pressure gas holder.
2. modified chemical reaction device as claimed in claim 1, it is characterised in that:Universal wheel is installed on the support.
3. modified chemical reaction device as claimed in claim 1, it is characterised in that:The upper end of the reactor is provided with pad Sealing ring is provided with ring recess, gasket groove.
4. modified chemical reaction device as claimed in claim 1, it is characterised in that:Observation is provided with the reactor Window.
5. modified chemical reaction device as claimed in claim 1, it is characterised in that:It is provided with the interlayer of the reactor Temperature sensor, the signal of temperature sensor is shown by being arranged on the display on reactor surface.
6. modified chemical reaction device as claimed in claim 1, it is characterised in that:The feed pipe, discharge nozzle, aerating The pipeline connected on pipe, blast pipe and relief tube is provided with valve.
7. modified chemical reaction device as claimed in claim 1, it is characterised in that:Temperature biography is provided with the reactor Sensor.
CN201720361265.3U 2017-04-08 2017-04-08 A kind of modified chemical reaction device Expired - Fee Related CN206597541U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720361265.3U CN206597541U (en) 2017-04-08 2017-04-08 A kind of modified chemical reaction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720361265.3U CN206597541U (en) 2017-04-08 2017-04-08 A kind of modified chemical reaction device

Publications (1)

Publication Number Publication Date
CN206597541U true CN206597541U (en) 2017-10-31

Family

ID=60143850

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720361265.3U Expired - Fee Related CN206597541U (en) 2017-04-08 2017-04-08 A kind of modified chemical reaction device

Country Status (1)

Country Link
CN (1) CN206597541U (en)

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171031

Termination date: 20180408

CF01 Termination of patent right due to non-payment of annual fee