CN206587780U - Semimicro kelvin distiller - Google Patents

Semimicro kelvin distiller Download PDF

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Publication number
CN206587780U
CN206587780U CN201720273139.2U CN201720273139U CN206587780U CN 206587780 U CN206587780 U CN 206587780U CN 201720273139 U CN201720273139 U CN 201720273139U CN 206587780 U CN206587780 U CN 206587780U
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CN
China
Prior art keywords
ground
cucurbit
semimicro
distiller
branch pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720273139.2U
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Chinese (zh)
Inventor
回素敏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenyang Tenglong Glass Instrument Manufacturing Co Ltd
Original Assignee
Shenyang Tenglong Glass Instrument Manufacturing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenyang Tenglong Glass Instrument Manufacturing Co Ltd filed Critical Shenyang Tenglong Glass Instrument Manufacturing Co Ltd
Priority to CN201720273139.2U priority Critical patent/CN206587780U/en
Application granted granted Critical
Publication of CN206587780U publication Critical patent/CN206587780U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model is related to semimicro kelvin distiller.The semimicro kelvin distiller includes:Ground cucurbit, ground condenser pipe, the curved branch pipe with nitrogen ball, the cucurbit has interlayer set, cucurbit bottom is waste liquid outlet, cucurbit one end outer wall is provided with bottleneck branch pipe, the middle part outer wall of cucurbit is provided with the frosted cup with plug, and the curved branch pipe with nitrogen ball connects ground cucurbit and ground condenser pipe respectively.Easy to use using frosted plug at the semimicro kelvin distiller that the utility model is provided, its liquid feeding, it is adaptable to the micro semimicro between constant, with steam distillation, the content analysis for making nitrogen to organic matter is determined, and distillate purity is high.

Description

Semimicro kelvin distiller
Technical field
The utility model is related to semimicro kelvin distiller, more particularly to a kind of chemical analysis instrument.
Background technology
At present, semimicro distiller is determined by using steam distillation to the content analysis for making nitrogen to organic matter, but It is that nitrogen ball is not used when using steam distillation in existing semimicro distiller, so that the purity drop of distillate It is low.
Utility model content
The semimicro kelvin distiller provided for the drawbacks described above of prior art, the utility model, solves above-mentioned skill Art problem is high there is provided a kind of distillate purity, semimicro distiller easy to use.
In order to achieve the above object, the utility model provides following technical scheme:
Semimicro kelvin distiller includes:Ground cucurbit, ground condenser pipe, the curved branch pipe with nitrogen ball, the steaming Evaporating bottle has interlayer set, and cucurbit bottom is waste liquid outlet, and cucurbit one end outer wall is provided with outside bottleneck branch pipe, the middle part of cucurbit Wall is provided with the frosted cup with plug, and the curved branch pipe with nitrogen ball connects ground cucurbit and ground condenser pipe respectively.
Wherein, do not vacuumized between ground cucurbit and the interlayer set, be used as the passage of steam.
Wherein, the waste liquid outlet direction is straight down.
Wherein, the bottleneck branch pipe that described cucurbit one end outer wall is provided with is the entrance as steam.
Wherein, the frosted cup of the band plug is with clogging at the passage that frosted glass bottom is connected with ground cucurbit, try Liquid is entered by frosted cup, enters ground cucurbit by the passage of frosted cup and ground cucurbit.
Wherein, the nitrogen ball of the curved branch pipe with nitrogen ball improves the purity of distillate.
Wherein, the upper end of the ground condenser pipe is connected with the curved branch pipe with nitrogen ball through frosted.
Wherein, the tail end of the ground condenser pipe is inserted in the container for filling boric acid absorbing liquid, the boric acid absorbing liquid Holder absorption nitrogen.
Wherein, the ground cucurbit, the ground of ground condenser pipe use beam ground, the curved branch pipe with nitrogen ball with Ground cucurbit is integral type structure.
The beneficial effects of the utility model are:Used at the semimicro kelvin distiller that the utility model is provided, its liquid feeding Frosted plug is easy to use, it is adaptable to the micro semimicro between constant, with steam distillation, makees the content of nitrogen to organic matter Analysis is determined, and distillate purity is high.
In order to be able to be further understood that feature of the present utility model and technology contents, refer to new below in connection with this practicality The detailed description of type and accompanying drawing, however accompanying drawing only provide with reference to and explanation use, not for being any limitation as to the utility model.
Brief description of the drawings
Below in conjunction with the accompanying drawings, by the way that embodiment of the present utility model is described in detail, it will make of the present utility model Technical scheme and other beneficial effects are apparent.
Fig. 1 is the structural representation of the utility model semimicro kelvin distiller.
Embodiment
Further to illustrate technological means and its effect that the utility model is taken, below in conjunction with of the present utility model Preferred embodiment and its accompanying drawing are described in detail.
Referring to Fig. 1, semimicro kelvin distiller includes:Ground cucurbit 1, ground condenser pipe 2, with the curved of nitrogen ball Branch pipe 3, the cucurbit 1 has interlayer set 4, and the bottom of cucurbit 1 is waste liquid outlet 5, and one end outer wall of cucurbit 1 is provided with bottleneck branch Pipe 6, the middle part outer wall of cucurbit 1 is provided with the frosted cup 7 with plug, and the curved branch pipe with nitrogen ball connects ground distillation respectively Bottle 1 and ground condenser pipe 2.
Further, do not vacuumized between ground cucurbit 1 and the interlayer set 4, be used as the passage of steam.
Further, the direction of waste liquid outlet 5 is straight down.
Further, the bottleneck branch pipe 6 that one end outer wall of cucurbit 1 is provided with is the entrance as steam.
Further, the frosted cup 7 of the band plug is with clogging the passage that frosted glass bottom is connected with ground cucurbit 1 Place, test solution is entered by frosted cup 7, enters ground cucurbit 1 by the passage of frosted cup 7 and ground cucurbit 1.
Further, the nitrogen ball of the curved branch pipe 3 with nitrogen ball improves the purity of distillate.
Further, the upper end of the ground condenser pipe 2 is connected with the curved branch pipe 3 with nitrogen ball through frosted.
Further, the tail end of the ground condenser pipe 2 is inserted in the container for filling boric acid absorbing liquid, the boric acid absorbing liquid Holder absorption nitrogen.
Further, the ground cucurbit 1, the ground of ground condenser pipe 2 use beam ground, the curved branch with nitrogen ball Pipe 3 is integral type structure with ground cucurbit 1.
Moulding and principle
It is made up of ground cucurbit 1 and ground condenser pipe 2, cucurbit 1 also has interlayer set 4, but does not vacuumize but make For the passage of steam, the branch pipe below bottle wall is at waste liquid outlet 5, bottleneck branch pipe 6 is that have what band was filled on the entrance of steam, extra heavy pipe Frosted cup 7, test solution is exactly to be added from this cup, and the curved branch pipe 3 of tool nitrogen ball is connected with condenser pipe 2, and nitrogen ball is to improve distillation The purity of liquid is used, and the upper end of straight cold finger 2 is connected with distillation bottleneck 3 through frosted.Condenser pipe 2 be tail pipe be inserted in fill boric acid absorption (provided for oneself) in the container of liquid, be used as absorbed nitrogen.Because ground is more convenient to installation and renewal part using beam ground.
It is described above, embodiment only of the present utility model, but protection domain of the present utility model do not limit to In this, any one skilled in the art can readily occur in change in the technical scope that the utility model is disclosed Or replace, it should all cover within protection domain of the present utility model.Therefore, protection domain of the present utility model should be described with power The protection domain that profit is required is defined.

Claims (9)

1. semimicro kelvin distiller, it is characterised in that including:Ground cucurbit, ground condenser pipe, the curved branch with nitrogen ball Pipe, the cucurbit has interlayer set, and cucurbit bottom is waste liquid outlet, and cucurbit one end outer wall is provided with bottleneck branch pipe, distillation The middle part outer wall of bottle is provided with the frosted cup with plug, and the curved branch pipe with nitrogen ball connects ground cucurbit respectively and ground is cold Solidifying pipe.
2. semimicro kelvin distiller according to claim 1, it is characterised in that the ground cucurbit covers it with interlayer Between do not vacuumize, be used as the passage of steam.
3. semimicro kelvin distiller according to claim 1, it is characterised in that the waste liquid outlet direction for it is vertical to Under.
4. semimicro kelvin distiller according to claim 1, it is characterised in that described cucurbit one end outer wall is provided with Bottleneck branch pipe is the entrance as steam.
5. semimicro kelvin distiller according to claim 1, it is characterised in that the frosted cup of the band plug is with plug plug At the passage that firmly frosted cup bottom is connected with ground cucurbit, test solution is entered by frosted cup, passes through frosted cup and ground cucurbit Passage enter ground cucurbit.
6. semimicro kelvin distiller according to claim 1, it is characterised in that the curved branch pipe with nitrogen ball Nitrogen ball improves the purity of distillate.
7. semimicro kelvin distiller according to claim 1, it is characterised in that the upper end of the ground condenser pipe and band The curved branch pipe for having nitrogen ball is connected through frosted.
8. semimicro kelvin distiller according to claim 1, it is characterised in that the tail end of the ground condenser pipe is inserted in In the container for filling boric acid absorbing liquid, the holder absorption nitrogen of the boric acid absorbing liquid.
9. semimicro kelvin distiller according to claim 1, it is characterised in that the ground cucurbit, ground condensation The ground of pipe uses beam ground, and the curved branch pipe with nitrogen ball is integral type structure with ground cucurbit.
CN201720273139.2U 2017-03-20 2017-03-20 Semimicro kelvin distiller Expired - Fee Related CN206587780U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720273139.2U CN206587780U (en) 2017-03-20 2017-03-20 Semimicro kelvin distiller

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720273139.2U CN206587780U (en) 2017-03-20 2017-03-20 Semimicro kelvin distiller

Publications (1)

Publication Number Publication Date
CN206587780U true CN206587780U (en) 2017-10-27

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720273139.2U Expired - Fee Related CN206587780U (en) 2017-03-20 2017-03-20 Semimicro kelvin distiller

Country Status (1)

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CN (1) CN206587780U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109959608A (en) * 2017-12-25 2019-07-02 中核建中核燃料元件有限公司 A kind of nitrogen auto analyzer digest tube processing method
CN111855381A (en) * 2020-08-13 2020-10-30 郭喜丰 Continuous distillation device suitable for detecting large-batch samples

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109959608A (en) * 2017-12-25 2019-07-02 中核建中核燃料元件有限公司 A kind of nitrogen auto analyzer digest tube processing method
CN111855381A (en) * 2020-08-13 2020-10-30 郭喜丰 Continuous distillation device suitable for detecting large-batch samples

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171027