CN206587741U - It is a kind of that there is the reactor for being separated by filtration washing function - Google Patents
It is a kind of that there is the reactor for being separated by filtration washing function Download PDFInfo
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- CN206587741U CN206587741U CN201621373613.0U CN201621373613U CN206587741U CN 206587741 U CN206587741 U CN 206587741U CN 201621373613 U CN201621373613 U CN 201621373613U CN 206587741 U CN206587741 U CN 206587741U
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Abstract
The utility model is related to a kind of reactor for having and being separated by filtration washing function, including kettle, and outside is provided with chuck to be passed through heating agent, motor, filter is connected with filtering mouthful below the agitating device that lower section connection is extend into kettle, kettle, the bottom of kettle is connected with exhibition valve.Compared with prior art, the utility model can be used for the endothermic reaction, realize good separation of solid and liquid, reaction, filtering and isolation integral so that course of reaction is efficiently completed in closed environment.
Description
Technical field
The utility model is related to field of chemical equipment, more particularly, to a kind of reaction for having and being separated by filtration washing function
Kettle.
Background technology
In chemical reaction field, the reaction of separation of solid and liquid is frequently encountered, whole course of reaction will be under closed environment sometimes
Carry out, otherwise reaction effect can be restricted, filtering and separation process need to also be completed in reactor, and can be according to technique need
Ask in closed environment so that liquid and solid are separated from reactor into respective next workshop section respectively, use tradition
Reactor can not complete this class process, the consersion unit operation that can complete this kind of process is often complicated, and that introduces herein is anti-
Device is answered to make up this defect of traditional reactor, and it is easy to operate.
In addition, consersion unit general structure is more complicated, cleaning is inconvenient；Dead angle is easily produced in whipping process, especially
It also easily causes stirring material deposition, cleans not thorough enough, subsequent material is stirred for high viscosity liquid after liquid discharge
Mix generation influence.
Chinese patent CN204017840U discloses a kind of reactor for collecting reaction washing and filtering one, belongs to chemical reaction
A kind of engineering device technique field, and in particular to improvement of polyolefin catalyst synthetic reaction device.Transfer time can be reduced by providing one kind
Number, shortens the production time, improves filter efficiency, reduces catalyst loss, and then the reaction washing improved product quality and yield
Filtration integrated reactor, but the patent can not realize the good separation between solid-liquid.
Utility model content
The purpose of this utility model is exactly the defect in order to overcome above-mentioned prior art presence and provides one kind and can be used for inhaling
Thermal response, realize that having for good separation of solid and liquid is separated by filtration the reactor of washing function.
The purpose of this utility model can be achieved through the following technical solutions：
It is a kind of have be separated by filtration the reactor of washing function, including
Kettle, outside is provided with chuck to be passed through heating agent,
Motor, the agitating device that lower section connection is extend into kettle,
Filter is connected with filtering mouthful below described kettle, the bottom of kettle is connected with exhibition valve.
Described upper exhibition valve is made up of rotation hand wheel, valve rod and valve body, and turn rotation hand wheel control valve rod is driven on valve body
Lower movement, separation of solid and liquid is realized by the cooperation of filter and upper exhibition valve：Upper exhibition valve is closed, and opens the ball below filter
Valve, liquid discharge；Close all ball valves, turn handwheel, which is opened, to be opened up solidliquid mixture in valve, kettle kettle can be discharged out of kettle,
So as to realize separation of solid and liquid.The part is mainly used in reactor, the bottom discharging of storage tank and other containers, blowing, sampling and nothing
Dead band shut-off operation, turn handwheel can control moving up and down for valve body by valve rod, and the solid material above valve body is with a small amount of liquid
Body can flow out from bottom, by operating ball valve and upper exhibition valve below visor, realize that solid-liquid material flows out from reactor respectively,
Reach the purpose of separation of solid and liquid.
Described filter is made up of flange, filter, filter cloth, fixed card slot and visor,
Described flange is located at the filtering mouthful lower section of end socket below kettle to connect kettle and visor,
Described filter is located between flange and visor, and filter is provided with equally distributed hole, can be according to solids
The particle diameter of material carries out the filter of selection different meshes,
Described filter cloth is fixed on filter, can be selected and changed not according to the particle diameter of solid material
The filter cloth of same specification,
The lower section of described visor sets ball valve, is passed in and out by switching control liquid material.
Solid-liquid discharging can be realized by the switching of exhibition valve in control and the ball valve different time below visor, can so be ensured
Separation of solid and liquid is realized in the closed environment of reactor.
The edge of described filter is O-ring seal, to ensure when liquid material is released, and solid material will not be with
Liquid material flows out.
Hydraulic barrier is provided with described kettle, strengthens mixing effect, solid material deposition bottom dead angle position is reduced.
The entrance for being respectively equipped with heat transferring medium over and under of described chuck and outlet.
Entrance and the outlet of inert gas are additionally provided with above described kettle.
, can be in the comprehensive universal cleaning of evaporator of any angle also with 360 degree of rotating wash bowls in described kettle.
Described motor is variable ratio frequency changer fire-proof motor.
Compared with prior art, the utility model has advantages below：
(1) important advantage of the present utility model is can realize reaction, washing and separation of solid and liquid in closed environment, and operate
Simply, need to be heated to certain temperature based on material in project could react Gu expression available for the endothermic reaction, if running into heat release
Also can it react, only need to be toward same such as refrigerant in kettle external jacket, available for the endothermic reaction；
(2) separation of liquid material and solid material is realized in environment closed in reactor, and smoothly by liquid
The discharge reactor of body material and solid material respectively, reaction, filtering and isolation integral so that course of reaction is in closed environment
In efficiently complete；
(3) by being equipped with agitating device, hydraulic barrier and chuck so that the reactor possesses scattered and heat exchange work(
Can, the multifunctionality of enhanced equipment.
(4) after the completion of reacting, device interior is effectively cleaned using 360 degree of self-cleaning balls, stockpiling for material is prevented,
In order to subsequent operation.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
In figure, 1- kettlies, 2- chucks, 3- heat transferring mediums outlet, 4- filters, 5- ball valves, 6- is filtered and opened up on mouth, 7-
Valve, 8- visors, 9- heat transferring medium entrances, 10- liquid material entrances, 11-360 degree rotating wash bowls, 12- solid material inlets, 13- electricity
Machine, 14- inert gas entrances, 15- inert gas outlets, 16- manholes, 17- agitators, 18- hydraulic barriers.
Embodiment
The utility model is described in detail with specific embodiment below in conjunction with the accompanying drawings.Following examples will be helpful to this
The technical staff in field further understands the utility model, but does not limit the utility model in any form.It should be pointed out that
To those skilled in the art, without departing from the concept of the premise utility, some deformations can also be made
And improvement.These belong to protection domain of the present utility model.
Embodiment 1
It is a kind of that there is the reactor for being separated by filtration washing function, its structure as shown in figure 1, including kettle 1, chuck 2, stirring
The components such as device 17, hydraulic barrier 18, filter 4, upper exhibition valve 7.Chuck 2 is used for being passed through heating agent, in chuck 2 over and under
Heat transferring medium entrance 9 and heat transferring medium outlet 3 are respectively equipped with, motor 13 is variable ratio frequency changer fire-proof motor, and lower section connection extend into kettle
Filter 4 is connected with agitator 17 in body 1, the filtering mouthful 6 of the lower section of kettle 1, the bottom of kettle 1 is connected with exhibition valve 7.
Upper exhibition valve is made up of rotation hand wheel, valve rod and valve body, and turn rotation hand wheel control valve rod drives valve body to move up and down.
The part is mainly used in reactor, the bottom discharging of storage tank and other containers, blowing, sampling and turns off operation, turn without dead band
Handwheel can control moving up and down for valve body by valve rod, and the solid material above valve body can flow out with a small amount of liquid from bottom, lead to
The ball valve and upper exhibition valve crossed below operation visor, realize that solid-liquid material flows out from reactor respectively, reach the mesh of separation of solid and liquid
's.
Filter 4 is made up of flange, filter, filter cloth, fixed card slot and visor 8, and flange is located at the lower section of kettle 1 and sealed
The lower section of filtering mouthful 6 of head is to connect kettle 1 and visor 8, and filter is located between flange and visor, and filter is provided with uniform point
The hole of cloth, according to the particle diameter of solid material can select the filter of different meshes, and filter cloth is fixed on filter,
The filter cloth of different size can be selected and changed according to the particle diameter of solid material, and the lower section of visor 8 sets ball valve
5, passed in and out by switching control liquid material.
Solid-liquid discharging can be realized by the switching for the ball valve different time that valve 7 and the lower section of visor 8 are opened up in control, can so be protected
Card realizes separation of solid and liquid in the closed environment of reactor.The edge of filter is O-ring seal, to ensure in liquid material
During releasing, solid material will not flow out with liquid material.
Hydraulic barrier 18 is provided with kettle 1, mixing effect can be strengthened, solid material deposition bottom dead angle position is reduced
Put.The top of kettle 1 is additionally provided with inert gas entrance 14, inert gas outlet 15, liquid material entrance 10, solid material inlet
12nd, manhole 16, can be in the comprehensive universal cleaning of evaporator of any angle also with 360 degree of rotating wash bowls 11 in kettle 1.
Embodiment 2
By taking the load titanium reaction in polypropylene catalyst preparation process as an example, the course of reaction will carry out carrying titanium twice or repeatedly
Reaction, the utility model device fully can provide facility for it, illustrate structure of the present utility model and operation principle.
Being passed through inertia by inert gas entrance first into kettle protects gas nitrogen to be purged, and nitrogen passes through indifferent gas
Body outlet discharge kettle, to ensure that course of reaction is carried out in closed oxygen-free environment.Added by liquid inlet opening into reactor
Enter titanium tetrachloride, open motor, agitator is stirred in advance under the drive of motor to material, by solid material inlet to anti-
Answer and carrier is added in kettle, adjust the speed of service of motor so that solid-liquid material is well mixed, and steam then is passed through into heat transferring medium
Entrance is passed through chuck, to be slowly heated to solidliquid mixture, and control steam flow causes solidliquid mixture to be warming up to necessarily
Temperature, now, adds another solid material electron donor, steam condensate is exported by heat transferring medium to flow out；Titanium is carried for the first time
After reaction, opening top has the ball valve of filter, and liquid material passes through filter, warp by by filtering mouth
Outside ball valve discharge kettle, solid material is trapped within above filter；Carry out second and carry titanium reaction, pass through liquid inlet opening
The titanium tetrachloride being preheated is added, stirring is opened, carries out carrying titanium reaction a period of time, after reaction, repeats the above steps, beat
Opening ball valve so that liquid material flows out kettle；Carry after the completion of titanium reaction, inert media hexane be passed through by liquid material entrance,
Stirring is opened, reacted material is washed, is repeated the above steps after a period of time and liquid is released kettle, it is so several
It is secondary, the effect washed to reaction mass is reached, closing top has now opens up valve hand wheel in the ball valve of filter, rotation so that
Flap rises, and solid material can flow out kettle by upper exhibition valve outlet under gravity, if solid material could not be whole
Outflow, can inject inert media by the ball valve below filter, and the solid material remained on filter is rinsed up,
And then operated by upper exhibition valve outlet into next workshop section.After reaction is completed and is delivered to next workshop section, 360 degree of cleanings are utilized
Ball is cleaned to kettle.
Specific embodiment of the utility model is described above.It is to be appreciated that the utility model not office
It is limited to above-mentioned particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims,
This has no effect on substantive content of the present utility model.
Claims (8)
1. it is a kind of with the reactor for being separated by filtration washing function, including
Kettle, outside is provided with chuck to be passed through heating agent,
Motor, the agitating device that lower section connection is extend into kettle,
Characterized in that, being connected with filter at filtering below described kettle mouthful, the bottom of kettle is connected with exhibition valve；
Described filter is made up of flange, filter, filter cloth, fixed card slot and visor,
Described flange is located at the filtering mouthful lower section of end socket below kettle to connect kettle and visor,
Described filter is located between flange and visor, and filter is provided with equally distributed hole,
Described filter cloth is fixed on filter,
The lower section of described visor sets ball valve, is passed in and out by switching control liquid material.
2. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described is upper
Exhibition valve is made up of rotation hand wheel, valve rod and valve body, and turn rotation hand wheel control valve rod drives valve body to move up and down.
3. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described mistake
The edge of filter plate is O-ring seal.
4. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described kettle
Hydraulic barrier is provided with vivo.
5. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described folder
The entrance and the outlet that are respectively equipped with heat transferring medium over and under of set.
6. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described kettle
Entrance and the outlet of inert gas are additionally provided with above body.
7. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described kettle
In vivo also with 360 degree of rotating wash bowls.
8. it is according to claim 1 a kind of with the reactor for being separated by filtration washing function, it is characterised in that described electricity
Machine is variable ratio frequency changer fire-proof motor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621373613.0U CN206587741U (en) | 2016-12-14 | 2016-12-14 | It is a kind of that there is the reactor for being separated by filtration washing function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621373613.0U CN206587741U (en) | 2016-12-14 | 2016-12-14 | It is a kind of that there is the reactor for being separated by filtration washing function |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206587741U true CN206587741U (en) | 2017-10-27 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621373613.0U Active CN206587741U (en) | 2016-12-14 | 2016-12-14 | It is a kind of that there is the reactor for being separated by filtration washing function |
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| CN (1) | CN206587741U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108579167A (en) * | 2018-07-03 | 2018-09-28 | 江苏中伟机械制造有限公司 | A kind of solid-liquid separation device |
| CN111715164A (en) * | 2020-05-29 | 2020-09-29 | 国家能源集团宁夏煤业有限责任公司 | Reaction kettle |
| CN111871345A (en) * | 2020-06-10 | 2020-11-03 | 成都思达能环保设备有限公司 | Reactor retrofit method for carrying out reactions and filtration concentration |
-
2016
- 2016-12-14 CN CN201621373613.0U patent/CN206587741U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108579167A (en) * | 2018-07-03 | 2018-09-28 | 江苏中伟机械制造有限公司 | A kind of solid-liquid separation device |
| CN111715164A (en) * | 2020-05-29 | 2020-09-29 | 国家能源集团宁夏煤业有限责任公司 | Reaction kettle |
| CN111871345A (en) * | 2020-06-10 | 2020-11-03 | 成都思达能环保设备有限公司 | Reactor retrofit method for carrying out reactions and filtration concentration |
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