CN206566537U - A kind of rectifying device of low boiling or volatile liquid - Google Patents
A kind of rectifying device of low boiling or volatile liquid Download PDFInfo
- Publication number
- CN206566537U CN206566537U CN201720289499.1U CN201720289499U CN206566537U CN 206566537 U CN206566537 U CN 206566537U CN 201720289499 U CN201720289499 U CN 201720289499U CN 206566537 U CN206566537 U CN 206566537U
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- China
- Prior art keywords
- low boiling
- tower body
- volatile liquid
- rectifying device
- fixedly connected
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model is related to rectifying device technical field, and disclose the rectifying device of a kind of low boiling or volatile liquid, including mounting seat, the inside of mounting seat is installed with distribution box, the top of distribution box is fixedly mounted on the inside of having heaters, heater and is installed with the muff being provided with the outside of tower body, tower body bottom positioned at mounting seat upper surface, the inside of tower body is fixedly connected with active carbon layer, and the upper surface of active carbon layer is fixedly connected with zeolite packed layer.The low boiling or volatile liquid rectifying device are provided with sealing device, low boiling extraction passage in sealing device is produced to the good low boiling of rectifying or volatile raw material, in the incipient stage of rectifying, valve in low boiling extraction passage is closed, if a small amount of raw material overflows, raw material can be also stored temporarily in annular seal space, substantially increase the sealing effectiveness of the rectifying device of the low boiling or volatile liquid.
Description
Technical field
The utility model is related to rectifying device technical field, and the rectifying of specially a kind of low boiling or volatile liquid is set
It is standby.
Background technology
In the fields such as medicine, medical treatment, organic chemistry, the compound containing chiral gamma-butyrolactone structure is occupied to be weighed very much
The status wanted, because the compound containing chiral gamma-butyrolactone often shows preferable bioactivity.Chiral or achirality
Gamma-butyrolacton just belongs to the liquid of low boiling and highly volatile, finally needs to carry out crude product rectifying just in process of production
Can purifying.
Rectifying is a kind of distillating method for making liquid mixture obtain high-purity separation using flowing back, and is industrial apply most
Wide liquid mixture lock out operation, is widely used in the departments such as oil, chemical industry, light industry, food, metallurgy.Existing rectifying device
Respectively there is excellent lack when carrying out rectifying to low boiling or volatile liquid, it would be desirable to which a kind of rate of recovery is higher, lose smaller
Rectifying device, this be accomplished by further improve rectifying device sealing property, therefore, we have proposed this new low boiling
The rectifying device of point or volatile liquid.
Utility model content
(1) technical problem solved
In view of the shortcomings of the prior art, the utility model provides the rectifying device of a kind of low boiling or volatile liquid,
Possess sealing effectiveness more preferable advantage during for low boiling or volatile liquid rectifying, solve existing equipment sealing inadequate
The problem of good.
(2) technical scheme
For realize it is above-mentioned be directed to low boiling or volatile liquid rectifying when the more preferable purpose of sealing effectiveness, the utility model
Following technical scheme is provided：A kind of rectifying device of low boiling or volatile liquid, including mounting seat, the inside of the mounting seat
Distribution box is installed with, the top of the distribution box, which is fixedly mounted on the inside of having heaters, the heater, to be installed with
The muff positioned at mounting seat upper surface is provided with the outside of tower body, the tower body bottom, the inside of the tower body is fixedly connected
Active layer of charcoal, the upper surface of the active carbon layer is fixedly connected with zeolite packed layer, and the outside on the tower body top, which is fixed, to be connected
Division board is connected to, side of the division board away from tower body is fixedly connected with placement plate, and peace is fixed in the upper surface of the placement plate
Equipped with condenser, the output end of the condenser is fixedly connected with condenser pipe, and the one end of the condenser pipe away from condenser is fixed
The top inside tower body is connected to, the top of the tower body is fixedly connected with sealing device, and the sealing device includes low boiling
Passage is produced, the top of the low boiling extraction passage is fixedly connected with encryption pipe, and the inside of the encryption pipe offers sealing
Chamber, the top of the encryption pipe is provided with sealing-plug.
It is preferred that, low boiling extraction passage is internally provided with valve.
It is preferred that, the muff is ceramics.
It is preferred that, the surface of the sealing-plug is provided with barrier film.
It is preferred that, the quantity of the zeolite packed layer is three, and three zeolite packed layers are successively set on inside tower body
Both sides.
It is preferred that, the shape of the heater is adapted with the shape of tower body bottom.
(3) beneficial effect
Compared with prior art, the utility model provides the rectifying device of a kind of low boiling or volatile liquid product,
Possesses following beneficial effect：
1st, the rectifying device of the low boiling or volatile liquid, by setting the low boiling in sealing device, sealing device
Extraction passage is produced to the good low boiling of rectifying or volatile liquid, in the incipient stage of rectifying, low boiling extraction passage
In valve close, if a small amount of liquid overflows, the liquid of spilling can be also stored temporarily in annular seal space, substantially increase this
The sealing effectiveness of the rectifying device of low boiling or volatile liquid, the loss of fluid product is further reduced.
2nd, the rectifying device of the low boiling or volatile liquid, by setting muff, due to low boiling or volatile
Liquid requires higher to temperature controlled, and muff can ensure the stability of heating-up temperature, will not be influenceed by external environment,
So as to ensure that the practicality of the rectifying device of the low boiling or volatile liquid.
Brief description of the drawings
Fig. 1 is the utility model structural representation；
Fig. 2 is the utility model schematic diagram of sealing device.
In figure：1 mounting seat, 2 distribution boxs, 3 heaters, 4 muffs, 5 tower bodies, 6 active carbon layers, 7 zeolite packed layers, 8 every
Plate, 10 condensers, 11 condenser pipes, 12 sealing devices, 121 low boilings extraction passage, 122 encryption pipes, 123 sealings are placed from plate, 9
Chamber, 124 sealing-plugs.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is carried out
Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the utility model, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belongs to the scope of the utility model protection.
Refer to Fig. 1-2, a kind of rectifying device of low boiling or volatile liquid, including mounting seat 1, mounting seat 1 it is interior
Portion is installed with distribution box 2, and having heaters 3, shape and the bottom of tower body 5 of heater 3 is fixedly mounted in the top of distribution box 2
Shape is adapted, and the inner side of heater 3, which is installed with the outside of tower body 5, the bottom of tower body 5, to be provided with positioned at the upper table of mounting seat 1
The muff 4 in face, muff 4 is ceramics, by setting muff 4, because low boiling or volatile liquid are to temperature control
Requirement it is higher, muff 4 can ensure the stability of heating-up temperature, will not be influenceed by external environment, so as to ensure that this
The practicality of the rectifying device of low boiling or volatile liquid, the inside of tower body 5 is fixedly connected with active carbon layer 6, active carbon layer 6
Upper surface be fixedly connected with zeolite packed layer 7, the quantity of zeolite packed layer 7 is three, and three zeolite packed layers 7 are set gradually
Division board 8 is fixedly connected with the outside of both sides inside tower body 5, the top of tower body 5, side of the division board 8 away from tower body 5 is fixed
Placement plate 9 is connected with, the upper surface for placing plate 9 is installed with condenser 10, the output end of condenser 10 is fixedly connected with cold
Solidifying pipe 11, the one end of condenser pipe 11 away from condenser 10 is fixedly connected on the top inside tower body 5, and the top of tower body 5, which is fixed, to be connected
Sealing device 12 is connected to, sealing device 12 includes low boiling and produces passage 121, and low boiling produces being internally provided with for passage 121
Valve, the top of low boiling extraction passage 121 is fixedly connected with encryption pipe 122, and the inside of encryption pipe 122 offers annular seal space
123, encryption pipe 122 top be provided with sealing-plug 124, the surface of sealing-plug 124 is provided with barrier film, prevent sealing-plug 124 with
The raw material of rectifying reacts, good to rectifying by setting the low boiling in sealing device 12, sealing device 12 to produce passage 121
Low boiling or volatile raw material produced, in the incipient stage of rectifying, the valve in low boiling extraction passage 121 is closed,
If a small amount of raw material overflows, raw material can be also stored temporarily in annular seal space 123, substantially increase the low boiling or volatile liquid
The sealing effectiveness of the rectifying device of body.
The electric elements occurred in this article are electrically connected with extraneous main controller and 220V civil powers, and main controller can be meter
Calculation machine etc. plays the conventionally known equipment of control.
In summary, the rectifying device of the low boiling or volatile liquid, by setting sealing device 12, sealing device 12
In low boiling extraction passage 121 the good low boiling of rectifying or volatile liquid are produced, it is low in the incipient stage of rectifying
Valve in boiling point extraction passage 121 is closed, and if a small amount of liquid overflows, can be also stored temporarily in annular seal space 123, thus
Significantly improve the sealing effectiveness of the low boiling or volatile liquid rectifying device.
The rectifying device of the low boiling or volatile liquid, by setting muff 4, due to low boiling or volatile liquid
Body requires higher to temperature controlled, and muff 4 can ensure the stability of heating-up temperature, will not be influenceed by external environment,
So as to ensure that the practicality of the rectifying device of the low boiling or volatile liquid.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating
In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to
Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those
Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Also there is other identical element in process, method, article or equipment including the key element.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art,
It is appreciated that these embodiments can be carried out in the case where not departing from principle of the present utility model and spirit a variety of changes, repaiies
Change, replace and modification, scope of the present utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. the rectifying device of a kind of low boiling or volatile liquid, including mounting seat (1), it is characterised in that：The mounting seat (1)
Inside be installed with distribution box (2), having heaters (3), the heater is fixedly mounted in the top of the distribution box (2)
(3) guarantor being provided with the outside of tower body (5), tower body (5) bottom positioned at mounting seat (1) upper surface is installed with the inside of
Temperature set (4), the inside of the tower body (5) is fixedly connected with active carbon layer (6), and the upper surface of the active carbon layer (6), which is fixed, to be connected
It is connected on the outside of zeolite packed layer (7), tower body (5) top and is fixedly connected with division board (8), the division board (8) is remote
The side of tower body (5) is fixedly connected with placement plate (9), and the upper surface for placing plate (9) is installed with condenser (10), institute
The output end for stating condenser (10) is fixedly connected with condenser pipe (11), and the one end of the condenser pipe (11) away from condenser (10) is consolidated
Surely the internal top of tower body (5) is connected to, the top of the tower body (5) is fixedly connected with sealing device (12), the sealing dress
Putting (12) includes low boiling extraction passage (121), and the top of the low boiling extraction passage (121) is fixedly connected with encryption pipe
(122), the inside of the encryption pipe (122) offers annular seal space (123), and the top of the encryption pipe (122) is provided with sealing
Fill in (124).
2. the rectifying device of a kind of low boiling according to claim 1 or volatile liquid, it is characterised in that：The low boiling
That puts extraction passage (121) is internally provided with valve.
3. the rectifying device of a kind of low boiling according to claim 1 or volatile liquid, it is characterised in that：The insulation
It is ceramics to cover (4).
4. the rectifying device of a kind of low boiling according to claim 1 or volatile liquid, it is characterised in that：The sealing
The surface of plug (124) is provided with barrier film.
5. the rectifying device of a kind of low boiling according to claim 1 or volatile liquid, it is characterised in that：The zeolite
The quantity of packed layer (7) is three, and three zeolite packed layers (7) are successively set on the internal both sides of tower body (5).
6. the rectifying device of a kind of low boiling according to claim 1 or volatile liquid, it is characterised in that：The heating
The shape of device (3) is adapted with the shape of tower body (5) bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720289499.1U CN206566537U (en) | 2017-03-23 | 2017-03-23 | A kind of rectifying device of low boiling or volatile liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720289499.1U CN206566537U (en) | 2017-03-23 | 2017-03-23 | A kind of rectifying device of low boiling or volatile liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206566537U true CN206566537U (en) | 2017-10-20 |
Family
ID=60055003
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720289499.1U Expired - Fee Related CN206566537U (en) | 2017-03-23 | 2017-03-23 | A kind of rectifying device of low boiling or volatile liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206566537U (en) |
-
2017
- 2017-03-23 CN CN201720289499.1U patent/CN206566537U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171020 Termination date: 20210323 |