CN206549651U - A kind of fixed reactor - Google Patents

A kind of fixed reactor Download PDF

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Publication number
CN206549651U
CN206549651U CN201720179799.4U CN201720179799U CN206549651U CN 206549651 U CN206549651 U CN 206549651U CN 201720179799 U CN201720179799 U CN 201720179799U CN 206549651 U CN206549651 U CN 206549651U
Authority
CN
China
Prior art keywords
housing
agitating shaft
cavity
stirring vane
fixed reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720179799.4U
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Chinese (zh)
Inventor
丁文超
马林玉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sichuan Shehong General Medical Instrument Co Ltd
Original Assignee
Sichuan Shehong General Medical Instrument Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sichuan Shehong General Medical Instrument Co Ltd filed Critical Sichuan Shehong General Medical Instrument Co Ltd
Priority to CN201720179799.4U priority Critical patent/CN206549651U/en
Application granted granted Critical
Publication of CN206549651U publication Critical patent/CN206549651U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The utility model discloses a kind of fixed reactor, including housing, motor, agitating shaft and cooling coil;Cooling coil, which suspends, is located at housing inner bottom part, agitating shaft is located in housing, the stirring vane of helically type is distributed with agitating shaft, puddler is welded with stirring vane, the top of agitating shaft is connected by swivel joint with feed tube, the first cavity is provided with agitating shaft, agitating shaft bottom is provided with some first fluid holes, and the first fluid hole is connected with cavity;Housing includes housing upper and lower housing portion, and housing upper is sealed with lower housing portion clamping and locked by retaining mechanism, and housing upper end is provided with charge door, and bottom is provided with discharging opening, and having heaters and temperature sensor are installed in inside;Temperature sensor with alarm located at hull outside is connected located at enclosure interior and by lead by feeler lever.The utility model adds mixability between solvent, ensure that synthesis procedure efficiently and stably runs and added the mixing effect of solvent.

Description

A kind of fixed reactor
Technical field
The utility model is related to chemical field, and in particular to a kind of fixed reactor.
Background technology
Because a variety of chemical changes of chemical enginnering process are premised on participating in being sufficiently mixed of the medium of reaction, to need Using stirring operation, more preferable effect could be obtained, reactor is a kind of mixing being used in production process, anti- It should wait in the pressure vessels for the chemical industry of one, it is widely used in the industries such as chemical industry, food, medicine, resins synthesis.Existing reactor leads to Often include reactor body, agitating shaft and stirring vane, agitating shaft is located in reactor, and coaxially connected with reactor body, Stirring vane Spiral distribution is on agitating shaft.Each solvent of the inside is mixed by agitating shaft, then reactor entered again Trip temperature is controlled, and is generally all heated to certain temperature, after the reaction condition for reaching solvent, and solvent starts reaction.However, only There is provided mixing not uniform enough between agitating device, solvent, cause there are many raw materials not react completely, anyway effect is poor, Cause the waste of resource.
Utility model content
The purpose of this utility model is to provide a kind of fixed reactor, adds the mixability between solvent, ensures Run and add to synthesis procedure efficient stable high-quality the mixing effect of solvent.
For up to above-mentioned purpose, the technical scheme that the utility model is used is:A kind of fixed reactor, including shell are provided Body, motor, agitating shaft and the cooling coil for being arranged on housing inner bottom part;Cooling coil, which suspends, is located at housing inner bottom part, stirring Axle position is and coaxially connected with housing in housing, is distributed with the stirring vane of helically type, stirring vane and welds on agitating shaft There is puddler, the top of agitating shaft is connected by swivel joint with feed tube, the first cavity, agitating shaft bottom are provided with agitating shaft Provided with some first fluid holes, the first fluid hole is connected with cavity;Housing include housing upper and lower housing portion, housing upper with Lower housing portion clamping is sealed and locked by retaining mechanism, and housing upper end is provided with charge door, and bottom is provided with discharging opening, and inside is installed Having heaters and temperature sensor;Temperature sensor is by feeler lever located at enclosure interior and by lead with being located at hull outside Alarm is connected.
It is preferred that, the second cavity is provided with stirring vane, the second cavity is connected with the first cavity, stirring vane provided with Second fluid hole of the second cavity connection.
It is preferred that, swivel joint is single loop swivel joint.
It is preferred that, retaining mechanism includes being arranged on the upper latch segment of housing upper lower end outside and is arranged on lower housing portion Lower latch segment on the outside of upper end, upper latch segment is equal with lower locking number of blocks, and provided with use between upper latch segment and lower latch segment In both clamping screws of locking.
It is preferred that, the top of housing is provided with the support for installing motor, and lower end is provided with support frame.
It is preferred that, housing upper lower surface is provided with a circle spacing preiection, and lower housing portion upper surface is provided with a circle for limit The limited impression of the raised embedded clamping in position, and a circle sealing ring is additionally provided between spacing preiection and limited impression.
In summary, the utility model has advantages below:
1st, this programme is by setting swivel joint, while ensureing that agitating shaft is rotated, can also be toward addition in agitating shaft Solvent.Due to solvent of the agitating shaft in rotary state, agitating shaft under the influence of centrifugal force, so as to be thrown out of agitating shaft, Enter in cavity can be with adding before solvent fully react, add the mixability between solvent, reduce resource Waste.
2nd, fixed reactor of the present utility model has temperature monitoring and warning function, improves the effect of operating personnel Rate, it is ensured that run to synthesis procedure efficient stable high-quality.
3rd, by the way that puddler is fixed on rotating vane, the stirring effect of fixed reactor internal solvent can further be increased Really.
Brief description of the drawings
Fig. 1 is the schematic diagram of the utility model fixed reactor;
Wherein, 1, housing upper;2nd, lower housing portion;3rd, motor;4th, support;5th, swivel joint;6th, lead;7th, feed tube; 8th, charge door;9th, alarm;10th, agitating shaft;11st, feeler lever;12nd, temperature sensor;13rd, clamping screw;14th, upper latch segment;15、 Lower latch segment;16th, sealing ring;17th, heater;18th, stirring vane;19th, the first fluid hole;20th, puddler;21st, cooling coil; 22nd, discharging opening;23rd, support frame.
Embodiment
Embodiment of the present utility model is described in detail below in conjunction with the accompanying drawings.
In one embodiment of the present utility model, as shown in Figure 1 there is provided a kind of fixed reactor, including housing, electricity Machine 3, agitating shaft 10 and the cooling coil 21 for being arranged on housing inner bottom part;Cooling coil 21, which suspends, is located at housing inner bottom part, stirs Axle 10 is mixed in housing, and it is coaxially connected with housing, the stirring vane 18 of helically type, paddle are distributed with agitating shaft 10 Puddler 20 is welded with piece 18, the top of agitating shaft 10 is connected with feed tube 7 by swivel joint 5, is provided with agitating shaft 10 First cavity, the bottom of agitating shaft 10 is provided with some first fluid holes 19, and the first fluid hole 19 is connected with cavity;Housing includes housing Top 1 and lower housing portion 2, housing upper 1 are sealed with the clamping of lower housing portion 2 and locked by retaining mechanism, and housing upper end is provided with Charge door 8, bottom is provided with discharging opening 22, and having heaters 17 and temperature sensor 12 are installed in inside;Temperature sensor 12 is by visiting Bar 11 with alarm 9 located at hull outside is connected located at enclosure interior and by lead 6.
The second cavity is provided with optimal enforcement example of the present utility model, stirring vane 18, the second cavity and the first cavity connect Logical, stirring vane 18 is provided with the second fluid hole connected with the second cavity;Swivel joint 5 is single loop swivel joint;Locking Mechanism includes the lower lock for being arranged on the upper latch segment 14 of the lower end outside of housing upper 1 and being arranged on the outside of the upper end of lower housing portion 2 Tight block 15, upper latch segment 14 is equal with the lower quantity of latch segment 15, and is provided between upper latch segment 14 and lower latch segment 15 for locking Both tight clamping screws 13;The top of housing is provided with support frame 23 provided with the support 4 for installing motor 3, lower end;Housing upper 1 Lower surface is embedded in the spacing recessed of clamping provided with a circle provided with a circle spacing preiection, the upper surface of lower housing portion 2 for spacing preiection A circle sealing ring 16 is additionally provided between groove, and spacing preiection and limited impression.
Temperature sensor 12 is arranged at the first end of feeler lever 11, and enclosure interior, the of feeler lever 11 are arranged at by feeler lever 11 Two ends are located at hull outside;Feeler lever 11 is hollow structure, is passed through for lead 6;Feeler lever 11 is stainless steel metal material, can be protected Lead 6 is not by the chemicals attack in housing.Feeler lever 11 is extension type, to adapt to different size of reactor and/or make Temperature sensor 12 is located at the diverse location in housing.
Alarm 9 is arranged at hull outside, and temperature sensor 12 is connected by lead 6, and lead 6 is that low-resistance copper is led Line, the length of lead 6 can be adjusted so that alarm 9 can be arranged at the place apart from reactor farther out.
During work, first toward a kind of solvent is added thereto in housing, agitating shaft 10 is set to immerse in solvent, then control housing Temperature, reaches the temperature that reaction needs.Then driving agitating shaft 10 is rotated, when solvent is rotated, toward agitating shaft 10 Interior to add another solvent, the solvent is entered in housing by agitating shaft 10 from the first fluid hole 19, with adding before Solvent reaction., can also be molten toward adding in agitating shaft 10 while ensureing that agitating shaft 10 is rotated by setting swivel joint 5 Agent.Due to solvent of the agitating shaft 10 in rotary state, agitating shaft 10 under the influence of centrifugal force, so as to be thrown out of agitating shaft 10, enter in cavity can be with adding before solvent fully react., can be from multiple also, the quantity of fluid hole is multiple Position is entered in cavity, mixes more uniform.Furthermore it is possible to increase pressurizer, pressurizer is connected with feed tube 7, so that Increase the pressure of feed solution in charging, so as to strengthen the effect of mixing.
When the temperature in housing is higher than the setting value of reactant, alarm 9 sends alarm, reminds operating personnel to open cold But coil pipe 21 reduces reaction temperature, untill meeting the requirements.When the temperature in housing is less than the setting value of reactant, alarm Device 9 sends alarm, reminds operating personnel's heater 17 to improve reaction temperature, untill meeting the requirements.By this practicality New reactor, stabilizes production, and the yield of product brings up to more than 90%, and purity is stable more than 98%, so as to improve Product quality, production cost is further reduced.So as to ensure that synthesis procedure efficiently, stably, low consumption, high-quality, environmentally friendly transport OK, so as to meet the needs of production.
Although being described in detail with reference to accompanying drawing to embodiment of the present utility model, it should not be construed as pair The restriction of the protection domain of this patent.In the scope described by claims, those skilled in the art are without creative labor The dynamic various modification and variation that can be made still belong to the protection domain of this patent.

Claims (6)

1. a kind of fixed reactor, it is characterised in that:Including housing, motor(3), agitating shaft(10)And be arranged in housing The cooling coil of bottom(21);The cooling coil(21)Suspend and be located at housing inner bottom part, the agitating shaft(10)Positioned at housing It is interior and coaxially connected with housing, agitating shaft(10)On the stirring vane of helically type is distributed with(18), stirring vane(18)Upper weldering It is connected to puddler(20), agitating shaft(10)Top pass through swivel joint(5)With feed tube(7)Connection, the agitating shaft(10) Inside it is provided with the first cavity, agitating shaft(10)Bottom is provided with some first fluid holes(19), first fluid hole(19)With cavity Connection;The housing includes housing upper(1)And lower housing portion(2), the housing upper(1)With lower housing portion(2)Clamping is close Seal and locked by retaining mechanism, the housing upper end is provided with charge door(8), bottom is provided with discharging opening(22), inside is provided with Heater(17)And temperature sensor(12);The temperature sensor(12)Pass through feeler lever(11)Located at enclosure interior and by drawing Line(6)With the alarm located at hull outside(9)It is connected.
2. fixed reactor as claimed in claim 1, it is characterised in that:The stirring vane(18)Inside it is provided with second empty Chamber, second cavity is connected with the first cavity, stirring vane(18)Provided with the second fluid hole connected with the second cavity.
3. fixed reactor as claimed in claim 1, it is characterised in that:The swivel joint(5)Connect for single loop rotation Head.
4. fixed reactor as claimed in claim 1, it is characterised in that:The retaining mechanism includes being arranged on housing upper (1)The upper latch segment of lower end outside(14)And it is arranged on lower housing portion(2)Lower latch segment on the outside of upper end(15), it is described to lock Tight block(14)With lower latch segment(15)Quantity is equal, and upper latch segment(14)With lower latch segment(15)Between be provided be used for lock two The clamping screw of person(13).
5. fixed reactor as claimed in claim 1, it is characterised in that:The top of the housing is provided with the branch for installing motor Frame(4), lower end is provided with support frame(23).
6. fixed reactor as claimed in claim 1, it is characterised in that:The housing upper(1)Lower surface is provided with one Enclose spacing preiection, the lower housing portion(2)Upper surface is embedded in the limited impression of clamping provided with a circle for spacing preiection, and spacing A circle sealing ring is additionally provided between raised and limited impression(16).
CN201720179799.4U 2017-02-27 2017-02-27 A kind of fixed reactor Expired - Fee Related CN206549651U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720179799.4U CN206549651U (en) 2017-02-27 2017-02-27 A kind of fixed reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720179799.4U CN206549651U (en) 2017-02-27 2017-02-27 A kind of fixed reactor

Publications (1)

Publication Number Publication Date
CN206549651U true CN206549651U (en) 2017-10-13

Family

ID=60361714

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720179799.4U Expired - Fee Related CN206549651U (en) 2017-02-27 2017-02-27 A kind of fixed reactor

Country Status (1)

Country Link
CN (1) CN206549651U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114345280A (en) * 2022-01-17 2022-04-15 万华化学集团股份有限公司 Hypergravity reactor and method for preparing phosphorus pentafluoride in hypergravity reactor
CN114380604A (en) * 2021-12-27 2022-04-22 长兴正发热电耐火材料有限公司 Refractory plastic material with high thermal shock resistance and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114380604A (en) * 2021-12-27 2022-04-22 长兴正发热电耐火材料有限公司 Refractory plastic material with high thermal shock resistance and preparation method thereof
CN114345280A (en) * 2022-01-17 2022-04-15 万华化学集团股份有限公司 Hypergravity reactor and method for preparing phosphorus pentafluoride in hypergravity reactor
CN114345280B (en) * 2022-01-17 2024-04-09 万华化学集团股份有限公司 Supergravity reactor and method for preparing phosphorus pentafluoride in supergravity reactor

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171013

Termination date: 20190227

CF01 Termination of patent right due to non-payment of annual fee