CN206549623U - A kind of high temperature light-catalyzed reaction kettle - Google Patents

A kind of high temperature light-catalyzed reaction kettle Download PDF

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Publication number
CN206549623U
CN206549623U CN201720268711.6U CN201720268711U CN206549623U CN 206549623 U CN206549623 U CN 206549623U CN 201720268711 U CN201720268711 U CN 201720268711U CN 206549623 U CN206549623 U CN 206549623U
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Prior art keywords
kettle
sapphire
high temperature
catalyzed reaction
lid
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CN201720268711.6U
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Chinese (zh)
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徐清
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Anhui Kemi Machinery Technology Co Ltd
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Anhui Kemi Machinery Technology Co Ltd
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Abstract

The utility model discloses a kind of high temperature light-catalyzed reaction kettle, including kettle, kettle cover and heating furnace;The kettle is located in heating furnace, and kettle upper end is provided with kettle cover;The kettle cover includes lid, gland and sapphire, and lid is that sapphire is provided with hollow lid, lid cavity, and sapphire upper end is provided with gland;The sapphire is located at the middle part of lid cavity, and provided with the black spacer of admant between its outer wall and lid inwall, sapphire upper and lower side further respectively has the first soft graphite pad, the second soft graphite pad.The utility model has the advantage of:(1) it is simple in construction, easy to operate;(2) sapphire structures are used, it is high temperature resistant, high pressure resistant;(3) sapphire is placed between two layers of flexible graphite pad, then reaches protection sapphire eyeglass by increasing the black spacer of admant and graphite breakage-proof cover, prevents the graphite of soft graphite pad from crushing, so as to reach sealed purpose.

Description

A kind of high temperature light-catalyzed reaction kettle
Technical field
The utility model is related to reactor technical field, more particularly to a kind of high temperature light-catalyzed reaction kettle.
Background technology
From TiO in 19722(Nature, 1972,238 since being proved to photocatalysis performance:37-38), semiconductor light Catalysis technique is developed so far, and waste water, waste gas, waste oil and water hydrogen manufacturing, CO are handled using solar energy by catalysis material2Also Original etc. solves social environment with showing huge application prospect (Appl.Catal.B in terms of energy problem:Environ., 2002,37:1-15;Chem.Soc.Rev.,2009,38:253-278;Appl.Catal.B:Environ.,2013,129:39- 47)。
Although the efficient catalysis material of development of new is the important research point of field concern, light-catalyzed reaction kettle It is that light source, catalyst and reactant combine together, as the nucleus equipment of photocatalytic process, the quality of its performance is directly affected To the treatment effect of photocatalytic system, and the structure composition of reactor, light source position and reaction condition is controllable etc. that design is urged light Change giving full play to for reaction efficiency most important, and influence analysis and its post-processing of reaction product.
The vital part of high temperature light-catalyzed reaction kettle is sapphire eyeglass, and the part high temperature resistant is but very frangible.Accordingly, mesh In preceding light-catalyzed reaction kettle structure, protection is fixed to it provided with screw-type structure more around sapphire and seals.So And, the structure but can not effectively prevent sapphire from scratching and kettle leakage.
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, and there is provided simple in construction, easy to operate, the resistance to height of one kind Temperature, the high temperature light-catalyzed reaction kettle that can effectively prevent sapphire scuffing and kettle leakage.
The utility model is achieved through the following technical solutions:A kind of high temperature light-catalyzed reaction kettle, including kettle, kettle cover And heating furnace;The kettle is located in heating furnace, and kettle upper end is provided with kettle cover;The kettle cover includes lid, gland and sapphire, Lid is that sapphire is provided with hollow lid, lid cavity, and sapphire upper end is provided with gland;It is empty that the sapphire is located at lid The middle part of chamber, provided with the black spacer of admant between its outer wall and lid inwall, it is flexible that sapphire upper and lower side further respectively has first Graphite pads, the second soft graphite pad.
It is used as one of preferred embodiment of the present utility model, the first soft graphite pad, the internal diameter of the second soft graphite pad Place further respectively has the first graphite breakage-proof cover, the second graphite breakage-proof cover.
As one of preferred embodiment of the present utility model, described its circumference of kettle upper end edge is upwardly extended provided with projection, kettle Lid lower end relevant position is then provided with the groove matched with projection.
As one of preferred embodiment of the present utility model, graphite pads are connected between the raised and groove.
As one of preferred embodiment of the present utility model, flange is provided with along kettle periphery between the kettle cover and heating furnace.
As one of preferred embodiment of the present utility model, it is fixedly linked between the flange and kettle cover by fastener.
As one of preferred embodiment of the present utility model, leader is also transversely provided with the flange.
As one of preferred embodiment of the present utility model, kettle cover side wall is provided with valve interface and instrumentation tap, kettle Cover end and be provided with pressure gauge.
As one of preferred embodiment of the present utility model, the heating furnace is provided with binding post.
As one of preferred embodiment of the present utility model, it is fixedly linked between the kettle cover and gland by fastener.
The advantage of the utility model compared with prior art is:
(1) it is simple in construction, easy to operate;
(2) sapphire structures are used, it is high temperature resistant, high pressure resistant;
(3) sapphire is placed between two layers of flexible graphite pad, then is reached by increasing the black spacer of admant and graphite breakage-proof cover Sapphire eyeglass is protected, prevents the graphite of soft graphite pad from crushing, so as to reach sealed purpose.
Brief description of the drawings
Fig. 1 is a kind of overall structure diagram of high temperature light-catalyzed reaction kettle in embodiment 1.
In figure:1 is kettle, and 11 be projection, and 2 be kettle cover, and 21 be groove, and 22 be lid, and 23 be gland, and 24 be sapphire, 241 be the black spacer of admant, and 242 be the first soft graphite pad, and 243 be the second soft graphite pad, and 244 be the first graphite breakage-proof cover, 245 be the second graphite breakage-proof cover, and 3 be heating furnace, and 31 be binding post, and 4 be graphite pads, and 5 be flange, and 51 be handle.
Embodiment
Embodiment of the present utility model is elaborated below, the present embodiment using technical solutions of the utility model before Put and implemented, give detailed embodiment and specific operating process, but protection domain of the present utility model is not limited In following embodiments.
Embodiment 1
As shown in figure 1, a kind of high temperature light-catalyzed reaction kettle of the present embodiment, simple in construction, easy to operate, high temperature resistant, can Effectively prevent sapphire 24 from scratching and kettle leakage, including kettle 1, kettle cover 2 and heating furnace 3.
Kettle 1 is located in heating furnace 3, and the upper end of kettle 1 is provided with kettle cover 2;Its circumference of the upper end edge of kettle 1 is upwardly extended provided with convex 11 are played, the lower end relevant position of kettle cover 2 is then provided with the groove 21 matched with projection 11, and stone is connected between projection 11 and groove 21 Ink pad 4;Flange 5 is provided with along the periphery of kettle 1 between kettle cover 2 and heating furnace 3, passes through fastener stationary phase between flange 5 and kettle cover 2 Even, also it is transversely provided with leader 51 on flange 5.
Kettle cover 2 includes lid 22, gland 23 and sapphire 24;Lid 22 is to be set in hollow lid 22, the cavity of lid 22 There is sapphire 24, the upper end of sapphire 24 is provided with gland 23, is fixedly linked between gland 23 and lid 22 by fastener;Sapphire 24 are located at the middle part of the cavity of lid 22, and provided with the black spacer 241 of admant between its outer wall and the inwall of lid 22, sapphire is about 24 End further respectively has the first soft graphite pad 242, the second soft graphite pad 243, first the 242, second flexible stone of soft graphite pad The inner radius of ink pad 243 further respectively has the first graphite breakage-proof cover 244, the second graphite breakage-proof cover 245.
Further, valve interface and instrumentation tap are additionally provided with the side wall of kettle cover 2, the upper end of kettle cover 2 is provided with pressure gauge.
Further, heating furnace is provided with binding post 31.
Installation method:
(1) kettle cover 2 is disposed vertically, and the second graphite breakage-proof cover 245 and the second soft graphite pad 243 is put into kettle cover 2, gently Put down gently into sapphire 24, the outer radius of sapphire 24 places the black spacer 241 of admant, the first graphite, which is placed above, then at sapphire 24 prevents The broken soft graphite pad 242 of set 244 and first, covers gland 23, gently tightens firmware;
(2) by the horizontal positioned of kettle cover 2, gently push the second graphite breakage-proof cover 245 to sapphire 24 eyeglass, be allowed to and eyeglass Contact;
(3) uniform, the symmetrical fastener tightened on gland 23;
(4) after being connected kettle cover 2 and its intraware with kettle 1, flange, fastener, then valve, instrument are installed, put It is placed in heating furnace.
The advantage of the present apparatus is:
(1) it is simple in construction, easy to operate;
(2) structure of sapphire 24 is used, it is high temperature resistant, high pressure resistant;
(3) sapphire 24 is placed between two layers of flexible graphite pad, then by increasing the black spacer 241 of admant and graphite breakage-proof cover The protection eyeglass of sapphire 24 is reached, prevents the graphite of soft graphite pad from crushing, reaches sealed purpose.
Preferred embodiment of the present utility model is the foregoing is only, it is all at this not to limit the utility model Any modifications, equivalent substitutions and improvements made within the spirit and principle of utility model etc., should be included in the utility model Protection domain within.

Claims (10)

1. a kind of high temperature light-catalyzed reaction kettle, it is characterised in that including kettle, kettle cover and heating furnace;The kettle is located at heating In stove, kettle upper end is provided with kettle cover;The kettle cover includes lid, gland and sapphire, and lid is hollow lid, lid cavity Interior to be provided with sapphire, sapphire upper end is provided with gland;The sapphire is located at the middle part of lid cavity, its outer wall and lid inwall Between further respectively have the first soft graphite pad, the second soft graphite pad provided with the black spacer of admant, sapphire upper and lower side.
2. high temperature light-catalyzed reaction kettle according to claim 1, it is characterised in that the first soft graphite pad, second The inner radius of soft graphite pad further respectively has the first graphite breakage-proof cover, the second graphite breakage-proof cover.
3. high temperature light-catalyzed reaction kettle according to claim 1, it is characterised in that described its circumference of kettle upper end edge is upward Extension is provided with projection, and kettle cover lower end relevant position is then provided with the groove matched with projection.
4. high temperature light-catalyzed reaction kettle according to claim 3, it is characterised in that be connected between the raised and groove Graphite pads.
5. high temperature light-catalyzed reaction kettle according to claim 1, it is characterised in that along kettle between the kettle cover and heating furnace External week is provided with flange.
6. high temperature light-catalyzed reaction kettle according to claim 5, it is characterised in that by tight between the flange and kettle cover Firmware is fixedly linked.
7. high temperature light-catalyzed reaction kettle according to claim 5, it is characterised in that one is also transversely provided with the flange Hand.
8. high temperature light-catalyzed reaction kettle according to claim 1, it is characterised in that kettle cover side wall connects provided with valve Mouth and instrumentation tap, kettle cover upper end are provided with pressure gauge.
9. high temperature light-catalyzed reaction kettle according to claim 1, it is characterised in that the heating furnace is provided with binding post.
10. according to any described high temperature light-catalyzed reaction kettles of claim 1-9, it is characterised in that the kettle cover and gland it Between be fixedly linked by fastener.
CN201720268711.6U 2017-03-17 2017-03-17 A kind of high temperature light-catalyzed reaction kettle Active CN206549623U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720268711.6U CN206549623U (en) 2017-03-17 2017-03-17 A kind of high temperature light-catalyzed reaction kettle

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Application Number Priority Date Filing Date Title
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CN206549623U true CN206549623U (en) 2017-10-13

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111774010A (en) * 2020-07-30 2020-10-16 安徽科幂机械科技有限公司 High-temperature high-pressure photocatalytic reaction device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111774010A (en) * 2020-07-30 2020-10-16 安徽科幂机械科技有限公司 High-temperature high-pressure photocatalytic reaction device
CN111774010B (en) * 2020-07-30 2022-07-12 安徽科幂仪器有限公司 High-temperature high-pressure photocatalytic reaction device

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