CN206519153U - A kind of impeller-type automatic material receiving precipitation reactor - Google Patents
A kind of impeller-type automatic material receiving precipitation reactor Download PDFInfo
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- CN206519153U CN206519153U CN201720156591.0U CN201720156591U CN206519153U CN 206519153 U CN206519153 U CN 206519153U CN 201720156591 U CN201720156591 U CN 201720156591U CN 206519153 U CN206519153 U CN 206519153U
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Abstract
The utility model provides a kind of impeller-type automatic material receiving precipitation reactor, it is related to chemical reaction device technical field, including support, reaction material collecting device and lowering or hoisting gear, react material collecting device and lowering or hoisting gear is located at the lower portion of support, reacting material collecting device includes stirring receiving mechanism, isothermal reaction tank and motor, the top plate of motor through support is connected with stirring receiving mechanism, lowering or hoisting gear drives the isothermal reaction tank for the side of being fixed thereon to move up and down, and realizes the insertion and separation of stirring receiving mechanism and isothermal reaction tank.The utility model can be used for chemical coprecipitation powder or chemical plating pulverizing process, device integrates heating, stirring, rewinding, continuous charging, continuous production can be accomplished, powder is continuously received, eliminate the solution troublesome operation such as standing, separation of solid and liquid for a long time, greatly accelerate experiment process, improve production efficiency, an industrialization route is provided for the preparation of ultrathin composite powder, with good economic results in society.
Description
Technical field
The utility model is related to chemical reaction device technical field, more particularly to a kind of impeller-type automatic material receiving precipitation reaction
Device.
Background technology
Laboratory is industrial through preparing ultrathin composite powder frequently with chemical coprecipitation or sol-gal process, and its principle is
Solubility salt is dissolved in the water formation aqueous solution, precipitating reagent or complexing agent is then added, under the conditions of certain pH value, forms heavy
Form sediment or gel.Co-precipitation or sol-gel process need to carry out at a certain temperature, so whole process is needed in constant temperature
Carried out in reactor, it is ensured that the reaction temperature needed for reaction.And in order to improve reaction rate, promote generation and the crystal of nucleus
Grow up, prevent powder from reuniting, whole process will be stirred ceaselessly, wait after reaction terminates, stand for a long time, outwell supernatant,
Sediment or gel are further centrifuged, dried, then superfine powder is made by processes such as follow-up roasting, reduction.It is whole
Individual co-precipitation or sol-gel process, technique are cumbersome, the poor continuity of production, if it is possible to accomplish continuously to add in course of reaction
Material, continuously receives powder, saves long-time standing separation process, will greatly improve experiment or production efficiency.
Utility model content
The technical problems to be solved in the utility model be for above-mentioned the deficiencies in the prior art there is provided one kind it is simple in construction,
Can effectively process simplification, improve experiment or production efficiency impeller-type automatic material receiving precipitation reactor.
In order to solve the above technical problems, technical solution adopted in the utility model is：A kind of impeller-type automatic material receiving sinks
Shallow lake reactor, including support, reaction material collecting device and lowering or hoisting gear, reaction material collecting device and lowering or hoisting gear are located at the framework of support
Inside, reaction material collecting device includes stirring receiving mechanism, isothermal reaction tank and motor, and motor is received through the top plate of support and stirring
Expect that mechanism is connected, lowering or hoisting gear drives the isothermal reaction tank for the side of being fixed thereon to move up and down, realize stirring receiving mechanism and perseverance
The insertion and separation of warm retort.
Preferably, isothermal reaction tank includes inner cylinder and outer barrel, heater strip, heater strip both sides are provided between inner cylinder and outer barrel
Provided with insulating materials.
Preferably, being provided with thermocouple temperature measuring apparatus at inner cylinder bottom centre.
Preferably, inner cylinder bottom is provided with water inlet pipe and outlet pipe.
Preferably, support include top plate, bottom plate and multiple columns, column upper and lower ends respectively with top plate and bottom plate phase
Even, motor is fixed on top plate through the centre bore of top plate center.
Preferably, motor is buncher.
Preferably, stirring receiving mechanism includes stirring rewinding cylinder and multiple special-shaped rewinding boxes, stirring rewinding cylinder circumference side
To provided with multiple vertical blades, special-shaped rewinding box is embedded between the two neighboring blade in bottom of stirring rewinding cylinder.
Preferably, the angle of the radius of blade and stirring rewinding cylinder is α, α is 30 ° -60 °.
Preferably, blade and special-shaped rewinding box material are PVC plastic, stainless steel or polytetrafluoroethylmaterial material.
Preferably, lowering or hoisting gear includes supporting plate and the folding stand, hydraulic stem, the cross bar that are arranged in pairs, folding stand bottom leads to
Cross cross bar to be connected, hydraulic stem is arranged at folding stand lower end, and folding stand upper end is connected with supporting plate, hydraulic stem is flexible to be driven above and below supporting plate
Lifting.
It is using the beneficial effect produced by above-mentioned technical proposal：The utility model can be used for chemical coprecipitation powder or
Chemical plating pulverizing process, device integrates heating, stirring, rewinding, can accomplish continuous charging, continuous production, continuously receive powder,
The solution troublesome operation such as standing, separation of solid and liquid for a long time is eliminated, experiment process is greatly accelerated, improves production efficiency, be
The preparation of ultrathin composite powder provides an industrialization route, with good economic results in society.
Brief description of the drawings
Fig. 1 is a kind of structural representation of impeller-type automatic material receiving precipitation reactor of the utility model.
Fig. 2 is the structural representation of another state of Fig. 1.
Fig. 3 is the structural representation of Fig. 1 medium-height trestles.
Fig. 4 is the explosive view of stirring receiving mechanism in Fig. 1.
Fig. 5 is the top view of stirring rewinding cylinder in Fig. 1.
Fig. 6 is the structural representation of rewinding box in Fig. 1.
Fig. 7 is the structural representation of temperature-controlling reaction apparatus in Fig. 1.
In figure：1st, support；11st, top plate；12nd, bottom plate；13rd, centre bore；14th, column；2nd, material collecting device is reacted；21st, stir
Receiving mechanism；211st, stirring rewinding cylinder；2111st, blade；212nd, special-shaped rewinding box；22nd, isothermal reaction tank；221st, inner cylinder；
2211st, water inlet pipe；2212nd, outlet pipe；222nd, outer barrel；223rd, thermocouple temperature measuring apparatus；224th, heater strip；225th, insulating materials；
23rd, motor；3rd, lowering or hoisting gear；31st, supporting plate；32nd, folding stand；33rd, hydraulic stem；34th, cross bar.
Embodiment
In order that the purpose of this utility model, technical scheme and advantage are more clearly understood, below in conjunction with accompanying drawing and implementation
Example, the utility model is further elaborated.It should be appreciated that specific embodiment described herein is only to explain
The utility model, is not used to limit the utility model.
As shown in Figures 1 to 7, a kind of impeller-type automatic material receiving precipitation reactor, including support 1, reaction material collecting device 2 and
Lowering or hoisting gear 3, reaction material collecting device 2 and lowering or hoisting gear 3 are located at the lower portion of support 1, and reaction material collecting device 2 includes stirring and received
Expect mechanism 21, isothermal reaction tank 22 and motor 23, the top plate 11 of motor 23 through support 1 is connected with stirring receiving mechanism 21, risen
Falling unit 3 drives the isothermal reaction tank 22 for the side of being fixed thereon to move up and down, and realizes stirring receiving mechanism 21 and isothermal reaction tank
22 insertion and separation.Reaction material collecting device 2 and lowering or hoisting gear 3 are arranged at the lower portion of support 1, by controlling lowering or hoisting gear
3 lifting action, realizes the insertion and separation of stirring receiving mechanism 21 and isothermal reaction tank 22, when the addition for carrying out reaction raw materials
When, isothermal reaction tank 22 is located at lower position, when raw material addition terminates, it is necessary to be heated and stirred or rewinding to reaction solution
When, lowering or hoisting gear 3 is raised above, and isothermal reaction tank 22 is raised to the position for being coated at stirring receiving mechanism 21, you can carried out
Stirring and the operation of rewinding, eliminate the time of standing, improve the efficiency of experiment and production.
Preferably, isothermal reaction tank 22 includes inner cylinder 221 and outer barrel 222, it is provided with and adds between inner cylinder 221 and outer barrel 222
Heated filament 224, the both sides of heater strip 224 are provided with insulating materials 225.22 points of isothermal reaction tank is inner cylinder 221 and outer barrel 222, inner cylinder 221
Directly contacted with the solution of reaction, outer barrel 222 and lowering or hoisting gear 3 are contacted, heater strip 224 is provided between inner cylinder 221 and outer barrel 222
Reaction solution in inner cylinder 221 is heated, while in order to avoid heater strip 224 is directly heated and made to inner cylinder 221 and outer barrel 222
It is uneven into inner cylinder 221 and the surface local heating of outer barrel 222, while scattered and disappeared in order to avoid heat is excessive by outer barrel 222, so
Insulating materials 225 is provided with the both sides of heater strip 224, insulating materials 225 has certain protection to inner cylinder 221 and outer barrel 222
Effect.
Preferably, being provided with thermocouple temperature measuring apparatus 223 at the bottom centre of inner cylinder 221.Heat at the bottom centre of inner cylinder 221
Galvanic couple temperature measuring equipment 223 can carry out effective monitoring to the heating process of heater strip 224, when the temperature of reaction solution in inner cylinder 221
Degree reaches that to a certain degree then heater strip 224 stops heating reaction solution, is easy to the entirety control to heating process.
Preferably, the bottom of inner cylinder 221 is provided with water inlet pipe 2211 and outlet pipe 2212.In order that isothermal reaction tank 22 is realized
The effect of automatic feeding water and automatic outletting, saves the process manually added water, corresponding to set water inlet pipe 2211 in the bottom of inner cylinder 221
With outlet pipe 2212, and be correspondingly arranged on the valve of control break-make, be easy to it is continual carry out multiple course of reaction, save a large amount of
Time and manpower, and can guarantee that the accuracy of experiment.
Preferably, support 1 include top plate 11, bottom plate 12 and multiple columns 14, the upper and lower ends of column 14 respectively with top plate
11 are connected with bottom plate 12, and motor 23 is fixed on top plate 11 through the centre bore 13 of the center of top plate 11.The top plate 11 of support 1 is led
It is used for the motor 23 that fixed control stirring receiving mechanism 21 is rotated, motor 23 is located at the top of top plate 11, stirs receiving mechanism
21 are located at below top plate and are connected with the output shaft of motor 23.By the power output of motor 23 to being reacted in isothermal reaction tank 22
Liquid is stirred the action with rewinding.
Preferably, motor 23 is buncher.The various process of stirring or rewinding, motor 23 are in for reaction solution
Rotating speed it is different, it is necessary to be stirred to reaction solution in the course of reaction of isothermal reaction tank 22, then reaction solution is made using the slow-speed of revolution
Stirring is abundant, when the reaction for needing to complete reaction also carries out the collection of sediment, then motor is tuned into high-revolving pattern,
Stirring receiving mechanism 21 is set to carry out the collection of sediment in the case of high-revolving, therefore motor 23 selects buncher, so as to right
The different processes that should be tested use different velocities of rotation.
Preferably, stirring receiving mechanism 21 includes stirring rewinding cylinder 211 and multiple special-shaped rewinding boxes 212, rewinding is stirred
211 circumferencial directions of cylinder are provided with multiple vertical blades 2111, and special-shaped rewinding box 212 is embedded in the bottom adjacent two of stirring rewinding cylinder 211
Between individual blade 2111.Rewinding box 212 is to insert mode between blade 2111, quick release.Stir receiving mechanism 21
Stirring rewinding cylinder 21 be mainly used in stirring to reaction solution, stirring rewinding 211 circumferencial directions of cylinder are provided with multiple vertical blades
2111, contacted by multiple blades 2111 and reaction solution, increase contact area, it is ensured that the uniformity of stirring.It is multiple
Special-shaped rewinding box 212 is mainly used in the collection of sediment, and with higher speed stirring is thrown to by the sediment that will react generation
Between blade 2111 on rewinding 211 side walls of cylinder, and then special-shaped rewinding box 212 is dropped down onto under realizing sediment under Gravitative Loads
In, realize the action process of automatic material receiving.
Preferably, the angle of the radius of blade 2111 and stirring rewinding cylinder 211 is α, α is 30 ° -60 °.The He of blade 2111
The angle of the radius of stirring rewinding cylinder 211 directly decides mixing effect, can be effective when angle is arranged between 30 ° -60 °
Increase the contact area of blade 2111 and reaction solution, while when sediment collection is carried out, the angle is led to sediment
It is optimal to effect, the collection efficiency of sediment can be effectively improved.
Preferably, blade 2111 and the special-shaped material of rewinding box 212 are PVC plastic, stainless steel or polytetrafluoroethylmaterial material.
The problem of on the one hand selection of blade 2111 considers its service life, while it is also contemplated that corrosion resistance and being difficult and other are chemical
The characteristics of material reacts.More common is PVC plastic, stainless steel or polytetrafluoroethylmaterial material, and this several material price is relative
It is cheap, and be difficult to react with other chemical substances, it is easy to get with raw material, economical advantage.
Preferably, lowering or hoisting gear 3 includes supporting plate 31 and the folding stand 32, hydraulic stem 33, the cross bar 34 that are arranged in pairs, fold
The bottom of frame 32 is connected by cross bar 34, and hydraulic stem 33 is arranged at the lower end of folding stand 32, and the upper end of folding stand 32 is connected with supporting plate 31, liquid
Depression bar 33 is flexible to drive the oscilaltion of supporting plate 31.Lowering or hoisting gear 3 is opened and shunk by the Foldable frame 32 of hydraulic stem 33, and then
The upper down conversion that the oscilaltion of supporting plate 31 is easy to complex reaction process to carry out the position of isothermal reaction tank 22 is realized, realizes that stirring is received
The process of material.
Operating process：The preparation of aluminum oxide dispersion strengthening iron powder
Deionized water is added into isothermal reaction tank 22, ferric nitrate, aluminum nitrate is added, ammoniacal liquor is added, then adds lemon
Lemon acid is used as complexing agent.Control lowering or hoisting gear 3 rises supporting plate 31, and stirring material collecting device 21 is immersed in the liquid level of isothermal reaction tank 22
Lower specified location, starts motor 23 and starts stirring, rotating speed is controlled in 300r/min, and isothermal reaction tank 22 is started to warm up.Treat constant temperature
Reactor is warming up to 50 DEG C, and motor 23 accelerates to 400r/min.When solution colour disappears, the rotational speed regulation of motor is arrived
1100r/min, the supporting plate 31 of lowering or hoisting gear 3 slowly declines, the guide effect of the precipitated phase of generation in centrifugal force and blade 2111
Under be collected into rewinding box 212.
The utility model can be used for chemical coprecipitation powder or chemical plating pulverizing process, and the heating of device collection, stirring, rewinding are
One, can accomplish continuous charging, continuous production, continuously receive powder, eliminate the solution cumbersome behaviour such as standing, separation of solid and liquid for a long time
Make, greatly accelerate experiment process, improve production efficiency, an industrialization road is provided for the preparation of ultrathin composite powder
Line, with good economic results in society.
Preferred embodiment of the present utility model is these are only, it is all in this practicality not to limit the utility model
Any modifications, equivalent substitutions and improvements made within new spirit and principle etc., should be included in guarantor of the present utility model
Within the scope of shield.
Claims (10)
1. a kind of impeller-type automatic material receiving precipitation reactor, it is characterised in that：Including support（1）, reaction material collecting device（2）And liter
Falling unit（3）, the reaction material collecting device（2）And lowering or hoisting gear（3）Positioned at support（1）Lower portion, the reaction rewinding
Device（2）Including stirring receiving mechanism（21）, isothermal reaction tank（22）And motor（23）, the motor（23）Through support（1）
Top plate（11）With stirring receiving mechanism（21）It is connected, the lowering or hoisting gear（3）Drive the isothermal reaction tank for the side of being fixed thereon
（22）Move up and down, realize stirring receiving mechanism（21）With isothermal reaction tank（22）Insertion and separation.
2. a kind of impeller-type automatic material receiving precipitation reactor according to claim 1, it is characterised in that：The isothermal reaction
Tank（22）Including inner cylinder（221）And outer barrel（222）, the inner cylinder（221）And outer barrel（222）Between be provided with heater strip（224）, institute
State heater strip（224）Both sides are provided with insulating materials（225）.
3. a kind of impeller-type automatic material receiving precipitation reactor according to claim 2, it is characterised in that：The inner cylinder
（221）Thermocouple temperature measuring apparatus is provided with bottom centre（223）.
4. a kind of impeller-type automatic material receiving precipitation reactor according to claim 2, it is characterised in that：The inner cylinder
（221）Bottom is provided with water inlet pipe（2211）And outlet pipe（2212）.
5. a kind of impeller-type automatic material receiving precipitation reactor according to claim 1, it is characterised in that：The support（1）
Including top plate（11）, bottom plate（12）With multiple columns（14）, the column（14）Upper and lower ends respectively with top plate（11）And bottom plate
（12）It is connected, the motor（23）Through top plate（11）The centre bore of center（13）It is fixed on top plate（11）On.
6. a kind of impeller-type automatic material receiving precipitation reactor according to claim 1, it is characterised in that：The motor（23）
For buncher.
7. a kind of impeller-type automatic material receiving precipitation reactor according to claim 1, it is characterised in that：The stirring rewinding
Mechanism（21）Including stirring rewinding cylinder（211）With multiple special-shaped rewinding boxes（212）, the stirring rewinding cylinder（211）Circumferencial direction
Provided with multiple vertical blades（2111）, the special-shaped rewinding box（212）It is embedded in stirring rewinding cylinder（211）The two neighboring leaf in bottom
Piece（2111）Between.
8. a kind of impeller-type automatic material receiving precipitation reactor according to claim 7, it is characterised in that：The blade
（2111）With stirring rewinding cylinder（211）The angle of radius be α, α is 30 ° -60 °.
9. a kind of impeller-type automatic material receiving precipitation reactor according to claim 7, it is characterised in that：The blade
（2111）With special-shaped rewinding box（212）Material is PVC plastic, stainless steel or polytetrafluoroethylmaterial material.
10. a kind of impeller-type automatic material receiving precipitation reactor according to claim 1, it is characterised in that：The lifting dress
Put（3）Including supporting plate（31）With the folding stand being arranged in pairs（32）, hydraulic stem（33）, cross bar（34）, the folding stand（32）Bottom
Portion passes through cross bar（34）It is connected, the hydraulic stem（33）It is arranged at folding stand（32）Lower end, the folding stand（32）Upper end and support
Plate（31）It is connected, the hydraulic stem（33）It is flexible to drive supporting plate（31）Oscilaltion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720156591.0U CN206519153U (en) | 2017-02-21 | 2017-02-21 | A kind of impeller-type automatic material receiving precipitation reactor |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720156591.0U CN206519153U (en) | 2017-02-21 | 2017-02-21 | A kind of impeller-type automatic material receiving precipitation reactor |
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| CN206519153U true CN206519153U (en) | 2017-09-26 |
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| CN201720156591.0U Active CN206519153U (en) | 2017-02-21 | 2017-02-21 | A kind of impeller-type automatic material receiving precipitation reactor |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109999744A (en) * | 2019-04-23 | 2019-07-12 | 中海油能源发展股份有限公司 | A kind of experimental system suitable for supercritical water oxidation intermittent duty |
| CN113667504A (en) * | 2021-07-28 | 2021-11-19 | 中铁城市发展投资集团有限公司 | Multifunctional asphalt heating box |
-
2017
- 2017-02-21 CN CN201720156591.0U patent/CN206519153U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109999744A (en) * | 2019-04-23 | 2019-07-12 | 中海油能源发展股份有限公司 | A kind of experimental system suitable for supercritical water oxidation intermittent duty |
| CN113667504A (en) * | 2021-07-28 | 2021-11-19 | 中铁城市发展投资集团有限公司 | Multifunctional asphalt heating box |
| CN113667504B (en) * | 2021-07-28 | 2024-01-30 | 中铁城市发展投资集团有限公司 | Multifunctional asphalt heating box |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20210119 Address after: 214400 No.1, beihuajia village, Shennan village, Shengang street, Jiangyin City, Wuxi City, Jiangsu Province Patentee after: Jiangsu Shuwei New Material Technology Co.,Ltd. Address before: 050091 no.626, Hongqi Street, Shijiazhuang City, Hebei Province Patentee before: HEBEI College OF INDUSTRY AND TECHNOLOGY |
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| TR01 | Transfer of patent right |