CN206518912U - One kind condensation interface is with collecting Backflow bottle integrated apparatus - Google Patents
One kind condensation interface is with collecting Backflow bottle integrated apparatus Download PDFInfo
- Publication number
- CN206518912U CN206518912U CN201720089018.2U CN201720089018U CN206518912U CN 206518912 U CN206518912 U CN 206518912U CN 201720089018 U CN201720089018 U CN 201720089018U CN 206518912 U CN206518912 U CN 206518912U
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- China
- Prior art keywords
- backflow
- receiving flask
- condensation
- integrated apparatus
- cold finger
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- 238000009833 condensation Methods 0.000 title claims abstract description 27
- 230000005494 condensation Effects 0.000 title claims abstract description 27
- 238000010992 reflux Methods 0.000 claims abstract description 25
- 238000007599 discharging Methods 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000000227 grinding Methods 0.000 claims abstract description 13
- 238000004821 distillation Methods 0.000 abstract description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000003321 amplification Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000010808 liquid waste Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 238000012913 prioritisation Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 229940099259 vaseline Drugs 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model provides a kind of condensation interface with collecting Backflow bottle integrated apparatus, including straight cold finger, flow back receiving flask, the drain being connected with the top of backflow receiving flask, refluxing opening, discharging opening and the condensation water inlet and condensation-water drain located at straight cold finger surface, the refluxing opening is located at backflow receiving flask side middle part, discharging opening is located at backflow receiving flask bottom, described straight cold finger one end is connected with backflow receiving flask side, the other end is provided with condenser pipe upper grinding port, water inlet is condensed close to one end of connection backflow receiving flask, condensation-water drain is close to one end of condenser pipe upper grinding port.For prior art, the utility model device is attached using straight cold finger and collection two parts of Backflow bottle, is reduced the connection of dovetail pipe, can effectively be reduced the height of whole rectifier unit, the air-tightness of device is set to have significant raising simultaneously, it is convenient to be provided for distillation process.
Description
Technical field
The utility model discloses one kind condensation interface with collecting Backflow bottle integrated apparatus, belong to rectifying separator skill
Art field.
Background technology
Rectifying isolation technics is widely used in the production process of petrochemical industry, medicine and pesticide intermediate etc., be product purification,
Reclaim the significant element with liquid waste processing.In distillation process, overhead vapours needs to condense and flow back by condensing unit.Tradition
Condensing unit generally by condenser pipe, dovetail pipe and collect Backflow bottle constitute, connected during installation between all parts with ground,
Because connection often comes off or poor sealing at ground, cause gas leakage at ground, therefore rectifying column gas can be caused more than part
Close property weakens, and influences experiment effect；Simultaneously because needing dovetail pipe to connect, the height of whole device is added.
Utility model content
Utility model purpose：For above-mentioned technical problem, the utility model provides a kind of condensation interface and flowed back with collecting
Bottle integrated apparatus.
Technical scheme：The utility model provides a kind of condensation interface with collecting Backflow bottle integrated apparatus, including straight
Condenser pipe, backflow receiving flask, with backflow receiving flask at the top of be connected drain, refluxing opening, discharging opening and located at straight condensation
The condensation water inlet and condensation-water drain of pipe surface, the refluxing opening are located at back located at backflow receiving flask side middle part, discharging opening
Receiving flask bottom is flowed, described straight cold finger one end is connected with backflow receiving flask side, and the other end is provided with condenser pipe upper grinding port,
Water inlet is condensed close to one end of connection backflow receiving flask, condensation-water drain is close to one end of condenser pipe upper grinding port.
It is preferred that, described straight cold finger one end is provided with ground under condenser pipe, and backflow receiving flask side, which is provided with receiving flask, grinds
Mouthful, by the mutual cooperation of ground in ground under condenser pipe and receiving flask, straight cold finger one end and backflow receiving flask can be made
Side is connected.
Further preferably, ground is located at the top of refluxing opening in the receiving flask.
It is preferred that, the straight cold finger is with the horizontal 30 degree.
It is preferred that, the opening of the refluxing opening is tilted to below horizontal plane.
It is preferred that, the straight cold finger length is about 25mm, and external diameter is Φ 40mm, and inner tube external diameter is Φ 40mm.
It is preferred that, the refluxing opening internal diameter is that Φ 6mm, discharging opening internal diameter are Φ 5mm, drain and backflow receiving flask junction
Internal diameter be Φ 6mm.
It is preferred that, the condenser pipe upper grinding port is connected with the side line ground of the stripping tube of rectifying column, refluxing opening and rectifying column
The phegma charging aperture of stripping tube is connected by rubber tube.
The utility model condenses interface can ensure the flat of air pressure with collecting Backflow bottle integrated apparatus, wherein drain
Weighing apparatus, refluxing opening ensures that some can be back in rectifier unit after the condensed pipework condensation of overhead vapours, and discharging opening ensures tower
The produced quantity on top, maintains the material balance of whole rectifier unit.
Such scheme of the present utility model, can there is following different specific prioritization scheme：
Described Novel condensation interface is carried out with collecting Backflow bottle integrated apparatus using straight cold finger to overhead vapours
Condensation, the outer grinding port of condenser pipe is directly connected with ground in the side line of collection Backflow bottle.Straight cold finger length is about 25mm,
External diameter is Φ 40mm, and internal diameter is Φ 15mm.Condenser pipe is with the horizontal 30 °, the turnover condensation a diameter of Φ 6mm in the mouth of a river.
Described Novel condensation interface is with collecting Backflow bottle integrated apparatus, and it is that Φ 6mm are returned to collect Backflow bottle provided with internal diameter
Head piece, Φ 5mm discharging openings, Φ 6mm vacuum ports and No. 19 receive interior ground, collect Backflow bottle side line ground and are ground with condenser pipe lower end
Mouth connection, collects Backflow bottle design drain, can maintain air pressure balance.
Described Novel condensation interface is with collecting Backflow bottle integrated apparatus, the upper end ground and rectifying column of straight cold finger
The connection of stripping tube side line ground, the discharging opening and the phegma charging aperture of rectifying column stripping tube for collecting Backflow bottle pass through rubber tube
Connection.
Technique effect：Relative to prior art, the utility model device is using straight cold finger and collects Backflow bottle two
Part is attached, and reduces the connection of dovetail pipe, can effectively reduce the height of whole rectifier unit, while making the airtight of device
Property have significant raising, it is convenient to be provided for distillation process.
Brief description of the drawings
Fig. 1 is the utility model condensation interface with collecting Backflow bottle integrated apparatus structural representation；
Fig. 2 is unmodified traditional condensation reflux unit：Straight cold finger 1, backflow receiving flask 2, dovetail pipe 3, emptying
Mouthfuls 4, refluxing opening 5, discharging opening 6, ground 8, condenser pipe upper grinding port 9, condensation water inlet 10 and under ground 7, condenser pipe in dovetail pipe
Condensation-water drain 11.
Embodiment
Below in conjunction with the accompanying drawings and instantiation, the utility model is further elucidated, it should be understood that these examples are merely to illustrate
The utility model rather than limitation scope of the present utility model.
Embodiment 1
The utility model condenses interface with collecting Backflow bottle integrated apparatus, is specifically shown in Fig. 1, including straight cold finger 1, returns
Stream receiving flask 2, with the drain 3 being connected at the top of backflow receiving flask 2, refluxing opening 4, discharging opening 5 and located at the table of straight cold finger 1
The condensation water inlet 9 and condensation-water drain 10 in face, refluxing opening 4 is located at the side middle part of backflow receiving flask 2, and discharging opening 5 is located at backflow
The bottom of receiving flask 2, one end of straight cold finger 1 is connected with backflow receiving flask 2 side, and the other end is provided with condenser pipe upper grinding port 8, cold
Solidifying water inlet 9 is close to one end of connection backflow receiving flask 2, and condensation-water drain 10 is close to one end of condenser pipe upper grinding port 8.
The one end of straight cold finger 1 is provided with ground 7 under condenser pipe, and backflow receiving flask 2 side leads to provided with ground 6 in receiving flask
The mutual cooperation of ground 6 in ground 7 and receiving flask under condenser pipe is crossed, the one end of straight cold finger 1 and backflow receiving flask 2 side can be made
Face is connected.
Ground 6 is located at the top of refluxing opening 4 in receiving flask.
Straight cold finger 1 is with the horizontal 30 degree；The opening of refluxing opening 4 is tilted to below horizontal plane.
The length of straight cold finger 1 is about 25mm, and external diameter is Φ 40mm, and inner tube external diameter is Φ 15mm.
The internal diameter of refluxing opening 4 is that Φ 6mm, the internal diameter of discharging opening 5 are the interior of Φ 5mm, drain 3 and backflow receiving flask 2 junction
Footpath is Φ 6mm.
Condenser pipe upper grinding port 8 is connected with the side line ground of the stripping tube of rectifying column, refluxing opening 4 and rectifying column stripping tube
Phegma charging aperture is connected by rubber tube.
Before experiment, first package unit is cleaned up and dried in an oven, vaseline is then smeared at all grounds,
Ground 7 is connected with ground 6 in backflow receiving flask under straight cold finger, and receiving flask refluxing opening 4 passes through rubber tube and rectifying column vapour
The phegma charging aperture for carrying pipe is connected, and coolant is passed through from 9,10 outflows.After rectifying experiment stablizes infinite reflux for a period of time,
Start liquid level in continuous feed and discharging, natural back flow control receiving flask, discharging opening 5 collects tower top discharging.The utility model
Condense interface and collect Backflow bottle integrated apparatus, the air-tightness of device and the height of the whole rectifier unit of reduction can be effectively improved
Degree.
The utility model is simple in construction, easy to operate, as needed, and the utility model can be proportionally amplified,
There is industrial value after amplification.
Claims (6)
1. one kind condensation interface is with collecting Backflow bottle integrated apparatus, it is characterised in that received including straight cold finger (1), backflow
Collection bottle (2), drain (3), refluxing opening (4), the discharging opening (5) and cold located at straight being connected with backflow receiving flask (2) top
The condensation water inlet (9) and condensation-water drain (10) on solidifying pipe (1) surface, the refluxing opening (4) is located at backflow receiving flask (2) side
Middle part, discharging opening (5) is located at backflow receiving flask (2) bottom, described straight cold finger (1) one end and backflow receiving flask (2) side
It is connected, the other end is provided with condenser pipe upper grinding port (8), condensation water inlet (9) is cold close to one end of connection backflow receiving flask (2)
Solidifying water out (10) is close to one end of condenser pipe upper grinding port (8)；
Described straight cold finger (1) one end is provided with ground (7) under condenser pipe, and backflow receiving flask (2) is sideways provided with mill in receiving flask
Mouth (6), by the mutual cooperation of ground (6) in ground under condenser pipe (7) and receiving flask, can make straight cold finger (1) one end
It is connected sideways with backflow receiving flask (2)；Ground (6) is located at the top of refluxing opening (4) in receiving flask.
2. condensation interface according to claim 1 is with collecting Backflow bottle integrated apparatus, it is characterised in that the straight is cold
Solidifying pipe (1) is with the horizontal 30 degree.
3. condensation interface according to claim 1 is with collecting Backflow bottle integrated apparatus, it is characterised in that the refluxing opening
(4) opening is tilted to below horizontal plane.
4. condensation interface according to claim 1 is with collecting Backflow bottle integrated apparatus, it is characterised in that the straight is cold
Solidifying pipe (1) length is about 25mm, and external diameter is Φ 40mm, and inner tube external diameter is Φ 15mm.
5. condensation interface according to claim 1 is with collecting Backflow bottle integrated apparatus, it is characterised in that the refluxing opening
(4) internal diameter that internal diameter is Φ 6mm, discharging opening (5) internal diameter is Φ 5mm, drain (3) and backflow receiving flask (2) junction is Φ
6mm。
6. condensation interface according to claim 1 is with collecting Backflow bottle integrated apparatus, it is characterised in that the condenser pipe
Upper grinding port (8) is connected with the side line ground of the stripping tube of rectifying column, and the phegma of refluxing opening (4) and rectifying column stripping tube is fed
Mouth is connected by rubber tube.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720089018.2U CN206518912U (en) | 2017-01-20 | 2017-01-20 | One kind condensation interface is with collecting Backflow bottle integrated apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720089018.2U CN206518912U (en) | 2017-01-20 | 2017-01-20 | One kind condensation interface is with collecting Backflow bottle integrated apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206518912U true CN206518912U (en) | 2017-09-26 |
Family
ID=59890304
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720089018.2U Expired - Fee Related CN206518912U (en) | 2017-01-20 | 2017-01-20 | One kind condensation interface is with collecting Backflow bottle integrated apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206518912U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
| CN111855381A (en) * | 2020-08-13 | 2020-10-30 | 郭喜丰 | Continuous distillation device suitable for detecting large-batch samples |
-
2017
- 2017-01-20 CN CN201720089018.2U patent/CN206518912U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
| CN111855381A (en) * | 2020-08-13 | 2020-10-30 | 郭喜丰 | Continuous distillation device suitable for detecting large-batch samples |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180424 Address after: 214047 701-704, room D, 606 Ning six road, Nanjing chemical industry park, Jiangsu. Patentee after: Nanjing Ke Yi new material Co., Ltd Address before: No. 1, Wen Yuan Road, Nanjing, Jiangsu Province, Jiangsu Patentee before: Nanjing Normal University |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170926 Termination date: 20200120 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |