CN206492490U - A kind of reaction unit that reaction is participated in for gas - Google Patents

A kind of reaction unit that reaction is participated in for gas Download PDF

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Publication number
CN206492490U
CN206492490U CN201720186076.7U CN201720186076U CN206492490U CN 206492490 U CN206492490 U CN 206492490U CN 201720186076 U CN201720186076 U CN 201720186076U CN 206492490 U CN206492490 U CN 206492490U
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China
Prior art keywords
reaction
gas
reaction vessel
participated
inlet duct
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CN201720186076.7U
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Chinese (zh)
Inventor
杨孝容
唐琼
马旭光
田冲
成英
易志刚
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Leshan Normal University
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Leshan Normal University
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Abstract

The utility model discloses a kind of reaction unit that reaction is participated in for gas, including reaction vessel and inlet duct, the reaction vessel upper end is provided with upper grinding port and temperature socket, side grinding mouthful is additionally provided with the reaction vessel radial direction lateral body, the inlet duct includes air inlet pipe and the gas-filling device being connected with air inlet pipe, and the inlet duct is arranged on reaction vessel radial direction lateral body bottom with reaction vessel junction.The beneficial effects of the utility model are:Increase contact area and the time of contact of gas and reaction solution, equivalent to the concentration of increase gas, make reaction more abundant, be conducive to improving reaction yield.

Description

A kind of reaction unit that reaction is participated in for gas
Technical field
The utility model is related to a kind of experiment equipment, more particularly to a kind of reaction unit that reaction is participated in for gas.
Background technology
In chemical experiment, liquid substance is held commonly using flask as reaction vessel, distillation container etc., with making With advantage that is convenient, having a wide range of application.
Current existing reaction unit, mostly using many mouthfuls of flasks of upper opening, is led to gas by the bottleneck on top Enter in liquid and tested.
Experiment is carried out using this reaction unit to have the disadvantage that:
1st, the contact area of gas and liquid is small, reacts insufficient, easily causes waste of material.
2nd, the bottleneck adding liquid from upper end is needed, the addition and sampling of raw material is not easy to.
It if the 3, producing volatile materials, can not be reclaimed, cause to waste and even pollute.
4th, it is unfavorable for test experience temperature.
The content of the invention
The utility model spy provides a kind of reaction unit that reaction is participated in for gas, to solve the defect of prior art.
Technical scheme is as follows:
A kind of reaction unit that reaction is participated in for gas, it is characterised in that described including reaction vessel and inlet duct Reaction vessel top is provided with upper grinding port and thermometer socket, is additionally provided with side grinding mouthful on the reaction vessel radial direction lateral body, it is described enter Device of air includes air inlet pipe and the gas-filling device being connected with air inlet pipe, and the inlet duct is set with reaction vessel junction In reaction vessel radial direction lateral body bottom.
In such scheme, the gas-filling device is to be provided with equally distributed capillary on ring pipe, the ring pipe Hole, in an experiment gas entered by pore in reaction vessel, increase the contact area of gas and liquid in this way, Gas characteristic is moved upwards, and gas from vessel bottom is filled with the time of contact for increasing gas and solution so that reaction is more abundant, Be conducive to improving reaction yield.
In such scheme, stop valve is additionally provided with the inlet duct, the stop valve is arranged on inlet duct and reaction Near container junction, stop valve prevents liquid in experimentation from being back in air inlet pipe.
In such scheme, the intraoral wall of the upper grinding port inwall and side grinding is frosted wall.
In such scheme, grinding port plug A or return duct of the upper grinding port provided with adaptation, when being tested, when in experiment It is not required to use grinding port plug A when ventilation or not volatile material;Such as need to ventilate or there is volatile materials to use return duct, reduce volatilization The loss of property material, it is to avoid air pollution.
In such scheme, the grinding port plug B of the side grinding mouthful provided with adaptation.
In such scheme, the thermometer with sealing-plug or the TEMP with sealing-plug are provided with the temperature socket Device is popped one's head in, and reacting liquid temperature can be detected in real time, so as to controlling reaction temperature.
In summary, the beneficial effects of the utility model are:
1st, the contact area of increase gas and reaction solution, equivalent to the concentration of increase gas, and increases gas and solution Time of contact, make reaction more abundant, be conducive to improving reaction yield,.
2nd, opening up by side grinding mouthful, dropper can extend into container bottom, be easy to raw material add and sampling detection react into Stroke degree.
3rd, when needing to ventilate in experiment or having material volatile, flow tube or condenser pipe are taken back, it is to avoid the volatilization of material.
4th, reacting liquid temperature can be detected, in order to controlling reaction temperature.
Brief description of the drawings
Fig. 1:The utility model concrete structure Fig. 1
Fig. 2:The utility model concrete structure Fig. 2
Parts title wherein corresponding to reference is as follows:1- reaction vessels, 2- inlet ducts, 21- air inlet pipe, 22- gas-filling devices, 23- pores, 24- stop valves, 3- temperature sockets, 31- sealing-plugs, 32- thermometers, 4- upper grinding ports, 41- grinding port plugs A, 42- return duct, 5- side grindings mouthful, 51- grinding port plugs B.
Embodiment
For the present invention is better achieved, below in conjunction with the accompanying drawings and specific embodiment does to the present invention and said in further detail It is bright, but embodiments of the present invention are not limited to this.
Embodiment 1
As shown in figure 1, a kind of reaction unit that reaction is participated in for gas, it is characterised in that including reaction vessel 1 and entering Device of air 2, the reaction vessel top is provided with upper grinding port 4 and temperature socket 3, the radial direction lateral body of reaction vessel 1 and is additionally provided with Side grinding mouthful 5, the inlet duct 2 includes air inlet pipe 21 and the gas-filling device 22 being connected with air inlet pipe, the inlet duct 2 The radial direction lateral body bottom of reaction vessel 1 is arranged on the junction of reaction vessel 1.
It is preferred that, the gas-filling device 22 is to be provided with equally distributed pore on ring pipe, the ring pipe 23, in an experiment gas entered by pore in reaction vessel, increase the contact area of gas and liquid in this way, Gas from vessel bottom is filled with the time of contact for increasing gas and solution so that reaction is more abundant.
It is preferred that, stop valve 24 is additionally provided with the inlet duct, the stop valve 24 is arranged on inlet duct 2 and reaction Near the junction of container 1, stop valve 24 prevents liquid in experimentation from being back in air inlet pipe.
It is preferred that, the inwall of upper grinding port 4 and side grinding mouthful 5 inwalls are frosted wall.
It is preferred that, when being not required to ventilation in experiment or material is not volatile, grinding port plug of the upper grinding port 4 provided with adaptation A41。
It is preferred that, the grinding port plug B51 of the side grinding mouthful 5 provided with adaptation.
It is preferred that, the thermometer 32 with sealing-plug 31 of adaptation is provided with the temperature socket 3 or with sealing-plug 31 temperature sensing probe, reacting liquid temperature can be detected in real time, so as to controlling reaction temperature.
Below in conjunction with Fig. 1, a kind of use process for the reaction unit that reaction is participated in for gas in the present embodiment is carried out Explanation:
(1) when being tested, the liquid of experiment is passed through anti-by the grinding port plug B51 of opening side ground 5 by side grinding mouthful 5 Answer in container 1.
(2) adjustment thermometer 52 position, allows thermometer 52 to detect fluid temperature.
(3) gas of experiment is passed through air inlet pipe 21, opens stop valve 24, pass the gas through gas-filling device 22 and enter Enter in liquid.
Embodiment 2
As shown in Fig. 2 a kind of reaction unit that reaction is participated in for gas, it is characterised in that including reaction vessel 1 and entering Device of air 2, the upper end of reaction vessel 1 is provided with upper grinding port 4 and temperature socket 3, the radial direction lateral body of reaction vessel 1 and is additionally provided with Side grinding mouthful 5, the inlet duct 2 includes air inlet pipe 21 and the gas-filling device 22 being connected with air inlet pipe, the inlet duct 2 The radial direction lateral body bottom of reaction vessel 1 is arranged on the junction of reaction vessel 1.
It is preferred that, the gas-filling device 22 is to be provided with equally distributed pore on ring pipe, the ring pipe 23, in an experiment gas entered by pore in reaction vessel, increase the contact area of gas and liquid in this way, So that reaction is more abundant.
It is preferred that, stop valve 24 is additionally provided with the inlet duct 2, the stop valve 24 is arranged on inlet duct 2 and anti- Answer near the junction of container 1, stop valve 24 prevents liquid in experimentation from being back in air inlet pipe.
It is preferred that, the intraoral wall 5 of the inwall of upper grinding port 4 and side grinding is frosted wall.
It is preferred that, when having volatile materials in experiment or needing ventilation, return duct of the upper grinding port 4 provided with adaptation 42。
It is preferred that, the grinding port plug 51 of the side grinding mouthful 5 provided with adaptation.
It is preferred that, the thermometer 32 with sealing-plug 31 of adaptation is provided with the temperature socket 3 or with sealing-plug 31 temperature sensing probe, reacting liquid temperature can be detected in real time, so as to controlling reaction temperature.

Claims (7)

1. a kind of reaction unit that reaction is participated in for gas, it is characterised in that including reaction vessel (1) and inlet duct (2), Reaction vessel (1) upper end is provided with upper grinding port (4) and temperature socket (3), reaction vessel (1) the radial direction lateral body and is additionally provided with Side grinding mouthful (5), the inlet duct (2) includes air inlet pipe (21) and the gas-filling device (22) being connected with air inlet pipe (21), The inlet duct (2) is arranged on reaction vessel (1) radial direction lateral body bottom with reaction vessel (1) junction.
2. a kind of reaction unit that reaction is participated in for gas according to claim 1, it is characterised in that the gas fills Enter device (22) for ring pipe, equally distributed pore (23) is provided with the ring pipe.
3. a kind of reaction unit that reaction is participated in for gas according to claim 1, it is characterised in that the air inlet dress Put and stop valve (24) is additionally provided with (2), the stop valve (24) is arranged on inlet duct (2) and reaction vessel (1) junction is attached Closely.
4. a kind of reaction unit that reaction is participated in for gas according to claim 1, it is characterised in that the upper grinding port (4) inwall and side grinding mouthful (5) inwall are frosted wall.
5. a kind of reaction unit that reaction is participated in for gas according to claim 1, it is characterised in that the upper grinding port (4) grinding port plug A (41) or return duct (42) provided with adaptation.
6. a kind of reaction unit that reaction is participated in for gas according to claim 1, it is characterised in that the side grinding mouthful (5) the grinding port plug B (51) provided with adaptation.
7. a kind of reaction unit that reaction is participated in for gas according to claim 1, it is characterised in that the temperature is inserted The thermometer (32) with sealing-plug (31) or the temperature sensing probe with sealing-plug (31) of adaptation are provided with mouth (3).
CN201720186076.7U 2017-02-28 2017-02-28 A kind of reaction unit that reaction is participated in for gas Active CN206492490U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720186076.7U CN206492490U (en) 2017-02-28 2017-02-28 A kind of reaction unit that reaction is participated in for gas

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720186076.7U CN206492490U (en) 2017-02-28 2017-02-28 A kind of reaction unit that reaction is participated in for gas

Publications (1)

Publication Number Publication Date
CN206492490U true CN206492490U (en) 2017-09-15

Family

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Family Applications (1)

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CN201720186076.7U Active CN206492490U (en) 2017-02-28 2017-02-28 A kind of reaction unit that reaction is participated in for gas

Country Status (1)

Country Link
CN (1) CN206492490U (en)

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