CN206479383U - Sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method - Google Patents

Sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method Download PDF

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Publication number
CN206479383U
CN206479383U CN201621279384.6U CN201621279384U CN206479383U CN 206479383 U CN206479383 U CN 206479383U CN 201621279384 U CN201621279384 U CN 201621279384U CN 206479383 U CN206479383 U CN 206479383U
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China
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cylinder
fixed
homogenate
base
post
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CN201621279384.6U
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Chinese (zh)
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李梦琳
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FANGJIAPUZI (PUTIAN) GREEN FOOD CO., LTD.
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Putian Fang Shop Food Nutrition Research Center
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Abstract

The utility model provides sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method, belong to field of pesticide detection, the present apparatus includes base frame, the upper end of base frame is fixed with electric rotating machine, the machine shaft lower end of electric rotating machine is fixed with grinding stone, the casing end of electric rotating machine is fixed with a pair of connecting rods, the lower end side of connecting rod, which is fixed with, holds post one, telescoping tube is fixed with base frame lower end inner wall, the upper end of telescoping tube is fixed with base cylinder, the homogenate cylinder that cylindrical upper end is opening is connected with base cylinder, it is homogenized cylinder spacing by base cylinder, grinding stone can enter in homogenate cylinder, the outer wall of base cylinder is fixed with a pair and horizontally disposed holds post two, the one end for holding post two is connected on base drum outer wall, hold post two corresponding with holding the position of post one, the upper end cover of cylinder is homogenized provided with cover in a ring, one layer of screen pack is fixed with cover inwall.The present apparatus can realize the quick homogenate of sample, and filtration can be realized simultaneously.

Description

Sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method
Technical field
The utility model belongs to field of pesticide detection, is related to sample in a kind of garden stuff pesticide residue detection solvent extraction method even Sizing device.
Background technology
The development of agriculture industrialization makes the production of agricultural product be increasingly dependent on the allogenes such as agricultural chemicals, antibiotic and hormone Matter.China's agricultural chemicals remains high in the consumption of agricultural product, and the unreasonable use of these materials will cause the agriculture in agricultural product Medicine residual is exceeded, influences consumer's edible safety, consumer can be caused to cause a disease, develop abnormal when serious, or even directly result in It is poisoned to death.Residues of pesticides are exceeded also to influence the trade of agricultural product, and countries in the world are paid much attention to Pesticide Residue, to each Plant agricultural byproducts Pesticide Residues and all define increasingly stricter limit standard, China's Agricultural outlet is faced choosing for sternness War.
Current Fast Determination of Pesticide Residue method species is various, studies carefully and is broadly divided into two major classes for its principle:Biochemical measurement Method and chromatographic detection.Enzyme inhibition rate method wherein in biochemical assay is due to low with quick, sensitive, easy to operate, cost Honest and clean the features such as, it is listed in national proposed standard method (GB/T 5009.199-2003), it has also become to organophosphor in fruits and vegetables and ammonia Carbamate pesticide residue carries out one of mainstream technology of live fast qualitative primary dcreening operation detection, has obtained more and more widely should With.
During sample extraction, different extracting modes can be taken according to the difference of fruits and vegetables species, wherein just there is homogenate Method, current mode of operation is that related solvents and sample contents are put into bruisher to carry out homogenate a few minutes, and this kind of mode is needed To be realized using specific refiner, and the mask work of impurity and liquid can not be carried out after homogenate, and refiner is complicated, Wasted one's talent on a petty job with Detecting Pesticide.
The content of the invention
The purpose of this utility model is that there is provided a kind of garden stuff pesticide residue for the above-mentioned problems in the prior art Detect that sample homogenization apparatus can be real in sample homogenization apparatus in solvent extraction method, garden stuff pesticide residue detection solvent extraction method The quick homogenate of existing sample, filtration can be realized simultaneously, current refiner is solved and wastes one's talent on a petty job, function existing defects etc. Problem.
The purpose of this utility model can be realized by following technical proposal:A kind of garden stuff pesticide residue detects solvent extraction Sample homogenization apparatus in method, it is characterised in that:The homogenization apparatus includes base frame in the shape of a frame, and the upper end of the base frame is fixed with The electric rotating machine set straight down, the casing of the electric rotating machine is connected in the base frame upper end, the electricity of the electric rotating machine Machine rotating shaft lower end is fixed with the grinding stone in cylinder, and the casing end of the electric rotating machine is fixed with a pair straight down Connecting rod, the upper end of the connecting rod is connected on the casing of the electric rotating machine, and the lower end side of the connecting rod is fixed with Horizontally disposed to hold post one in cylinder, described one end for holding post one is connected in the connecting rod, in the base frame lower end The telescoping tube being vertically arranged is fixed with wall, the lower end of the telescoping tube is connected on the base frame, the upper end of the telescoping tube It is fixed with the base cylinder that cylindrical upper end is opening, the base cylinder and is connected with the homogenate cylinder that cylindrical upper end is opening, institute State homogenate cylinder spacing by base cylinder, the grinding stone can enter in the homogenate cylinder, the outer wall of the base cylinder is fixed with one Post two is held to horizontally disposed, described one end for holding post two is connected on the base drum outer wall, the post two of holding holds post with described One position is corresponding, and the upper end cover of the homogenate cylinder is provided with cover in a ring, the cover inwall and is fixed with one layer of filtering Net, starts electric rotating machine, the lower surface of grinding stone is ground homogenate to fruits and vegetables sample, during this period, under the active force of both hands Base cylinder is slow close by grinding stone lower surface.
This homogenization apparatus substantially using process it is as follows:When being homogenized, cover is removed, by the fruits and vegetables sample of extraction It is put into homogenate cylinder, adds corresponding solvent, then hand grip post two moves up base cylinder, while hold post one and hold post two, Start electric rotating machine, the lower surface of grinding stone is ground homogenate to fruits and vegetables sample, during this period, the base cylinder under the active force of both hands It is slow that grinding stone lower surface is close, fruits and vegetables sample is sufficiently ground homogenate, make follow-up testing result more accurate, Grind after finishing, base cylinder is moved down, homogenate cylinder is taken out, cover is covered, be inverted by cylinder will be homogenized after column casing lid, now homogenate It is filtered off, impurity is retained in homogenate cylinder, completes the collection to filtrate.The present apparatus can realize the function of refiner, while energy Filtering function is enough played, grinding refinement is realized by manual compression, apparatus structure is simple, and effect is notable.
Sample homogenization apparatus, the lower end of the machine shaft in a kind of above-mentioned garden stuff pesticide residue detection solvent extraction method End outer wall, which is fixed with the retainer ring in annular, the retainer ring, has several screwed holes one, has on the grinding stone Several screwed holes two.
Retainer ring is welded on machine shaft, and the fixation of machine shaft and grinding stone is realized by screwed hole one and screwed hole two Connection.
Sample homogenization apparatus in a kind of above-mentioned garden stuff pesticide residue detection solvent extraction method, the upper end of the homogenate cylinder is convex Go out the upper end of the base cylinder.
Homogenate cylinder is set conveniently to be removed.
On sample homogenization apparatus in a kind of above-mentioned garden stuff pesticide residue detection solvent extraction method, the base cylinder both sides inwall With breach, there is fixture block on the both sides outer wall of the homogenate cylinder, the fixture block is located in the breach, the both sides of the cover With entering portion with the fixture block shape identical lid, it is described cover portion can cover set with the fixture block.
Clamping between homogenate cylinder and base cylinder is realized by the setting of fixture block and breach, grinding stone is not driven homogenate cylinder hair It is raw to rotate.Cover the setting in portion enable cover cover be located at homogenate cylinder on.
Sample homogenization apparatus in a kind of above-mentioned garden stuff pesticide residue detection solvent extraction method, the telescoping tube includes fixing Portion and pars contractilis, the lower end of the fixed part are connected on the base frame, and the upper end of the fixed part is opening and inner wall of end The gear in annular is fixed with along one, the upper end of the pars contractilis is connected in the base cylinder bottom, the lower end end of the pars contractilis Portion's outer wall is fixed with the gear in annular along two, and the gear is located in the fixed part along two.
The Telescopic of telescoping tube is realized by fixed part and pars contractilis.
Compared with prior art, this garden stuff pesticide residue detection solvent extraction method in sample homogenization apparatus have it is following excellent Point:
1st, sample homogenization apparatus can realize the quick homogenate of sample, energy in this garden stuff pesticide residue detection solvent extraction method It is enough to realize filtration simultaneously.
2nd, sample homogenization apparatus realizes grinding refinement by manual compression in this garden stuff pesticide residue detection solvent extraction method, Apparatus structure is simple, and effect is notable.
Brief description of the drawings
Fig. 1 is the structural representation of sample homogenization apparatus in this garden stuff pesticide residue detection solvent extraction method.
Fig. 2 is electric rotating machine and associated component in sample homogenization apparatus in this garden stuff pesticide residue detection solvent extraction method Structural representation.
Fig. 3 is that this garden stuff pesticide residue detects that the structure of homogenate cylinder and cover in sample homogenization apparatus in solvent extraction method is quick-fried Fried figure.
Fig. 4 is the structural representation that this garden stuff pesticide residue detects base cylinder in sample homogenization apparatus in solvent extraction method.
Fig. 5 is the Structure explosion diagram that this garden stuff pesticide residue detects telescoping tube in sample homogenization apparatus in solvent extraction method.
In figure, 1, base frame;2nd, electric rotating machine;3rd, machine shaft;4th, grinding stone;4a, screwed hole two;5th, connecting rod;6th, post is held One;7th, telescoping tube;7a, fixed part;7a1, keep off along one;7b, pars contractilis;7b1, keep off along two;8th, base cylinder;8a, breach;9th, it is homogenized Cylinder;9a, fixture block;10th, post two is held;11st, cover;11a, cover into portion;12nd, screen pack;13rd, retainer ring;13a, screwed hole one.
Embodiment
As shown in Figures 1 to 5, this garden stuff pesticide residue detects that sample homogenization apparatus is including in the shape of a frame in solvent extraction method Base frame 1, the upper end of base frame 1 is fixed with the electric rotating machine 2 set straight down, and the casing of electric rotating machine 2 is connected on base frame 1 End, the lower end of machine shaft 3 of electric rotating machine 2 is fixed with the grinding stone 4 in cylinder, and the casing end of electric rotating machine 2 is connected There are a pair of connecting rods 5 straight down, the upper end of connecting rod 5 is connected on the casing of electric rotating machine 2, the lower end one of connecting rod 5 Side be fixed with it is horizontally disposed in cylinder hold post 1, the one end for holding post 1 is connected in connecting rod 5, in the lower end of base frame 1 The telescoping tube 7 being vertically arranged is fixed with wall, the lower end of telescoping tube 7 is connected on base frame 1, and the upper end of telescoping tube 7, which is fixed with, is in Cylindrical top for opening base cylinder 8, base cylinder 8 in be connected with cylindrical upper end be opening homogenate cylinder 9, homogenate cylinder 9 by Base cylinder is 8 spacing, and grinding stone 4 can enter in homogenate cylinder 9, the outer wall of base cylinder 8 be fixed with a pair it is horizontally disposed hold post 2 10, hold post 2 10 one end is connected on base 8 outer walls of cylinder, holds that post 2 10 is corresponding with holding the position of post 1, the upper end cover for being homogenized cylinder 9 is provided with One layer of screen pack 12 is fixed with cover 11 in a ring, the inwall of cover 11.
This homogenization apparatus substantially using process it is as follows:When being homogenized, cover 11 is removed, by the fruits and vegetables of extraction Sample is put into homogenate cylinder 9, adds corresponding solvent, and then hand grip post 2 10 moves up base cylinder 8, while holding post 1 With hold post 2 10, start electric rotating machine 2, the lower surface of grinding stone 4 is ground homogenate to fruits and vegetables sample, during this period, in both hands Active force under base cylinder 8 it is slow that the lower surface of grinding stone 4 is close, fruits and vegetables sample is sufficiently ground homogenate, make follow-up Testing result is more accurate, after grinding is finished, and base cylinder 8 is moved down, and homogenate cylinder 9 is taken out, cover 11 is covered, after column casing lid 11 Homogenate cylinder 9 is inverted, now homogenate is filtered off, impurity is retained in homogenate cylinder 9, completes the collection to filtrate.Present apparatus energy The function of refiner is enough realized, while filtering function can be played, grinding refinement, apparatus structure letter are realized by manual compression Single, effect is notable.
The lower end outer wall of machine shaft 3, which is fixed with the retainer ring 13 in annular, retainer ring 13, has several There is several screwed holes two 4a on the 13a of screwed hole one, grinding stone 4.Retainer ring 13 is welded on machine shaft 3, passes through screwed hole One 13a and the 4a of screwed hole two realize being fixedly connected for machine shaft 3 and grinding stone 4.
It is homogenized the upper end of the upper end protrusion base cylinder 8 of cylinder 9.Homogenate cylinder 9 is set conveniently to be removed.
There is breach 8a on base 8 both sides inwalls of cylinder, being homogenized on the both sides outer wall of cylinder 9 has fixture block 9a, fixture block 9a, which is located at, to be lacked In mouthful 8a, the both sides of cover 11 have enters portion 11a with fixture block 9a shape identical lids, covers to cover into portion 11a and sets and fixture block 9a On.Clamping between homogenate cylinder 9 and base cylinder 8 is realized by fixture block 9a and breach 8a setting, grinding stone 4 is not driven homogenate cylinder 9 rotate.Cover portion 11a setting enable cover 11 cover be located at homogenate cylinder 9 on.
Telescoping tube 7 includes fixed part 7a and pars contractilis 7b, and fixed part 7a lower end is connected on base frame 1, fixed part 7a's Upper end is opening and inner wall of end is fixed with the gear in annular along a 7a1, and pars contractilis 7b upper end is connected in 8 bottoms of base cylinder, Pars contractilis 7b lower end outer wall is fixed with the gear in annular along two 7b1, and gear is located in fixed part 7a along two 7b1.Pass through Fixed part 7a and pars contractilis 7b realize the Telescopic of telescoping tube 7.
Sample homogenization apparatus can realize the quick homogenate of sample in this garden stuff pesticide residue detection solvent extraction method, can Realize filtration simultaneously.
Specific embodiment described herein is only to the utility model spirit explanation for example.The utility model institute Category those skilled in the art can make various modifications or supplement or using similar to described specific embodiment Mode substitute, but without departing from spirit of the present utility model or surmount scope defined in appended claims.

Claims (5)

1. sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method, it is characterised in that:The homogenization apparatus bag Base frame in the shape of a frame is included, the upper end of the base frame is fixed with the electric rotating machine set straight down, the casing of the electric rotating machine The base frame upper end is connected in, the machine shaft lower end of the electric rotating machine is fixed with the grinding stone in cylinder, the rotation The casing end of rotating motor is fixed with a pair of connecting rods straight down, and the upper end of the connecting rod is connected in the electric rotating machine Casing on, the lower end side of the connecting rod be fixed with it is horizontally disposed hold post one in cylinder, it is described to hold the one of post one End is connected in the connecting rod, is fixed with the base frame lower end inner wall under the telescoping tube being vertically arranged, the telescoping tube End is connected on the base frame, and the upper end of the telescoping tube is fixed with the base cylinder that cylindrical upper end is opening, the base cylinder The homogenate cylinder that cylindrical upper end is opening is connected with, the homogenate cylinder is spacing by base cylinder, and the grinding stone can enter In the homogenate cylinder, the outer wall of base cylinder be fixed with a pair it is horizontally disposed hold post two, described one end for holding post two is connected in On the base drum outer wall, the post two of holding holds that the position of post one is corresponding with described, and the upper end cover of the homogenate cylinder is provided with a ring Cover, one layer of screen pack is fixed with the cover inwall, starts electric rotating machine, the lower surface of grinding stone is carried out to fruits and vegetables sample Grinding homogenate, during this period, base cylinder is slow close by grinding stone lower surface under the active force of both hands.
2. sample homogenization apparatus, its feature in a kind of garden stuff pesticide residue detection solvent extraction method according to claim 1 It is, the lower end outer wall of the machine shaft, which is fixed with the retainer ring in annular, the retainer ring, has several There are several screwed holes two on screwed hole one, the grinding stone.
3. sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method according to claim 1 or 2, it is special Levy and be, the upper end of the base cylinder is protruded in the upper end of the homogenate cylinder.
4. sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method according to claim 1 or 2, it is special Levy and be, having on the base cylinder both sides inwall on breach, the both sides outer wall of the homogenate cylinder has fixture block, and the fixture block is located at In the breach, the both sides of the cover have enters portion with the fixture block shape identical lid, it is described cover can be covered into portion set with On the fixture block.
5. sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method according to claim 1 or 2, it is special Levy and be, the telescoping tube includes fixed part and pars contractilis, the lower end of the fixed part is connected on the base frame, the fixation The upper end in portion is opening and inner wall of end is fixed with the gear in annular along one, and the upper end of the pars contractilis is connected in the base cylinder Bottom, the lower end outer wall of the pars contractilis is fixed with the gear in annular along two, and the gear is located at the fixed part along two It is interior.
CN201621279384.6U 2016-11-25 2016-11-25 Sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method Expired - Fee Related CN206479383U (en)

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CN201621279384.6U CN206479383U (en) 2016-11-25 2016-11-25 Sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method

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Application Number Priority Date Filing Date Title
CN201621279384.6U CN206479383U (en) 2016-11-25 2016-11-25 Sample homogenization apparatus in a kind of garden stuff pesticide residue detection solvent extraction method

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108426756A (en) * 2018-05-15 2018-08-21 常州市金坛区农产品质量检验检测中心 A kind of differential speed change broken wall filtering all-in-one machine of fruits and vegetables sample homogenization
CN108693321A (en) * 2018-06-05 2018-10-23 深圳市安思科电子科技有限公司 A kind of Detecting Pesticide pretreatment unit
CN109490493A (en) * 2018-11-14 2019-03-19 望江县同心农业专业合作社 A kind of pesticide residue detection method
CN109490492A (en) * 2018-11-14 2019-03-19 望江县同心农业专业合作社 A kind of Pesticides Testing equipment

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108426756A (en) * 2018-05-15 2018-08-21 常州市金坛区农产品质量检验检测中心 A kind of differential speed change broken wall filtering all-in-one machine of fruits and vegetables sample homogenization
CN108693321A (en) * 2018-06-05 2018-10-23 深圳市安思科电子科技有限公司 A kind of Detecting Pesticide pretreatment unit
CN108693321B (en) * 2018-06-05 2020-11-13 普研(上海)标准技术服务股份有限公司 Pesticide residue detects preprocessing device
CN109490493A (en) * 2018-11-14 2019-03-19 望江县同心农业专业合作社 A kind of pesticide residue detection method
CN109490492A (en) * 2018-11-14 2019-03-19 望江县同心农业专业合作社 A kind of Pesticides Testing equipment
CN109490493B (en) * 2018-11-14 2021-05-11 云南孚尔质量检验检测有限公司 Pesticide residue detection method
CN109490492B (en) * 2018-11-14 2021-08-10 绍兴锦绣农业开发有限公司 Pesticide check out test set

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Date Code Title Description
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20190522

Address after: 351100 No. 1758 Chenghan East Avenue, Hanjiang District, Putian City, Fujian Province

Patentee after: FANGJIAPUZI (PUTIAN) GREEN FOOD CO., LTD.

Address before: 351100 Fujian Province Putian City Chengxiang District Licheng Middle Avenue 1539 Building 2 Ladder 1002

Patentee before: Putian Fang shop food nutrition research center

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170908

Termination date: 20191125