CN206444468U - Ammoniacal liquor preparation facilities - Google Patents

Ammoniacal liquor preparation facilities Download PDF

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Publication number
CN206444468U
CN206444468U CN201720111137.3U CN201720111137U CN206444468U CN 206444468 U CN206444468 U CN 206444468U CN 201720111137 U CN201720111137 U CN 201720111137U CN 206444468 U CN206444468 U CN 206444468U
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CN
China
Prior art keywords
ammonia
liquefied ammonia
ammoniacal liquor
tank
water inlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720111137.3U
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Chinese (zh)
Inventor
韩伟国
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lianyungang Heng Trade Chemical Co Ltd
Original Assignee
Lianyungang Heng Trade Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lianyungang Heng Trade Chemical Co Ltd filed Critical Lianyungang Heng Trade Chemical Co Ltd
Priority to CN201720111137.3U priority Critical patent/CN206444468U/en
Application granted granted Critical
Publication of CN206444468U publication Critical patent/CN206444468U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of ammoniacal liquor preparation facilities, including liquefied ammonia blending tank, ammonia sprayed tank and ammoniacal liquor holding vessel, in liquefied ammonia mixing pot sidewall, liquefied ammonia inlet tube, water inlet pipe are set, liquefied ammonia mixing pot bottom sets outlet pipe, outlet pipe connects ammoniacal liquor holding vessel, the liquefied ammonia inlet pipes are extended downwardly into below liquefied ammonia mixing jar liquid surface in one end in blending tank, and the ammoniacal liquor shunt cylinder for having some apertures on a side wall is set in liquefied ammonia inlet tube lower end.The utility model realizes the quick dissolving of liquefied ammonia by setting ammoniacal liquor shunt cylinder in liquefied ammonia inlet tube bottom;Water inlet is tangentially set, and makes mixed liquor formation vortex, is realized self stirring mixing, is improved dissolved efficiency;Set a sprayed tank to make the ammonia of effusion to be recycled, and the organic efficiency of turbine acceleration gas is set.The utility model is simple in construction, easy to use, good cooling effect, and ammoniacal liquor yield is high, safe.

Description

Ammoniacal liquor preparation facilities
Technical field
The utility model is related to ammoniacal liquor preparing technical field, more specifically to a kind of liquefied ammonia formula ammoniacal liquor preparing device.
Background technology
Liquefied ammonia is the important raw material of industry, is widely used in pharmacy, oil refining, synthetic fibers, synthetic resin, freezing, metallurgy In terms of.Liquefied ammonia synthesizes the compressed obtained liquefied ammonia product of ammonia by professional production producer, be reloaded into special steel cylinder or tank car by Highway and railway transportation are to each producer user, to produce various products as the raw material of industry.It is general be in the industrial production by Liquefied ammonia is dissolved in water and is made into industrial ammonia to use.
In the configuration process of ammoniacal liquor, when liquefied ammonia is dissolved in water, substantial amounts of heat can be produced, it is dangerous higher, if dissipated Heat not in time, then influences whether personal safety.And understand some ammonia and escaped from ammoniacal liquor, if this portion gas is directly arranged Put, not only waste material, thereby increases and it is possible to which meeting environment is polluted.
Utility model content
The purpose of this utility model is a kind of liquefied ammonia formula ammoniacal liquor preparing device of offer, it is intended to solved present in prior art Cooling effect is poor, the problem of security is low.
To achieve the above object, the utility model provides following technical scheme:
A kind of ammoniacal liquor preparation facilities, including liquefied ammonia blending tank, ammonia sprayed tank and ammoniacal liquor holding vessel, in liquefied ammonia blending tank side Wall sets liquefied ammonia inlet tube, water inlet pipe, and liquefied ammonia mixing pot bottom sets outlet pipe, outlet pipe connection ammoniacal liquor holding vessel, the liquid Ammonia inlet pipes are extended downwardly into below liquefied ammonia mixing jar liquid surface in one end in blending tank, and one is set in liquefied ammonia inlet tube lower end There is the ammoniacal liquor shunt cylinder of some apertures on the wall of side, described water inlet pipe is set in the part of tank interior along tank body tangential direction, The delivery port of water inlet pipe is slightly below liquefied ammonia mixing jar liquid surface;
Gas outlet is set at the top of liquefied ammonia blending tank, and gas outlet connection escape pipe, escape pipe connects ammonia sprayed tank Air inlet, the delivery port of ammonia sprayed tank is connected with ammoniacal liquor holding vessel by pipeline, valve is set on pipeline, on escape pipe Also set up and the first turbine is set in air chamber, air chamber, the second turbine is set in water inlet pipe, and two turbines are mutual by transmission device Connection.
Cooling device is set on liquefied ammonia mixing tank wall, and cooling device is panel radiator, described panel radiator Thermal insulation layer is laid in outside.
The rotating ratio of first turbine and the second turbine is 3:1.
Water inlet and circulated sprinkling pipe are also set up on described ammonia sprayed tank, water inlet is arranged on ammonia spray pot sidewall On, water inlet is connected by pipeline with the water inlet pipe of liquefied ammonia blending tank, and ammonia spray upper end sets spray head, circulated sprinkling pipe One end connects spray head, and the other end connects the pipeline of ammonia sprayed tank water outlet, and it is dense to also set up ammoniacal liquor in ammonia sprayed tank Degree meter.
It is of the present utility model to be beneficial in that:By setting ammoniacal liquor shunt cylinder in liquefied ammonia inlet tube bottom so that its energy It is enough that uniformly liquefied ammonia is injected in water, realize the quick dissolving of liquefied ammonia;Water inlet is tangentially set, and makes mixed liquor formation whirlpool Stream, realizes self stirring mixing, improves dissolved efficiency;Set a sprayed tank to make the ammonia of effusion to be recycled, and set Put the organic efficiency that turbine accelerates gas.The utility model is simple in construction, easy to use, good cooling effect, and ammoniacal liquor yield is high, peace Quan Xinggao.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Wherein 1- liquefied ammonia blending tank, 2- ammonias sprayed tank, 3- ammoniacal liquor holding vessel, 4- liquefied ammonia inlet tube, 5- shunt cylinders, 6- enter Water pipe, the turbines of 7- first, the turbines of 8- second, 9- outlet pipes, 10- circulated sprinkling pipes, 11- ammonia concns meter, 12- plate type radiators Device.
Embodiment
The utility model is described in further detail with reference to Figure of description:
The utility model is related to a kind of preparation facilities of ammoniacal liquor, specifically, is that one kind mainly utilizes liquefied ammonia, ammonia conduct The preparation facilities of the ammoniacal liquor of auxiliary, it is prepared the liquefied ammonia blending tank 1 of ammoniacal liquor as raw material using liquefied ammonia, prepared using ammonia The ammonia sprayed tank 2 of ammoniacal liquor and the ammoniacal liquor holding vessel 3 for storing finished product ammoniacal liquor, on liquefied ammonia blending tank 1, are provided with liquefied ammonia inlet tube 4th, water inlet pipe 6, by the way that liquefied ammonia is mixed with pure water, so that the ammoniacal liquor product of output prescribed concentration, the finished product being mixed to get The outlet pipe 9 that ammoniacal liquor is set by liquefied ammonia mixing pot bottom, which is passed through in ammoniacal liquor holding vessel 3, to be stored, and ammoniacal liquor holding vessel 3 passes through The device of related constant temperature and pressure is set to ensure the constant of storage environment.
In the utility model, the liquid level of blending tank is stretched into one end that described liquefied ammonia inlet tube 4 is located in liquefied ammonia blending tank Hereinafter, so make liquefied ammonia directly carry out contact with pure water to mix, be not in, in order to make liquefied ammonia more uniformly be mixed, It can be installed additional in the lower end of liquefied ammonia inlet tube and be uniformly arranged aperture, such liquefied ammonia on a shunt cylinder 5, the side wall of shunt cylinder 5 Ensure that it keeps less flow and slower flow velocity when being overflowed from aperture, what the liquefied ammonia and water for increasing unit capacity were contacted Area, ammoniacal liquor mixing is abundant.
In order to further lift ammoniacal liquor mixed effect, the water outlet direction of water inlet pipe 6 can be also set to along liquefied ammonia blending tank tank The tangential direction of body, so the mouth of pipe of water inlet pipe 6 is also disposed under liquid level at the same time, the current meeting so discharged from water inlet pipe Make the mixed solution in tank body carry out rotation and form vortex, realize stirring certainly for mixed solution, mixed effect is more notable.
Because liquefied ammonia is dissolved in after water, substantial amounts of heat can be produced, these heats cannot be distributed.Substantial amounts of ammonia can be made from ammonia Dissipated in water, directly contribute the quality reduction of ammoniacal liquor;And liquefied ammonia blending tank pot temperature is high, easily to operator in regular job Member causes damage, in this regard, setting cooling device on the outer wall of liquefied ammonia blending tank, sets cooling device one is in order to liquefied ammonia Ammonia water mixture in blending tank is cooled down, the second is control ammoniacal liquor cools down the surface temperature of tank, to protect operator The personal safety of member.In the utility model, by being dropped in liquefied ammonia mixing tank wall arranging plate formula radiator 12 to tank body Temperature processing, is so just isolated liquefied ammonia blending tank outer wall section, one sufficiently can ensure in tank with the external world completely Ammoniacal liquor is adequately cooled, secondly can also ensure that the tank body of liquefied ammonia blending tank is not exposed to the external world, will not scald operating personnel Wound, further, also lays thermal insulation layer, its thermal insulation effect becomes apparent on the outside of described panel radiator.
The unnecessary ammonia produced during mixing ammoniacal liquor is discharged by the gas outlet at the top of liquefied ammonia blending tank, and in ammonia sprayed tank Middle carry out spray-absorption, forms weak aqua ammonia, so unnecessary ammonia is absorbed, the waste of raw material is on the one hand avoided, On the other hand it also avoid the pollution of environment.Because the ammonia amount entered in ammonia spray tank is less than the uptake of shower water, because Negative pressure state is continuously in this ammonia spray tank, therefore spray-absorption step lasts are carried out, the utility model is mixed in liquefied ammonia One air chamber is set on the pipeline set between tank and ammonia sprayed tank, the first turbine 7 is set in air chamber, it is corresponding, The second turbine 8 is provided with water inlet pipe, two turbines are connected by transmission device, when spraying process progress, due to ammonia When air-flow is through air chamber, with setting the first turbine 7 therein to collide, the concomitant rotation of the first turbine 7, turn of the first turbine are caused The rotation of the second turbine 8 of dynamic drive, so as to accelerate the flowing of the water in water inlet pipe, under certain condition, can be situated between without water pump Enter to make water to accelerate flowing, so that the energy is saved, conversely, when water pump intervenes the water flowing accelerated in water inlet pipe, also The first turbine 7 can be driven to accelerate the flowing of ammonia, so as to add the absorption efficiency of ammonia.Further, due to liquid plus Speed accelerates compared to gas, and it needs to expend more energy, therefore the rotation of the first turbine 7 and the second turbine 8 is compared for 3:1, Meanwhile, transmission device can be arranged into power according to the actual requirements can be disengaged, it is to avoid when being intervened because of water pump full-speed operation, First turbine rotates the damage for initiation of overrunning.
On described ammonia sprayed tank, a water inlet is set, water inlet equally connects with the water inlet pipe 6 on ammoniacal liquor blending tank Connect, water inlet is arranged on the side wall of ammonia spray tank, and water inlet is set higher than tank level, it is to avoid because ammoniacal liquor falls Stream causes unnecessary pollution, and spray head is set at the top of ammonia sprayed tank, and its bottom sets delivery port, and delivery port is stored up with ammoniacal liquor Deposit tank to connect by pipeline, a circulated sprinkling pipe 10 is set on spray head and pipeline, circulated sprinkling pipe 10 is by ammonia spray Ammoniacal liquor in tank 2 is sprayed repeatedly, to play the uptake that its is maximum, while setting ammoniacal liquor in the tank body of ammonia sprayed tank 2 Densimeter 11, when in ammonia spray tank ammonia concn and ammonia concn in ammoniacal liquor holding vessel it is mutually fair or closely when, Then ammoniacal liquor is passed through in ammoniacal liquor holding vessel.It is corresponding, it is respectively provided with controllable electricity on all pipelines set on ammonia sprayed tank Magnet valve.

Claims (4)

1. a kind of ammoniacal liquor preparation facilities, it is characterised in that:Including liquefied ammonia blending tank, ammonia sprayed tank and ammoniacal liquor holding vessel, in liquid Ammonia mixing pot sidewall sets liquefied ammonia inlet tube, water inlet pipe, and liquefied ammonia mixing pot bottom sets outlet pipe, outlet pipe connection ammoniacal liquor storage Tank, the liquefied ammonia inlet pipes are extended downwardly into below liquefied ammonia mixing jar liquid surface in one end in blending tank, under liquefied ammonia inlet tube End, which is set, the ammoniacal liquor shunt cylinders of some apertures on a side wall, described water inlet pipe is in the part of tank interior along tank body tangent line Direction is set, and the delivery port of water inlet pipe is slightly below liquefied ammonia mixing jar liquid surface;
Gas outlet is set at the top of liquefied ammonia blending tank, and gas outlet connection escape pipe, escape pipe connects the air inlet of ammonia sprayed tank Mouthful, the delivery port of ammonia sprayed tank is connected by pipeline with ammoniacal liquor holding vessel, valve is set on pipeline, is also set on escape pipe Put and the first turbine is set in air chamber, air chamber, the second turbine is set in water inlet pipe, and two turbines are mutually interconnected by transmission device Connect.
2. preparation facilities according to claim 1, it is characterised in that:Cooling device is set on liquefied ammonia mixing tank wall, Cooling device is panel radiator, and thermal insulation layer is laid on the outside of panel radiator.
3. preparation facilities according to claim 1, it is characterised in that:The rotating ratio of first turbine and the second turbine is 3:1.
4. preparation facilities according to claim 1, it is characterised in that:Also set up on described ammonia sprayed tank water inlet and Circulated sprinkling pipe, water inlet is arranged on ammonia spray pot sidewall, and water inlet is connected by the water inlet pipe of pipeline and liquefied ammonia blending tank Connect, ammonia spray upper end sets spray head, circulated sprinkling pipe one end connection spray head, other end connection ammonia sprayed tank water outlet Pipeline at mouthful, also sets up ammonia concn meter in ammonia sprayed tank.
CN201720111137.3U 2017-02-07 2017-02-07 Ammoniacal liquor preparation facilities Expired - Fee Related CN206444468U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720111137.3U CN206444468U (en) 2017-02-07 2017-02-07 Ammoniacal liquor preparation facilities

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720111137.3U CN206444468U (en) 2017-02-07 2017-02-07 Ammoniacal liquor preparation facilities

Publications (1)

Publication Number Publication Date
CN206444468U true CN206444468U (en) 2017-08-29

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720111137.3U Expired - Fee Related CN206444468U (en) 2017-02-07 2017-02-07 Ammoniacal liquor preparation facilities

Country Status (1)

Country Link
CN (1) CN206444468U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115121205A (en) * 2022-07-07 2022-09-30 唐山国环环保科技有限公司 Device for preparing ammonia water from liquid ammonia

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115121205A (en) * 2022-07-07 2022-09-30 唐山国环环保科技有限公司 Device for preparing ammonia water from liquid ammonia

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170829

Termination date: 20200207