CN206404363U - A kind of efficient low melting point organic matter crystallization apparatus - Google Patents
A kind of efficient low melting point organic matter crystallization apparatus Download PDFInfo
- Publication number
- CN206404363U CN206404363U CN201720074268.9U CN201720074268U CN206404363U CN 206404363 U CN206404363 U CN 206404363U CN 201720074268 U CN201720074268 U CN 201720074268U CN 206404363 U CN206404363 U CN 206404363U
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- chamber
- filter
- cushion chamber
- cooling chamber
- diversion cavity
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Abstract
The utility model is related to field of chemical equipment, specifically related to a kind of efficient low melting point organic matter crystallization apparatus, including diversion cavity, cooling chamber, cushion chamber and filter, the cooling chamber is set in outside the cushion chamber, the diversion cavity is arranged on the cushion chamber top, and the filter is arranged on the cushion chamber lower end；Bucking ladder is provided with the diversion cavity, the bucking ladder bottom surface is arranged at the top of the cushion chamber；Connected on the inside of the cooling chamber with the cushion chamber, the cooling chamber top is connected with the diversion cavity；Multiple condenser pipes are provided with the cooling chamber, is provided between the cushion chamber and filter in regulating valve, the filter and is provided with screen pack.The utility model is equipped with using cooling chamber and cushion chamber, and the effect for first cool down and settling afterwards is formed in the presence of diversion cavity, can accelerating liquid cooling, the effect for passing through filter carries out fast filtering, collects and crystallize.
Description
Technical field
The utility model is related to field of chemical equipment, and in particular to a kind of efficient low melting point organic matter crystallization apparatus.
Background technology
During medicine, the manufacturing of fine chemical industry, there are a series of organic compounds, its fusing point is in 40~60
Between degree Celsius, sterling is in crystal state at normal temperatures, but purity is not enough or easily bond vitrified during summer high-temperature, causes transhipment
It is inaccurate with measuring.And this type organic is possible in Crystallizing process because crystallization is impure, or in centrifugal process
Melt because environment temperature rise and residual solvent are not dried in time and at once, it is difficult to separate.For this problem, one kind is needed badly
Low temperature crystallization equipment, makes rapid crystallization, and facilitate postorder to separate and dispel residual solvent.
The content of the invention
For the defect and deficiency of prior art, the purpose of this utility model is：A kind of simple in construction, design is provided to close
Reason, low melting point organic matter crystallization apparatus easy to use, the utility model are equipped with using cooling chamber and cushion chamber, are being led
Form the effect for first cool down and settling afterwards in the presence of stream chamber, can accelerating liquid cooling, and carried out soon by the effect of filter
Speed filtering, collects crystallization.
To achieve the above object, the technical solution adopted in the utility model is：
The efficient low melting point organic matter crystallization apparatus of the utility model, including diversion cavity, cooling chamber, cushion chamber and filtering
Device, the cooling chamber is set in outside the cushion chamber, and the diversion cavity is arranged on the cushion chamber top, and the filter is set
Put in the cushion chamber lower end；Bucking ladder is provided with the diversion cavity, the bucking ladder bottom surface is arranged at the cushion chamber top
Portion；Connected on the inside of the cooling chamber with the cushion chamber, the cooling chamber top is connected with the diversion cavity；In the cooling chamber
Multiple condenser pipes are provided with, is provided between the cushion chamber and filter in regulating valve, the filter and is provided with screen pack；
This programme is equipped with using cooling chamber and cushion chamber, realizes that overall cooling cools with radial flow in the presence of diversion cavity,
Formed and first cool down the effect that settles afterwards, can accelerating liquid cooling, the effect for passing through filter carries out fast filtering, collects and tie
It is brilliant；Diversion cavity is arranged on using bucking ladder, liquid can be flowed into along edge, plays a part of control flow direction.
It is preferred that, the bucking ladder is closed truncated cone or round platform, is more preferably inverted.
It is preferred that, the filter upper end is provided with thread groove, can be fixed on filter by the setting of thread groove
In regulating valve, the dismounting of filter can be easy to by thread groove, be easy to crystallization to collect.
It is preferred that, dividing plate is provided between the cooling chamber and cushion chamber, the dividing plate lower end is provided with space；Using every
The setting of plate ensure that liquid is tried one's best in cooling chamber and stop for a long time, it is ensured that the cooling effect and crystallization effect of liquid.
After said structure, the utility model has the beneficial effect that：
The utility model is equipped with using cooling chamber and cushion chamber, realized in the presence of diversion cavity overall cooling with
Radial flow cools, and is formed and first cool down the effect that settles afterwards, can accelerating liquid cooling, pass through the quick mistake of effect progress of filter
Filter, collect crystallization, and with easy to use, simple to operate, practicality it is good, it is with low cost the features such as.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Description of reference numerals：
1st, diversion cavity；2nd, cooling chamber；3rd, cushion chamber；4th, filter；5th, regulating valve；6th, bucking ladder；7th, condenser pipe；8th, every
Plate；9th, screen pack.
Embodiment
The utility model is further described below in conjunction with the accompanying drawings.
As shown in figure 1, the efficient low melting point organic matter crystallization apparatus of the utility model, including diversion cavity（1）, cooling chamber
（2）, cushion chamber（3）And filter（4）, the cooling chamber（2）It is set in the cushion chamber（3）Outside, the diversion cavity（1）If
Put in the cushion chamber（3）Top, the filter（4）It is arranged on the cushion chamber（3）Lower end；The diversion cavity（1）Inside set
It is equipped with bucking ladder（6）, the bucking ladder（6）Bottom surface is arranged at the cushion chamber（3）Top；The cooling chamber（2）Outside is with
End is closed, its inner side and the cushion chamber（3）Connection, its top and the diversion cavity（1）Connection；The cooling chamber（2）Inside set
It is equipped with multiple condenser pipes（7）, the cushion chamber（3）With filter（4）Between be provided with regulating valve（5）, the filter（4）It is interior
It is provided with screen pack（9）.
The bucking ladder（6）For closed inverted round table.The filter（4）Upper end is provided with thread groove, passes through screw thread
Filter can be fixed in regulating valve by the setting of groove, can be easy to the dismounting of filter by thread groove, be easy to crystallization to receive
Collection.The cooling chamber（2）With cushion chamber（3）Between be provided with dividing plate（8）, the dividing plate（8）Lower end is provided with space；Using every
The setting of plate ensure that liquid is tried one's best in cooling chamber and stop for a long time, it is ensured that the cooling effect and crystallization effect of liquid.Institute
State cushion chamber（3）Top is closed, lower sides and cooling chamber（2）Connection, lower end passes through regulating valve and filter（4）Connection.
During use, synthetic solvent is poured onto diversion cavity（1）In bucking ladder（6）On, make liquid along marginal flow
Enter, into cooling chamber（2）, then condensed pipe cooling after enter cushion chamber from the space of the lower partition, the crystallization of formation passed through
Filter screen is collected.
Described above is only better embodiment of the present utility model, therefore all according to described in the utility model patent claim
The equivalent change or modification done of construction, feature and principle, be included in the utility model patent claim.
Claims (5)
1. a kind of efficient low melting point organic matter crystallization apparatus, it is characterised in that：Including diversion cavity（1）, cooling chamber（2）, buffering
Chamber（3）And filter（4）, the cooling chamber（2）It is set in the cushion chamber（3）Outside, the diversion cavity（1）It is arranged on described
Cushion chamber（3）Top, the filter（4）It is arranged on the cushion chamber（3）Lower end；The diversion cavity（1）Inside it is provided with trapezoidal
Platform（6）, the bucking ladder（6）Bottom surface is arranged at the cushion chamber（3）Top；The cooling chamber（2）Inner side and the cushion chamber
（3）Connection, the cooling chamber（2）Top and the diversion cavity（1）Connection；The cooling chamber（2）Inside it is provided with multiple condenser pipes
（7）, the cushion chamber（3）With filter（4）Between be provided with regulating valve（5）, the filter（4）Inside it is provided with screen pack
（9）.
2. efficient low melting point organic matter crystallization apparatus according to claim 1, it is characterised in that：The bucking ladder（6）For
Closed truncated cone or round platform.
3. efficient low melting point organic matter crystallization apparatus according to claim 2, it is characterised in that：The bucking ladder（6）For
Inverted truncated cone or round platform.
4. efficient low melting point organic matter crystallization apparatus according to claim 1, it is characterised in that：The filter（4）On
End is provided with thread groove, with the regulating valve（5）It is flexibly connected.
5. efficient low melting point organic matter crystallization apparatus according to claim 1, it is characterised in that：The cooling chamber（2）With
Cushion chamber（3）Between be provided with dividing plate（8）, the dividing plate（8）Lower end is provided with space.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720074268.9U CN206404363U (en) | 2017-01-21 | 2017-01-21 | A kind of efficient low melting point organic matter crystallization apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720074268.9U CN206404363U (en) | 2017-01-21 | 2017-01-21 | A kind of efficient low melting point organic matter crystallization apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206404363U true CN206404363U (en) | 2017-08-15 |
Family
ID=59557079
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720074268.9U Active CN206404363U (en) | 2017-01-21 | 2017-01-21 | A kind of efficient low melting point organic matter crystallization apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206404363U (en) |
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2017
- 2017-01-21 CN CN201720074268.9U patent/CN206404363U/en active Active
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