CN206355642U - A kind of novel extraction apparatus - Google Patents
A kind of novel extraction apparatus Download PDFInfo
- Publication number
- CN206355642U CN206355642U CN201621461144.8U CN201621461144U CN206355642U CN 206355642 U CN206355642 U CN 206355642U CN 201621461144 U CN201621461144 U CN 201621461144U CN 206355642 U CN206355642 U CN 206355642U
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- China
- Prior art keywords
- extraction
- vacuum
- discharge pipe
- tank body
- porous plate
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Abstract
The utility model is related to a kind of novel extraction apparatus, described device includes support frame, extraction tank body, tank deck vacuum meter, extraction porous plate, vacuum connector pipe, point liquid glass observation visor, top discharge pipe, bottom discharge pipe and ball valve, the extraction tank body is arranged on support frame, the top of the extraction tank body is arranged at intervals with tank deck vacuum meter and vacuum connector pipe with being connected in extractor body, the tank deck vacuum meter can monitor the vacuum of extraction tank interior, and the other end of the vacuum connector pipe can be connected setting with vacuum equipment.The present apparatus is simple in construction, design science is reasonable, and extraction is abundant, no dead angle, rapid operation, and solvent volatilization is few, and operating environment will not be polluted.
Description
Technical field
The utility model belongs to extraction equipment technical field, especially a kind of novel extraction apparatus.
Background technology
At present, the extraction extraction element of immunodepressant such as tacrolimus, ascosin, sirolimus etc. is big in extraction
All extract insufficient and current extracting operation all complex, waste time and energy, solvent volatilization is more, easily to operating environment
Pollute, to using bringing inconvenience.
The content of the invention
The purpose of this utility model is to overcome in place of the deficiencies in the prior art that there is provided a kind of novel extraction apparatus, the dress
Put simple in construction, design science rationally, extraction is abundant, no dead angle, rapid operation, solvent volatilization is few, and operating environment will not be made
Into pollution.
The utility model solves its technical problem and takes following technical scheme to realize：
A kind of novel extraction apparatus, described device includes support frame, extraction tank body, tank deck vacuum meter, extraction porous plate, true
Empty connecting line, point liquid glass observation visor, top discharge pipe, bottom discharge pipe and ball valve, the extraction tank body are arranged at support frame
On, the top of the extraction tank body is arranged at intervals with tank deck vacuum meter and vacuum connector pipe with being connected in extractor body, institute
The vacuum of extraction tank interior can be monitored by stating tank deck vacuum meter, and the other end of the vacuum connector pipe can be set with vacuum
The standby setting that is connected；
Coaxial close set extracts porous plate in the extractor body above bottom in the extractor body, and the extraction is more
The conical round tabular of orifice plate, the side of the extraction porous plate matches setting with extracting the shape of inner tank wall, and the extraction is porous
Along the circumferential direction uniform interval is formed with multiple poroid passages set straight down on plate；
The bottom of the extraction tank body is connected setting, the bottom of the top discharge pipe by a ball valve with the top of top discharge pipe
Hold be connected with a point top for liquid glass observation visor setting, the bottom and the top of bottom discharge pipe of this point of liquid glass observation visor
Be connected setting, and a ball valve is also provided with the bottom discharge pipe.
Moreover, the extraction porous plate is arranged at 1/10~1/8 extractor above the bottom in extractor body
Body is highly located.
Moreover, a diameter of 1~2.5mm of the poroid passage.
Advantage of the present utility model and good effect are：
The present apparatus includes support frame, extraction tank body, tank deck vacuum meter, extraction porous plate, vacuum connector pipe, point liquid glass
Observe on visor, top discharge pipe, bottom discharge pipe and ball valve, extraction porous plate along the circumferential direction uniform interval be formed with it is multiple it is vertical to
The poroid passage of lower setting, poroid passage provides the percolation passage of two-phase, makes the dispersed phase of coalescence occur to crush, adds two
Mutually the uniformity of flowing, substantially increases mass transfer effect, and the device is in operation in use, between tank base and top discharge pipe
Ball valve is closed, and the other end of vacuum connector pipe is connected with vacuum equipment, you can carry out vacuum pumping to extraction tank body,
After vacuumizing is finished, the bottom of bottom discharge pipe is placed in comprising immunodepressant tacrolimus, ascosin or sirolimus
Ethyl acetate and aqueous phase mixed solution in, open two ball valves, in the presence of vacuum, extract tank body bottom by point
Liquid glass observation visor, top discharge pipe, the above-mentioned mixed solution of bottom discharge pipe automatic sucking, after absorption is finished, bottom is opened in gap
Ball valve 30s, to admit air into the extractor body, carries out tacrolimus containing immunodepressant, the son in air blending tank body
The ethyl acetate solution mixed with water of capsule mycin, sirolimus, process is extracted and stood after 3 times repeatedly, and suppression is immunized after extraction
Preparation tacrolimus, ascosin, sirolimus component more than 99% are dissolved in ethyl acetate phase, by bottom aqueous phase by dividing
Liquid glass observation visor must contain the ethyl acetate phase of tacrolimus, ascosin, sirolimus after separating, the device component extracting
Fully, no dead angle, rapid operation, because the extractive reaction is carried out all in extractor body, therefore solvent volatilization is few, will not be to behaviour
Polluted as environment, the device have accelerate two-phase laminated flow extraction function, it is adaptable to extract immunodepressant tacrolimus,
The extraction of ascosin, sirolimus, it is easy to use.
Brief description of the drawings
Fig. 1 is structure connection diagram of the present utility model；
Fig. 2 is that enlarged diagram is looked up in the structure connection of extraction porous plate in Fig. 1.
Embodiment：
Below by specific embodiment, the utility model is described in further detail, following examples be it is descriptive, no
It is limited, it is impossible to which protection domain of the present utility model is limited with this.
Structure, annexation and the method not being described in detail in the utility model, can be understood as public affairs in the art
Know general knowledge.
A kind of novel extraction apparatus, as depicted in figs. 1 and 2, it is true that described device includes support frame 4, extraction tank body 3, tank deck
Empty table 1, extraction porous plate 5, vacuum connector pipe 2, point liquid glass observation visor 8, top discharge pipe 7, bottom discharge pipe 9 and ball valve,
The extraction tank body is arranged on support frame, and the top of the extraction tank body is arranged at intervals with tank deck with being connected in extractor body
Vacuum meter and vacuum connector pipe, the tank deck vacuum meter can monitor the vacuum of extraction tank interior, the bonding in vacuum
The other end of pipeline can be connected setting with vacuum equipment, so that the extraction tank interior can be connected with vacuum equipment
Connect setting；
Coaxial close set extracts porous plate in the extractor body above bottom in the extractor body, and the extraction is more
The conical round tabular of orifice plate, the side of the extraction porous plate matches setting with extracting the shape of inner tank wall, and the extraction is porous
Along the circumferential direction uniform interval is formed with multiple poroid passages 11 set straight down on plate；The bottom of the extraction tank body passes through
One ball valve 6 is connected setting with the top of top discharge pipe, and the bottom of the top discharge pipe and point liquid glass observe a top phase for visor
Connection is set, and the bottom of this point of liquid glass observation visor is connected setting with the top of bottom discharge pipe, is also set on the bottom discharge pipe
Put a ball valve 10.
The present apparatus includes support frame, extraction tank body, tank deck vacuum meter, extraction porous plate, vacuum connector pipe, point liquid glass
Observe on visor, top discharge pipe, bottom discharge pipe and ball valve, extraction porous plate along the circumferential direction uniform interval be formed with it is multiple it is vertical to
The poroid passage of lower setting, poroid passage provides the percolation passage of two-phase, makes the dispersed phase of coalescence occur to crush, adds two
Mutually the uniformity of flowing, substantially increases mass transfer effect, and the device is in operation in use, between tank base and top discharge pipe
Ball valve is closed, and the other end of vacuum connector pipe is connected with vacuum equipment, you can carry out vacuum pumping to extraction tank body,
After vacuumizing is finished, the bottom of bottom discharge pipe is placed in comprising immunodepressant tacrolimus, ascosin or sirolimus
Ethyl acetate and aqueous phase mixed solution in, open two ball valves, in the presence of vacuum, extract tank body bottom by point
Liquid glass observation visor, top discharge pipe, the above-mentioned mixed solution of bottom discharge pipe automatic sucking, after absorption is finished, bottom is opened in gap
Ball valve 30s, to admit air into the extractor body, carries out tacrolimus containing immunodepressant, the son in air blending tank body
The ethyl acetate solution mixed with water of capsule mycin, sirolimus, process is extracted and stood after 3 times repeatedly, and suppression is immunized after extraction
Preparation tacrolimus, ascosin, sirolimus component more than 99% are dissolved in ethyl acetate phase, by bottom aqueous phase by dividing
Liquid glass observation visor must contain the ethyl acetate phase of tacrolimus, ascosin, sirolimus after separating, the device component extracting
Fully, no dead angle, rapid operation, because the extractive reaction is carried out all in extractor body, therefore solvent volatilization is few, will not be to behaviour
Polluted as environment, the device have accelerate two-phase laminated flow extraction function, it is adaptable to extract immunodepressant tacrolimus,
The extraction of ascosin, sirolimus, it is easy to use.
In the present embodiment, the extraction porous plate is arranged at 1/10~1/8 above the bottom in extractor body
Extraction tank body highly locate.
In the present embodiment, a diameter of 1~2.5mm of the poroid passage.
Claims (3)
1. a kind of novel extraction apparatus, it is characterised in that：Described device includes support frame, extraction tank body, tank deck vacuum meter, extraction
Porous plate, vacuum connector pipe, point liquid glass observation visor, top discharge pipe, bottom discharge pipe and ball valve, the extraction tank body are set
In on support frame, the top of the extraction tank body is arranged at intervals with tank deck vacuum meter and bonding in vacuum with being connected in extractor body
Pipeline, the tank deck vacuum meter can monitor the vacuum of extraction tank interior, and the other end of the vacuum connector pipe can
Be connected setting with vacuum equipment；
Coaxial close set extracts porous plate, the extraction porous plate in the extractor body above bottom in the extractor body
Conical round tabular, the side of the extraction porous plate matches setting with extracting the shape of inner tank wall, on the extraction porous plate
Along the circumferential direction uniform interval is formed with multiple poroid passages set straight down；
The bottom of the extraction tank body is connected setting by a ball valve with the top of top discharge pipe, the bottom of the top discharge pipe and
The top of point liquid glass observation visor is connected settings, and the bottom that this point of liquid glass observes visor is connected with the top of bottom discharge pipe
It is logical to set, it is also provided with a ball valve on the bottom discharge pipe.
2. novel extraction apparatus according to claim 1, it is characterised in that：The extraction porous plate is arranged at distance extraction
The extraction tank body of 1/10~1/8 above bottom in tank body is highly located.
3. novel extraction apparatus according to claim 1 or 2, it is characterised in that：A diameter of the 1 of the poroid passage~
2.5mm。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621461144.8U CN206355642U (en) | 2016-12-29 | 2016-12-29 | A kind of novel extraction apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621461144.8U CN206355642U (en) | 2016-12-29 | 2016-12-29 | A kind of novel extraction apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206355642U true CN206355642U (en) | 2017-07-28 |
Family
ID=59375945
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621461144.8U Expired - Fee Related CN206355642U (en) | 2016-12-29 | 2016-12-29 | A kind of novel extraction apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206355642U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108245928A (en) * | 2016-12-29 | 2018-07-06 | 天津领世生物科技开发有限公司 | Novel extraction apparatus |
| CN108744589A (en) * | 2018-05-31 | 2018-11-06 | 荆门它山之石电子科技有限公司 | A kind of chemical experiment extraction detection device |
-
2016
- 2016-12-29 CN CN201621461144.8U patent/CN206355642U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108245928A (en) * | 2016-12-29 | 2018-07-06 | 天津领世生物科技开发有限公司 | Novel extraction apparatus |
| CN108744589A (en) * | 2018-05-31 | 2018-11-06 | 荆门它山之石电子科技有限公司 | A kind of chemical experiment extraction detection device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170728 Termination date: 20181229 |