CN206355614U - A kind of thin film evaporation enrichment facility - Google Patents

A kind of thin film evaporation enrichment facility Download PDF

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Publication number
CN206355614U
CN206355614U CN201720001109.6U CN201720001109U CN206355614U CN 206355614 U CN206355614 U CN 206355614U CN 201720001109 U CN201720001109 U CN 201720001109U CN 206355614 U CN206355614 U CN 206355614U
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CN
China
Prior art keywords
liquid
thin film
gas
atomizer
condenser
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720001109.6U
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Chinese (zh)
Inventor
陈红专
刘朝阳
郝福申
尹涛
王峰
苏萌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shijiazhuang Jiuzhou Veterinary Drug Co Ltd
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Shijiazhuang Jiuzhou Veterinary Drug Co Ltd
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Priority to CN201720001109.6U priority Critical patent/CN206355614U/en
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Publication of CN206355614U publication Critical patent/CN206355614U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model is related to a kind of thin film evaporation enrichment facility, it includes being provided with heating wire in material liquid storehouse, preheating device, supersonic atomizer, thin film evaporator, gas-liquid separator, the first condenser, the second condenser, concentrate collecting tank, recovered liquid collecting tank and vacuum generating device, the preheating device;The supersonic atomizer includes atomizer body, is arranged on the intrinsic air blower of atomizer, controller, the liquid level sensor for being arranged on atomizer body bottom portion, when the utility model is used, first open vavuum pump, Chinese medicine material liquid is by preheating, it is atomization subsequently into atomizer body, subsequently into formation gas-liquid film in thin film evaporator, the gas-liquid film enters rotating separation after gas-liquid separator, recovered liquid is formed after gas is condensed, the condensed rear formation concentrate of liquid after separation, thickening efficiency is improved, concentration time is shortened.

Description

A kind of thin film evaporation enrichment facility
Technical field
The utility model is related to Chinese medicine manufacture field, and in particular to a kind of thin film evaporation enrichment facility.
Background technology
The concentration of Chinese medicine extract and evaporation technology are the behaviour being often related in pharmacy, health products and food service industry Make unit.At present, conventional concentrator mainly has nature film forming concentrator and inside and outside circulation concentrator.But, it is natural Film forming concentrate and interior circulation concentration there are problems that thickening efficiency is low, cocnentration factor is small, it is poor for applicability,;Outer circulation Although the first two that concentrator concentrated effect compares improves notable, heat time length, the low skill of thickening efficiency are still had Art problem.Therefore efficient, low energy consumption is developed, the evaporation concentration equipment that equipment is simple, operation is gentleer turns into art technology Personnel are badly in need of the technical problem solved.
The content of the invention
Technical problem to be solved in the utility model is to provide a kind of thin film evaporation enrichment facility, and Chinese medicine material liquid is existed Under vacuum environment, thin film evaporation is carried out after preheated rear first ultrasonic atomizatio, makes the more natural film forming concentration film forming of film forming thinner, more equal It is even, thickening efficiency is improved, concentration time is shortened.
To achieve the above object, the technical solution of the utility model includes:Material liquid storehouse, preheating device, ultrasonic atomization Device, thin film evaporator, gas-liquid separator, the first condenser, the second condenser, concentrate collecting tank, recovered liquid collecting tank and Vacuum generating device, the material liquid storehouse is connected with the bottom of supersonic atomizer by catheter, outside the catheter It is provided with week in preheating device, the preheating device and is provided with heating wire;The supersonic atomizer include atomizer body, The intrinsic air blower of atomizer, controller, the liquid level sensor for being arranged on atomizer body bottom portion are arranged on, the liquid level is passed The signal input part connection of sensor signal output end and controller, the signal output part of the controller and the motor of air blower Signal input part is electrically connected, and orifice is evenly distributed with the top of the atomizer body;
The top of the atomizer body is connected with the bottom of thin film evaporator, and the top of the thin film evaporator is provided with Steam inlet, the bottom of the thin film evaporator is provided with steam (vapor) outlet, the top of the thin film evaporator and gas-liquid separator Top connection, the bottom of the gas-liquid separator connects with the top of the first condenser, the bottom of first condenser and Concentrate collecting tank is connected, and is connected at the top of the gas-liquid separator with the top of the second condenser, the bottom of second condenser Portion is connected with recovered liquid collecting tank, and the vacuum generating device includes vacuum tube and vavuum pump, and one end of the vacuum tube is with returning The connection of liquid collecting tank is received, the other end of the vacuum tube is connected with vavuum pump.
It is used as further improvement of the utility model:Flow control valve is additionally provided with catheter.
It is used as further improvement of the utility model:Thermometer is provided with the steam (vapor) outlet.
It is used as further improvement of the utility model:The model MTK-P260 of the liquid level sensor.
It is used as further improvement of the utility model:The model KCW-6TC of the supersonic atomizer.
The utility model good effect is as follows:
1. Chinese medicine material liquid under vacuum conditions, film steaming is carried out after preheated rear first ultrasonic atomizatio by the utility model Hair, by atomization, considerably increases the disengagement area of decoction, improves evaporation efficiency, and the material being atomized steams into film During hair, film forming more natural film forming concentration film forming is thinner, evenly, improves thickening efficiency, shortens concentration time, solvent evaporation Maximum is measured up to more than 90%, the more conventional concentration time can shorten more than 70%, reduce concentrated cost.
2. the utility model forms recovered liquid after the liquid isolated in gas-liquid separator is condensed, recovered liquid is collected into In collecting tank, realize material recycle, it is to avoid loss of material.
3. the intrinsic Chinese medicine material liquid of the utility model atomizer runs out of or during less than pre-set level, it can pass through Intelligent control, stops air blower air blast, it is seen that air blower stops closing atomizer body after air blast, has so both saved the energy, It is also prevented from device damage, extension device service life.
Brief description of the drawings
Fig. 1 is the utility model structural representation;
In accompanying drawing, 1 material liquid storehouse, 2 preheating devices, 3 catheters, 4 flow control valves, 5 atomizer bodies, 6 ultrasonic fogs Change chip, 8 air blowers, 9 controllers, 10 liquid level sensors, 11 orifices, 12 thin film evaporators, 12-1 steam inlets, 12-2 steamings Vapor outlet, 12-3 thermometers, 13 gas-liquid separators, 14 first condensers, 15 second condensers, 16 concentrate collecting tanks, 17 times Receive liquid collecting tank, 18 vacuum tubes, 19 vavuum pumps.
Embodiment
As shown in figure 1, the utility model includes material liquid storehouse 1, preheating device 2, supersonic atomizer, thin film evaporator 12nd, gas-liquid separator 13, the first condenser 14, the second condenser 15, concentrate collecting tank 16, recovered liquid collecting tank 17 and vacuum Generating means, the memory storage of material liquid storehouse 1 has Chinese medicine material liquid to be concentrated, and the material liquid storehouse 1 is disguised with ultrasonic fog The bottom put is connected by catheter 3, it is preferred that being additionally provided with flow control valve 4 on catheter 3, can control Chinese medicine material The flow of liquid.
The periphery of the catheter 3 is provided with preheating device 2, and the preheating device 2 is coated on the periphery of catheter 3, institute State and heating wire 2-1 is provided with preheating device;The supersonic atomizer includes atomizer body 5, is arranged on atomizer sheet Air blower 8, controller 9 in body 5, the liquid level sensor 10 for being arranged on the bottom of atomizer body 5, the liquid level sensor 10 Signal output part is connected with the signal input part of controller 9, the signal output part of the controller 9 and the motor of air blower 8 Signal input part is electrically connected, and the top of the atomizer body 5 is evenly distributed with orifice 11;Chinese medicine in material liquid storehouse 1 is former Feed liquid is flowed into atomizer body 5 by catheter 3, and the circulation of material liquid can be by pumping in aid conductive, preheating device Heating wire 2-1 heating so that Chinese medicine material liquid flow into atomizer body 5 preheated, after preheating in Medicine material liquid accumulates in the bottom of atomizer body 5, when the Chinese medicine material liquid liquid level of atomizer body 5 is raised to certain altitude or height When the liquid level of the preset height of setting in controller 9, signal is passed to controller 9 by liquid level sensor 10, and controller 9 will be believed Number the motor of air blower 8 is passed to, so as to start air blower rotation, then start atomizer body 5, atomizer body 5 starts The ultrasonic atomization chip 6 of the bottom of atomizer body 5 is arranged on, the Chinese medicine liquid inside atomizer body 5 is atomized, by This, decoction after atomization is under the promotion circulation effect of air blower 8, the mist of decoction after atomization from the top of atomizer body 5 Change hole 11 to enter in thin film evaporator 12, when the Chinese medicine material liquid in atomizer body 5 runs out of or during less than pre-set level, Signal is passed to controller 9 by liquid level sensor 10, and controller 9 passes to signal in the motor of air blower 8, stops air blower 8 Only air blast, is then shut off atomizer body 5, stops atomizing, has so both saved the energy, be also prevented from device damage, extends Service life of equipment, the top of the atomizer body 5 is connected with the bottom of thin film evaporator 12, the liquid level used in the present embodiment The model MTK-P260 of sensor 10, the model KCW-6TC of the supersonic atomizer used in the present embodiment.
Decoction after atomization enters in thin film evaporator 12, is provided with tubulation in thin film evaporator 12, that is, it is branched not Become rusty steel tubule, and the top of the thin film evaporator 12 is provided with steam inlet 12-1, and the bottom of the thin film evaporator 12 is set There is steam (vapor) outlet 12-2, it is preferred that being provided with thermometer 12-3 on the steam (vapor) outlet 12-2, thin film evaporator 12 can be monitored The temperature of interior steam, is easy to heat by steam in regulation and control in time, thin film evaporator 12, decoction is in thin film evaporator 12 Form gas-liquid film in tubulation to rise, the top of the thin film evaporator 12 is connected with the top of gas-liquid separator 13, and film steams Send out and gas-liquid film is formed in the tubulation in device 12, the gas-liquid film enters rotating separation after gas-liquid separator 13, the gas-liquid point Bottom from device 13 is connected with the top of the first condenser 14, and bottom and the concentrate collecting tank 16 of first condenser 14 connect Logical, the top of gas-liquid separator 13 is connected with the top of the second condenser 15, the bottom of second condenser 15 and recovery Liquid collecting tank 17 is connected, and gas-liquid film is formed in the tubulation in thin film evaporator 12, and the gas-liquid film enters gas-liquid separator 13 Rotating separation afterwards, after separation, gas enter the second condenser 15 it is condensed after form recovered liquid, be collected into recovered liquid collecting tank In 17, the liquid after separation forms concentrate after being condensed through the first condenser 14, is collected into concentrate collecting tank 16.
The vacuum generating device includes vacuum tube 18 and vavuum pump 19, and one end and the recovered liquid of the vacuum tube 18 are collected Tank 17 is connected, and the other end of the vacuum tube 18 is connected with vavuum pump 19, is opened after vavuum pump 19, can be filled the utility model Put interior formation vacuum state.
The utility model when in use, first opens vavuum pump 19, by being arranged on the vacuum meter on vacuum tube 18 to vacuum Degree is monitored, and makes below vacuum holding -0.05MPa, opens the steam inlet 12-1 on thin film evaporator 12, leads to steam Enter in thin film evaporator 12, thin film evaporator 12 is heated by steam, at the same time, open preheating device, heating wire 2-1 is added Heat, then slowly opens flow control valve 4, the Chinese medicine material liquid being stored in material liquid storehouse 1 is flowed into catheter 3, Ran Houjin Enter in atomizer body 5, Chinese medicine material liquid is in the process of circulation of catheter 3, and the heat transfer that heating wire 2-1 is produced is former to Chinese medicine Feed liquid, realizes preheating, is subsequently entered by pre-warmed Chinese medicine material liquid in atomizer body 5, when Chinese medicine material liquid liquid level During to default height, signal is passed to controller 9 by liquid level sensor 10, and controller 9 passes to signal the electricity of air blower 8 Machine, is rotated so as to start air blower 8, then starts atomizer body 5, thus, promotion stream of the decoction after atomization in air blower 8 Under logical effect, the decoction after atomization enters in thin film evaporator 12 from the orifice 11 at the top of atomizer body 5, after atomization Decoction enters in thin film evaporator 12, and decoction forms the rising of gas-liquid film in the tubulation in thin film evaporator 12, and the gas-liquid is thin Film enters rotating separation after gas-liquid separator 13, after separation, and gas enters the condensed rear formation recovered liquid of the second condenser 15, quilt It is collected into recovered liquid collecting tank 17, realizes material recycle, it is to avoid loss of material, the liquid after separation is through the first condenser 14 Concentrate is formed after condensation, is collected into concentrate collecting tank 16.
Chinese medicine material liquid under vacuum conditions, thin film evaporation is carried out after preheated rear first ultrasonic atomizatio by the utility model, By atomization, the disengagement area of decoction is considerably increased, evaporation efficiency is improved, the material being atomized enters thin film evaporation When, film forming more natural film forming concentration film forming is thinner, evenly, improves thickening efficiency, shortens concentration time, solvent evaporation amount Maximum is up to more than 90%, and the more conventional concentration time can shorten more than 70%, reduce concentrated cost.
The foregoing description of the disclosed embodiments, enables professional and technical personnel in the field to realize or new using this practicality Type.A variety of modifications to these embodiments will be apparent for those skilled in the art, determine herein The General Principle of justice can in other embodiments be realized in the case where not departing from spirit or scope of the present utility model.Cause This, the utility model is not intended to be limited to the embodiments shown herein, and is to fit to and principles disclosed herein The most wide scope consistent with features of novelty.

Claims (5)

1. a kind of thin film evaporation enrichment facility, it is characterised in that:It includes material liquid storehouse(1), preheating device(2), ultrasonic fog Makeup is put, thin film evaporator(12), gas-liquid separator(13), the first condenser(14), the second condenser(15), concentrate collect Tank(16), recovered liquid collecting tank(17)And vacuum generating device, the material liquid storehouse(1)Lead to the bottom of supersonic atomizer Cross catheter(3)Connection, the catheter(3)Periphery be provided with preheating device(2), electric heating is provided with the preheating device Silk (2-1);The supersonic atomizer includes atomizer body(5), be arranged on atomizer body(5)Interior air blower(8)、 Controller(9), be arranged on atomizer body(5)The liquid level sensor of bottom(10), the liquid level sensor(10)Signal it is defeated Go out end and controller(9)Signal input part connection, the controller(9)Signal output part and air blower(8)Motor Signal input part is electrically connected, the atomizer body(5)Top be evenly distributed with orifice(11);
The atomizer body(5)Top and thin film evaporator(12)Bottom connection, the thin film evaporator(12)It is upper Portion is provided with steam inlet(12-1), the thin film evaporator(12)Bottom be provided with steam (vapor) outlet(12-2), the film Evaporator(12)Top and gas-liquid separator(13)Top connection, the gas-liquid separator(13)Bottom with first condensation Device(14)Top connection, first condenser(14)Bottom and concentrate collecting tank(16)Connection, the gas-liquid separation Device(13)Top and the second condenser(15)Top connection, second condenser(15)Bottom and recovered liquid collecting tank (17)Connection, the vacuum generating device includes vacuum tube(18)And vavuum pump(19), the vacuum tube(18)One end with return Receive liquid collecting tank(17)Connection, the vacuum tube(18)The other end and vavuum pump(19)Connection.
2. a kind of thin film evaporation enrichment facility according to claim 1, it is characterised in that:Catheter(3)On be additionally provided with Flow control valve(4).
3. a kind of thin film evaporation enrichment facility according to claim 1, it is characterised in that:The steam (vapor) outlet(12-2)On It is provided with thermometer(12-3).
4. a kind of thin film evaporation enrichment facility according to claim 1, it is characterised in that:The liquid level sensor(10)'s Model MTK-P260.
5. a kind of thin film evaporation enrichment facility according to claim 1, it is characterised in that:The supersonic atomizer Model KCW-6TC.
CN201720001109.6U 2017-01-03 2017-01-03 A kind of thin film evaporation enrichment facility Expired - Fee Related CN206355614U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720001109.6U CN206355614U (en) 2017-01-03 2017-01-03 A kind of thin film evaporation enrichment facility

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720001109.6U CN206355614U (en) 2017-01-03 2017-01-03 A kind of thin film evaporation enrichment facility

Publications (1)

Publication Number Publication Date
CN206355614U true CN206355614U (en) 2017-07-28

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Application Number Title Priority Date Filing Date
CN201720001109.6U Expired - Fee Related CN206355614U (en) 2017-01-03 2017-01-03 A kind of thin film evaporation enrichment facility

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115382231A (en) * 2021-05-22 2022-11-25 杜马司科学仪器(江苏)有限公司 Liquid film rotation generator and falling film evaporator

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115382231A (en) * 2021-05-22 2022-11-25 杜马司科学仪器(江苏)有限公司 Liquid film rotation generator and falling film evaporator

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170728

CF01 Termination of patent right due to non-payment of annual fee