CN206334670U - One kind hydrogenation workshop hydrogenation process heater - Google Patents

One kind hydrogenation workshop hydrogenation process heater Download PDF

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Publication number
CN206334670U
CN206334670U CN201621470771.8U CN201621470771U CN206334670U CN 206334670 U CN206334670 U CN 206334670U CN 201621470771 U CN201621470771 U CN 201621470771U CN 206334670 U CN206334670 U CN 206334670U
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CN
China
Prior art keywords
hydrogenation
kettle
workshop
liquid
lid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621470771.8U
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Chinese (zh)
Inventor
杨会来
毛杰
孙学喜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wan Hui Pharmaceutical (anhui) Co Ltd
Original Assignee
Wan Hui Pharmaceutical (anhui) Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wan Hui Pharmaceutical (anhui) Co Ltd filed Critical Wan Hui Pharmaceutical (anhui) Co Ltd
Priority to CN201621470771.8U priority Critical patent/CN206334670U/en
Application granted granted Critical
Publication of CN206334670U publication Critical patent/CN206334670U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

Workshop hydrogenation process heater is hydrogenated with the utility model discloses one kind, including kettle and lid, lid is provided with thick liquid-feeding tube, thin liquid-feeding tube, hydrogenation pipe and magnetic agitation axle, unidirectional liquid valve is provided with thick liquid-feeding tube, thin liquid-feeding tube, the end that hydrogenation pipe stretches into kettle is provided with Non-return air valve, magnetic agitation axle is made up of fire-proof motor, reductor, magnetic coupling and agitator, the outside of kettle is respectively provided with heating unit positioned at top, middle part, bottom, and heating unit housing is brought into close contact with kettle outer wall.The utility model is heated to kettle internal upper part, middle part and the liquid of bottom respectively by three heating units, with firing rate it is fast, heat more uniform advantage;Kettle, lid and magnetic agitation axle formation magnetic seal autoclave, can solve the problems, such as traditional shaft sealing leakage, it is adaptable to be hydrogenated with workshop and hydrogenate this inflammable, explosive, the medium that is corrosive chemical reaction.

Description

One kind hydrogenation workshop hydrogenation process heater
Technical field
The utility model is related to pharmaceutical production apparatus field, and in particular to one kind hydrogenation workshop hydrogenation process heating Device.
Background technology
Hydro-reduction reaction is that an extremely wide class chemical reaction type is applied in chemical industry.In our daily lifes Used in chemicals production process in, used medicine and large quantities of agricultural chemicals for developping production during people's treatment disease Production synthesis in hydro-reduction reaction will occur.For example:Medicine " procaine " for anesthesia is by para-nitrotoluene As Material synthesis, wherein an important step, which is exactly the reaction of nitro hydro-reduction, switchs to amido.Catalytic hydrogenation include hydrogenation and Hydrogenolysis.
Tradition hydrogenation workshop hydrogenation process heater, the liquid in kettle exist not in heating process Foot part, one is that it is overall heating or bottom-heated, and firing rate is slow, heats uneven, close liquid level partially liq in kettle Temperature and big close to the temperature difference of reactor bottom liquid, influence product quality;Two be that kettle has shaft sealing leakage, in hydrogen Easily there is reactor explosion accident during change.
Utility model content
The purpose of this utility model is to overcome the above-mentioned problems in the prior art to be hydrogenated with workshop there is provided one kind Hydrogenation process heater.
To realize above-mentioned technical purpose, above-mentioned technique effect is reached, the utility model is to be achieved through the following technical solutions:
One kind hydrogenation workshop hydrogenation process heater, including kettle and lid, the lid add provided with thick Unidirectional liquid valve, the hydrogenation are provided with liquid pipe, thin liquid-feeding tube, hydrogenation pipe and magnetic agitation axle, the thick liquid-feeding tube, thin liquid-feeding tube The end that pipe stretches into kettle is provided with Non-return air valve, and the magnetic agitation axle is by fire-proof motor, reductor, magnetic coupling and stirring Device is constituted, and the outside of the kettle is respectively provided with heating unit, the heating unit housing and kettle positioned at top, middle part, bottom Outer wall is brought into close contact.
Further, the kettle and lid are connected by fixture, form integral type reactor.
Further, the sidepiece of lid is arranged with handling seat.
Further, heating unit enclosure interior is provided with electrothermal tube.
Further, heating unit housing in a ring, electrothermal tube structure in the shape of a spiral.
The beneficial effects of the utility model are:
1st, three heating units are heated to kettle internal upper part, middle part and the liquid of bottom respectively, and this three part is same Shi Jiare mode, with firing rate it is fast, heat more uniform advantage;The heating power of middle part heating unit is more than simultaneously Top, the heating power of lower heating unit so that the heat of kettle center section liquid can be transmitted with lower section upward, be entered One step improves the efficiency of heating surface, ensures product quality.
2nd, kettle, lid and magnetic agitation axle formation magnetic seal autoclave, this autoclave can solve traditional reaction The shaft sealing leakage problem that kettle packing seal, mechanical seal can not overcome, it is adaptable to be hydrogenated with workshop hydrogenation this inflammable, easy Quick-fried, the medium that is corrosive chemical reaction.
Certainly, implement any product of the present utility model to it is not absolutely required to while reaching all the above advantage.
Brief description of the drawings
In order to illustrate more clearly of the technical scheme of the utility model embodiment, make required for being described below to embodiment Accompanying drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the present utility model, For those of ordinary skill in the art, on the premise of not paying creative work, it can also be obtained according to these accompanying drawings Other accompanying drawings.
Fig. 1 is structural representation of the present utility model;
In accompanying drawing, the list of parts representated by each label is as follows:
1- kettlies, 2- lids, the thick liquid-feeding tubes of 3-, the thin liquid-feeding tubes of 4-, 5- hydrogenation pipes, 6- magnetic agitation axles, 7- heating units, 8- fixtures, 9- handlings seat.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the utility model, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made The all other embodiment obtained, belongs to the scope of the utility model protection.
Refer to shown in Fig. 1, the utility model is hydrogenated with workshop hydrogenation process heater, including kettle to be a kind of 1 and lid 2, lid 2 is provided with thick liquid-feeding tube 3, thin liquid-feeding tube 4, hydrogenation pipe 5 and magnetic agitation axle 6, thick liquid-feeding tube 3, thin liquid feeding In pipe 4 be provided with unidirectional liquid valve, hydrogenation pipe 5 stretch into kettle 1 end be provided with Non-return air valve, magnetic agitation axle 6 by fire-proof motor, subtract Fast machine, magnetic coupling and agitator composition, the outside of kettle 1 is respectively provided with heating unit 7 positioned at top, middle part, bottom, heated The housing of unit 7 is brought into close contact with the outer wall of kettle 1.
Wherein, kettle 1 and lid 2 are connected by fixture 8, form integral type reactor.
Wherein, the sidepiece of lid 2 is arranged with handling seat 9.
Wherein, the enclosure interior of heating unit 7 is provided with electrothermal tube, and the housing of heating unit 7 in a ring, tie in the shape of a spiral by electrothermal tube Structure.
One of the present embodiment has particular application as:Three heating units 7 are respectively to the internal upper part of kettle 1, middle part and bottom Liquid is heated, the mode that this three part is heated simultaneously, with firing rate it is fast, heat more uniform advantage;Simultaneously The heating power of middle part heating unit 7 is more than top, the heating power of lower heating unit so that the center section liquid of kettle 1 Heat can be transmitted upward with lower section, further increase the efficiency of heating surface, ensure product quality.Kettle 1, lid 2 and magnetic The formation magnetic seal autoclave of power agitating shaft 6, this autoclave can solve traditional reactor packing seal, mechanical seal can not The shaft sealing leakage problem overcome, it is adaptable to be hydrogenated with this inflammable, explosive, the medium that is corrosive chemistry of workshop hydrogenation anti- Should.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means With reference to specific features, structure, material or the feature that the embodiment or example are described be contained in it is of the present utility model at least one In embodiment or example.In this manual, the schematic representation of above-mentioned term is not necessarily referring to identical embodiment or Example.Moreover, specific features, structure, material or the feature of description can be in any one or more embodiments or examples In combine in an appropriate manner.
The utility model preferred embodiment disclosed above is only intended to help and illustrates the utility model.Preferred embodiment is simultaneously There is no the details that detailed descriptionthe is all, it is only described embodiment that the utility model is not limited yet.Obviously, according to this theory The content of bright book, can make many modifications and variations.This specification is chosen and specifically describes these embodiments, is in order to preferably Principle of the present utility model and practical application are explained, so that skilled artisan can be best understood by and utilize this Utility model.The utility model is only limited by claims and its four corner and equivalent.

Claims (5)

1. one kind hydrogenation workshop hydrogenation process heater, it is characterised in that:Including kettle and lid, on the lid Provided with thick liquid-feeding tube, thin liquid-feeding tube, hydrogenation pipe and magnetic agitation axle, unidirectional liquid valve is provided with the thick liquid-feeding tube, thin liquid-feeding tube, The end that the hydrogenation pipe stretches into kettle is provided with Non-return air valve, and the magnetic agitation axle is by fire-proof motor, reductor, magnetic couple Device and agitator composition, the outside of the kettle is respectively provided with heating unit, the heating unit shell positioned at top, middle part, bottom Body is brought into close contact with kettle outer wall.
2. hydrogenation workshop hydrogenation process heater according to claim 1, it is characterised in that:The kettle and Lid is connected by fixture, forms integral type reactor.
3. hydrogenation workshop hydrogenation process heater according to claim 1, it is characterised in that:The lid Sidepiece is arranged with handling seat.
4. hydrogenation workshop hydrogenation process heater according to claim 1, it is characterised in that:The heating is single First enclosure interior is provided with electrothermal tube.
5. hydrogenation workshop hydrogenation process heater according to claim 4, it is characterised in that:The heating is single First housing in a ring, electrothermal tube structure in the shape of a spiral.
CN201621470771.8U 2016-12-29 2016-12-29 One kind hydrogenation workshop hydrogenation process heater Expired - Fee Related CN206334670U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621470771.8U CN206334670U (en) 2016-12-29 2016-12-29 One kind hydrogenation workshop hydrogenation process heater

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621470771.8U CN206334670U (en) 2016-12-29 2016-12-29 One kind hydrogenation workshop hydrogenation process heater

Publications (1)

Publication Number Publication Date
CN206334670U true CN206334670U (en) 2017-07-18

Family

ID=59303086

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621470771.8U Expired - Fee Related CN206334670U (en) 2016-12-29 2016-12-29 One kind hydrogenation workshop hydrogenation process heater

Country Status (1)

Country Link
CN (1) CN206334670U (en)

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170718

Termination date: 20211229