CN206334641U - A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol - Google Patents

A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol Download PDF

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Publication number
CN206334641U
CN206334641U CN201621380597.8U CN201621380597U CN206334641U CN 206334641 U CN206334641 U CN 206334641U CN 201621380597 U CN201621380597 U CN 201621380597U CN 206334641 U CN206334641 U CN 206334641U
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China
Prior art keywords
feeding device
urea
propane diols
mixing
stirring tank
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CN201621380597.8U
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Chinese (zh)
Inventor
刘力源
梁明国
杨立群
蔺伟飞
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Yangquan Coal Group Qingdao Hengyuan Chemical Co Ltd
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Yangquan Coal Group Qingdao Hengyuan Chemical Co Ltd
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Abstract

Include mixing and stirring tank the utility model discloses a kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol, level gauge, heater, urea feeding device, propane diols feeding device chute, belt conveyor and elevator, level gauge, which is arranged on, is used for the content for measuring mixing and stirring tank propane diols in mixing and stirring tank, mix and heater is set on the outside of tank, urea feeding device and propane diols feeding device are connected with mixing and stirring tank, belt conveyor one end top is arranged on the downside of chute, elevator bottom charging aperture is connected with the belt conveyor other end.Propane diols feeding device includes propane diols storage tank and delivery pump, is connected propane diols storage tank with mixing and stirring tank by delivery pump.Device for mechanical degree is high, reduces labor intensity, reduces labour;Urea is avoided to open the moisture absorption caking for weighing and causing;Operating process does not need special technical staff simply;Many urea feeding device intervals work simultaneously, reduce the fault rate of feeding device.

Description

A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol
Technical field:
The utility model belongs to chemical machinery or equipment manufacturing technology field, and in particular to a kind of urea and propane diols synthesis The feed arrangement of propylene carbonate alcohol.
Background technology:
Propylene carbonate alcohol is a kind of important chemical products, is widely used in Polymeric Industry, gas separating technology and electricity Chemical industry.The alcoholysis of urea of urea and propane diols synthesizing acrylic alcohol, not only raw material urea is cheap and easy to get, and directly profit With the propane diols produced in dimethyl carbonate joint production of propylene glycol device production process, the follow-up sales of propane diols are solved the problems, such as, most For it is important that byproduct of reaction ammonia can be recycled to urea production unit, synthetic method realizes zero-emission, as current tool Competitive propylene carbonate alcohol production method.In industrial processes, it is necessary first to which urea feeding is added in reactor, Then reacted again in the presence of catalyst with propane diols.Conventional urea feeding process is:Urea is transported to device area by storehouse and hung Mouth is filled, material loading platform is then lifted into hoist crane, urea packaging is opened and urea is put into automatic quantitive scale, by urinating after metering The screw(-type) feeder of plain bin bottom gradually delivers to urea dissolution kettle, is blended under conditions of 80 DEG C with propane diols and catalyst Row primary reaction.Pilot process finds that conventional urea feeding process has problems with:(1) urea raw material dosage is big, and work is strong Degree is big, it is necessary to increase external coordination Labor Workers on the basis of original operating personnel;(2) urea is lifted into the laggard weigher of material loading platform, But weigher import is smaller, and amount of urea is larger, feed time can not meet former design production capacity;(3) air humidity is easily made Into urea moisture absorption caking, cause feed bin blowing difficult, and after urea moisture absorption, sack cleaner failure in urea feed bin top rises not To dust removing effects;(4) feeding device only has an electric hoist, and use intensity is very high, if there is failure, easily causes System shutdown.
The content of the invention:
The purpose of this utility model is to overcome the shortcoming of prior art there is provided a kind of alcoholysis of urea synthesizing acrylic The feeding device of alcohol, solves existing feeding device labor intensity greatly, appliance arrangement use intensity is high, weighing takes considerable time, The easy moisture absorption caking of urea.
To achieve these goals, the feeding device for the alcoholysis of urea synthesizing acrylic alcohol that the utility model is related to, Including mixing and stirring tank, level gauge, heater, urea feeding device and propane diols feeding device, level gauge is arranged on It is used for the content for measuring mixing and stirring tank propane diols in mixing and stirring tank, mixes and heater is set on the outside of tank, urine Plain feeding device and propane diols feeding device is connected with mixing and stirring tank.
The urea feeding device that the utility model is related to includes setting on the downside of chute, belt conveyor and elevator, chute On belt conveyor one end top, elevator bottom charging aperture is connected with the belt conveyor other end.Propane diols feeding device bag Propane diols storage tank and delivery pump are included, is connected propane diols storage tank with mixing and stirring tank by delivery pump.
The utility model compared with prior art, with advantages below:(1) device for mechanical degree is high, and reduction work is strong Degree, reduces labour;(2) urea is avoided to open the moisture absorption caking for weighing and causing;(3) operating process does not need special skill simply Art personnel;(4) many urea feeding devices interval or work simultaneously, reduce the fault rate of feeding device.
Brief description of the drawings:
The feeding device structure principle chart for the alcoholysis of urea synthesizing acrylic alcohol that Fig. 1 is related to for utility model.
Embodiment:
Below in conjunction with the accompanying drawings and the utility model is described in further detail by specific embodiment.
Embodiment 1:
The feeding device for the alcoholysis of urea synthesizing acrylic alcohol that the present embodiment is related to, including mixing and stirring tank 1, liquid level Device 2, heater 3, urea feeding device and propane diols feeding device, level gauge 2, which is arranged in mixing and stirring tank, to be used for Measure and heater 3, urea feeding device and third are set on the outside of the content of the propane diols of mixing and stirring tank 1, the tank body of mixing and stirring tank 1 Glycol feeding device is connected with mixing and stirring tank 1.
The urea feeding device that the present embodiment is related to includes chute 4, belt conveyor 5 and elevator 6, and the downside of chute 4 is set Put on one end top of belt conveyor 5, the bottom charging aperture of elevator 6 is connected with the other end of belt conveyor 5.Propane diols feeding is filled Put including propane diols storage tank 8 and delivery pump 7, connected propane diols storage tank 8 with mixing and stirring tank 1 by delivery pump 7.
Many are mixed in the feeding device practical work process for the alcoholysis of urea synthesizing acrylic alcohol that the present embodiment is related to The parallel operation of agitator tank 1 is closed, while setting many urea feeding devices.
The feeding device specific work process for the alcoholysis of urea synthesizing acrylic alcohol that the present embodiment is related to is:By the third two Alcohol is pumped into mixing and stirring tank 1 by delivery pump 7 from propane diols storage tank 8, treats that liquid level reaches process set value, stops adding, with Packed load weighted urea is poured into chute 4 by this simultaneously, and urea is slided along chute 4 falls into the one end of belt conveyor 5, by belt Conveyer 5 is transported to the bottom of elevator 6, and urea is transported up adding in mixing and stirring tank 1 from the top of elevator 6 by elevator 6, During propane diols and urea charging, it is stirred continuously and heats, temperature in mixing and stirring tank 1 is heated to 70-80 DEG C, urine Element dissolving with propane diols constitutive material mixed liquor, then raw material mixed liquor is delivered into the urea dissolution kettle of existing equipment with Catalyst mixing carries out primary reaction.

Claims (3)

1. a kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol, it is characterised in that filled including mixing and stirring tank, liquid level Put, heater, urea feeding device and propane diols feeding device, level gauge is arranged in mixing and stirring tank, mixes Heater is set on the outside of tank, and urea feeding device and propane diols feeding device are connected with mixing and stirring tank.
2. the feeding device of alcoholysis of urea synthesizing acrylic alcohol according to claim 1, it is characterised in that on urea Expect that device includes being arranged on belt conveyor one end top, elevator bottom on the downside of chute, belt conveyor and elevator, chute Charging aperture is connected with the belt conveyor other end.
3. the feeding device of alcoholysis of urea synthesizing acrylic alcohol according to claim 2, it is characterised in that propane diols Feeding device includes propane diols storage tank and delivery pump, is connected propane diols storage tank with mixing and stirring tank by delivery pump.
CN201621380597.8U 2016-12-15 2016-12-15 A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol Active CN206334641U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621380597.8U CN206334641U (en) 2016-12-15 2016-12-15 A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621380597.8U CN206334641U (en) 2016-12-15 2016-12-15 A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol

Publications (1)

Publication Number Publication Date
CN206334641U true CN206334641U (en) 2017-07-18

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Family Applications (1)

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CN201621380597.8U Active CN206334641U (en) 2016-12-15 2016-12-15 A kind of feeding device of alcoholysis of urea synthesizing acrylic alcohol

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111925351A (en) * 2020-08-28 2020-11-13 华东理工大学 Method for continuously dissolving urea and propylene glycol (or ethylene glycol)
CN113996231A (en) * 2021-12-31 2022-02-01 山东海科新源材料科技股份有限公司 Novel batching kettle for preparing urea fatty alcohol mixed liquid and using method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111925351A (en) * 2020-08-28 2020-11-13 华东理工大学 Method for continuously dissolving urea and propylene glycol (or ethylene glycol)
CN113996231A (en) * 2021-12-31 2022-02-01 山东海科新源材料科技股份有限公司 Novel batching kettle for preparing urea fatty alcohol mixed liquid and using method thereof

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