CN206315796U - A kind of sub-cooled formula pharmacy reaction kettle - Google Patents
A kind of sub-cooled formula pharmacy reaction kettle Download PDFInfo
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- CN206315796U CN206315796U CN201621396178.3U CN201621396178U CN206315796U CN 206315796 U CN206315796 U CN 206315796U CN 201621396178 U CN201621396178 U CN 201621396178U CN 206315796 U CN206315796 U CN 206315796U
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Abstract
The utility model is related to a kind of pharmacy special reactor, including base plate, the upper surface of the base plate is symmetrically installed with two pieces of supporting plates, a support ring is welded with every piece of supporting plate, a rotary shaft is mounted on by bearing in the middle part of each support ring, and it is welded with reaction sphere between two rotary shafts in two pieces of supporting plates, the medicine intermediate of question response is laid in reaction sphere, rotary electric machine is provided with by shaft coupling in the rotary shaft on the left of reaction sphere, rotary electric machine is by motor cabinet in L-type support, L-type support is welded in the supporting plate on the left of reaction sphere；The upper and lower ends of the reaction sphere inwall are symmetrically installed with four interior ice chests；The left and right sides of the reaction sphere outer wall is symmetrically installed with two outer ice chests.The utility model can realize the rotation fast reaction of medicine intermediate and efficiently cool down heat absorption function have the advantages that the reaction time is short, reaction is complete, good reaction effect, high working efficiency and endothermic effect are good.
Description
Technical field
The utility model is related to medicine intermediate processing technique field, specifically a kind of sub-cooled formula pharmacy reaction
Kettle.
Background technology
China about needs that the raw material supporting with chemical industry and intermediate are a variety of every year, and demand is up to more than ten thousand tons；In so-called medicine
Mesosome, is actually some industrial chemicals or chemical products that some are used in medicine synthesis process.This chemical products,
The production licence of medicine is not needed, can be produced in common chemical plant, as long as reaching the rank of some, you can for medicine
Synthesis.Medicine intermediate industry, by development in recent years, has become the output value billions of by a branch in chemical industry
The emerging industry of member, it competes also more white-hot therewith.In the industry early stage of development, because the smaller, return rate of investment is high, in medicine
Mesosome enterprise emerges like the mushrooms after rain.
The pharmaceutical intermediate overwhelming majority of Western medicine is obtained by organic synthesis, and many organic syntheses are substantially in reaction
Completed on kettle, but existing reactor substantially placed and reacted under inactive state, the reactor reaction time under inactive state is long,
React incomplete due to stirring insufficient be easily caused, reaction effect is poor, and operating efficiency is low；And in reactor course of reaction
Pharmaceutical intermediate can release amount of heat, and the phenomenon that the rotten influence of medicine intermediate is used occurs if temperature is too high.
Utility model content
In order to solve the above problems, the utility model provides a kind of sub-cooled formula pharmacy reaction kettle, can solve existing
Have medicine intermediate reaction time length under pharmaceutical intermediate reactor inactive state, reaction not exclusively, reaction effect it is poor, work imitate
Influence that rate is low and going bad occurs in reaction temperature height such as uses at the problem, it is possible to achieve the rotation fast reaction of medicine intermediate and height
Effect cooling heat absorption function, with the reaction time is short, reaction completely, good reaction effect, high working efficiency and endothermic effect it is good etc. excellent
Point.
To achieve these goals, the utility model is realized using following technical scheme：A kind of sub-cooled formula pharmacy
Reactor, including base plate, the upper surface of the base plate, which is symmetrically installed with two pieces of supporting plates, every piece of supporting plate, is welded with one
In the middle part of support ring, each support ring by bearing be mounted on two rotary shafts in a rotary shaft, and two pieces of supporting plates it
Between be welded with the medicine intermediate that question response is laid in reaction sphere, reaction sphere, pass through in the rotary shaft on the left of reaction sphere
Shaft coupling is provided with rotary electric machine, and rotary electric machine is by motor cabinet in L-type support, and L-type support is welded on positioned at reaction sphere
In the supporting plate in left side, L-type support plays a part of fixed support rotating motor, by rotary electric machine drive two rotary shafts it
Rotated in two support rings, two rotary shafts drive reaction sphere uniform rotation, pass through rotarily driving in the middle of medicine for reaction sphere
Body is uniformly overturn so that can fully be contacted between each composition of medicine intermediate, and reaction is cmpletely；Two above and below the reaction sphere
End, which is symmetrically installed with two discharge nozzles, each discharge nozzle, is mounted on an outlet valve, and outlet valve can control discharge nozzle
Open and close status, during the discharge nozzle being located at after reaction sphere, which is rotated, to be stopped below reaction sphere is medical after being finished as reaction
The flow pass of mesosome；The reaction sphere left and right sides is symmetrically arranged with four feed cavities, each feed cavity and is mounted on one
Individual inlet valve, opening and the closing of feed cavity are controlled by inlet valve, and reaction sphere rotates two above reaction sphere of anteposition and entered
Expect flow channel of the chamber as medicine intermediate；Collecting box is laid in the middle part of the base plate upper surface, the doctor after finishing is reacted
Medicine intermediate, which is flowed into collecting box, to be collected, and is evenly arranged with from top to bottom in the reaction sphere on dividing plate, dividing plate uniform
It is provided with to wear be used on material hole, dividing plate and lays the medicine intermediate fallen into, physical efficiency is led in the middle of reaction sphere rotation process traditional Chinese medicine
Cross to wear and flowed into above and below material hole, upset is uniform, and reaction effect is good.
The upper and lower ends of the reaction sphere inwall are symmetrically installed with four interior ice chests, positioned at the interior ice chest in reaction sphere upper end two
Between and be connected by conduit between the interior ice chest in reaction sphere lower end two, and it is each in be respectively connected with one one on ice chest
Number feed tube, a feed tube as coolant in interior ice chest entrance flow pass；The left and right sides of the reaction sphere outer wall
It is symmetrically installed with two outer ice chests, and each outer ice chest and is symmetrically installed with two No. two feed tubes, No. two feed tube conducts
Coolant can inhale during the course of the reaction in four interior ice chests in the entrance flow pass of coolant, the utility model in outer ice chest
The heat that reaction sphere upper and lower ends medicine intermediate is produced is received, and coolant can absorb during the course of the reaction in two outer ice chests
The heat that reaction sphere left and right ends intermediate is produced, so as to reach the effect of efficiently cooling heat absorption.
As a kind of optimal technical scheme of the present utility model, the lower end of the reaction sphere is symmetrically arranged with two and blocked
Two blocking mechanisms are respectively symmetrically installed on bar, the inwall of two pieces of supporting plates, when needing reaction sphere to stop, two resistances
Retaining device start-up operation stretches out stop two and blocks bar, can make it that reaction sphere is quickly stopped.
As a kind of optimal technical scheme of the present utility model, the blocking mechanism includes being arranged in correspondence supporting plate
It is fixed in the middle part of hydraulic cylinder, hydraulic cylinder in fixed board, fixed board plays a part of fixed supporting cylinder, fixed board is welded on correspondence branch
On the wall of fagging side, the top of hydraulic cylinder is provided with fixed block, fixed block by flange is provided with stopper, passes through hydraulic cylinder band
Dynamic fixed block motion, fixed block drives stopper stretching to stop and blocks bar, can make it that reaction sphere is quickly stopped.
As a kind of optimal technical scheme of the present utility model, frozen water or suction are contained with the interior ice chest, outer ice chest
Heat chemistry reagent, the utility model is used as coolant by the use of frozen water or endothermic chemical reagent.
During utility model works, inlet valve is in open mode in two feed cavities first above reaction sphere, then
The medicine intermediate of question response is put into from two feed cavities above reaction sphere, medicine intermediate drop into reaction sphere every
On plate, now rotary electric machine is started working, and rotary electric machine drives the rotation in two support rings of two rotary shafts, two rotations
Axle drive reaction sphere uniform rotation, by reaction sphere rotarily drive medicine intermediate dividing plate wear material hole in up and down flowing out stream
Enter and uniformly overturn so that can fully be contacted between each composition of medicine intermediate, cmpletely, medicine intermediate is anti-for reaction
Rotary electric machine is stopped after should fully reacting, and two blocking mechanisms are started working, and fixed block is driven by hydraulic cylinder
Motion, fixed block drives stopper stretching to stop and blocks bar, can make it that reaction sphere is quickly stopped, and is now placed under reaction sphere
The discharge nozzle top discharge valve of side is in open mode, and the medicine intermediate after reaction is finished is flowed into collecting box by discharge nozzle
In be collected, and coolant during the course of the reaction can be with absorbing reaction ball upper and lower ends in four interior ice chests in the utility model
The heat that medicine intermediate is produced, and coolant during the course of the reaction can be with absorbing reaction ball left and right ends in two outer ice chests
The heat that mesosome is produced, so as to reach the effect of efficiently cooling heat absorption, realizes rotation fast reaction and the height of medicine intermediate
Effect cooling heat absorption function.
The beneficial effects of the utility model are：Compared with prior art, the utility model can solve existing the utility model
Medicine intermediate reaction time length under pharmaceutical intermediate reactor inactive state, reaction are not exclusively, reaction effect is poor, operating efficiency
There is rotten influence and the problem such as uses in low and reaction temperature height, it is possible to achieve the rotation fast reaction of medicine intermediate and efficient
Cooling heat absorption function, has the advantages that the reaction time is short, reaction is complete, good reaction effect, high working efficiency and endothermic effect are good.
Brief description of the drawings
The utility model is further illustrated with reference to the accompanying drawings and examples.
Fig. 1 is structural representation of the present utility model.
Embodiment
In order that technological means, creation characteristic, reached purpose and effect that the utility model is realized are easy to understand, under
Face combines and is specifically illustrating, and the utility model is expanded on further.
As shown in figure 1, a kind of sub-cooled formula pharmacy reaction kettle, including base plate 1, the upper surface of the base plate 1 is symmetrically pacified
Equipped with two pieces of supporting plates 2, a support ring 3 is welded with every piece of supporting plate 2, each middle part of support ring 3 is pacified by bearing
Laid equipped with being welded between two rotary shafts 4 in a rotary shaft 4, and two pieces of supporting plates 2 in reaction sphere 5, reaction sphere 5
The medicine intermediate of question response, rotary electric machine 6 is provided with the rotary shaft 4 in the left side of reaction sphere 5 by shaft coupling, rotates electricity
Machine 6 is by motor cabinet in L-type support 7, and L-type support 7 is welded in the supporting plate 2 in the left side of reaction sphere 5, L-type support 7
Play a part of fixed support rotating motor 6, pass through turning in two support rings 3 for two rotary shafts 4 of drive of rotary electric machine 6
Dynamic, two rotary shafts 4 drive the uniform rotation of reaction sphere 5, are uniformly overturn, made by the medicine intermediate that rotarily drives of reaction sphere 5
Can fully contact between each composition of medicine intermediate, reaction is cmpletely；The upper and lower ends of reaction sphere 5 are symmetrically installed with
It is mounted on an outlet valve 9 on two discharge nozzles 8, each discharge nozzle 8, what outlet valve 9 can control discharge nozzle 8 beats Push And Release
Closed state, is located at medicine intermediate after the discharge nozzle 8 of the lower section of reaction sphere 5 is finished as reaction after reaction sphere 5, which is rotated, to be stopped
Flow pass；The left and right sides of reaction sphere 5 is symmetrically arranged with four feed cavities 10, each feed cavity 10 and is mounted on one
Individual inlet valve 11, opening and the closing of feed cavity 10 are controlled by inlet valve 11, and reaction sphere 5 rotates anteposition in the top of reaction sphere 5
Two feed cavities 10 as medicine intermediate flow channel；Collecting box 12 is laid in the middle part of the upper surface of base plate 1, is reacted
Medicine intermediate after finishing is flowed into collecting box 12 and is collected, and is evenly arranged with from top to bottom in the reaction sphere 5
It is evenly arranged with dividing plate 15, dividing plate 15 and wears material hole, be used on dividing plate 15 lay the medicine intermediate fallen into, in 5 turns of reaction sphere
Medicine intermediate flowed into above and below material hole by that can be worn during dynamic, and upset is uniform, and reaction effect is good.
The upper and lower ends of the inwall of reaction sphere 5 are symmetrically installed with four interior ice chests 16, in 5 upper end of reaction sphere two
It is connected between ice chest 16 and between the interior ice chest 16 in 5 lower end of reaction sphere two by conduit 17, and on each interior ice chest 16
Be respectively connected with a feed tube 18, a feed tube 18 as coolant in interior ice chest 16 entrance flow pass；It is described
The left and right sides of the outer wall of reaction sphere 5 is symmetrically installed with two outer ice chests 19, and each outer ice chest 19 and is symmetrically installed with two
No. two feed tubes 20, No. two feed tubes 20 as coolant in outer ice chest 19 entrance flow pass, four in the utility model
The heat that coolant can be produced with the upper and lower ends medicine intermediate of absorbing reaction ball 5 during the course of the reaction in interior ice chest 16, and two
The heat that coolant can be produced with the left and right ends intermediate of absorbing reaction ball 5 during the course of the reaction in individual outer ice chest 19, so as to reach
To the effect of efficient cooling heat absorption.
The lower end of the reaction sphere 5 is symmetrically arranged with two and blocks right respectively on bar 13, the inwall of two pieces of supporting plates 2
Title is provided with two blocking mechanisms 14, when needing reaction sphere 5 to stop, and two blocking mechanisms 14, which start working to stretch out, stops two
Bar 13 is blocked, can make it that reaction sphere 5 is quickly stopped.
The blocking mechanism 14 includes the hydraulic cylinder 141 being arranged in correspondence supporting plate 2, and the middle part of hydraulic cylinder 141 is fixed
In fixed board 142, fixed board 142 plays a part of fixed supporting cylinder 141, and fixed board 142 is welded on the correspondence side wall of supporting plate 2
On, the top of hydraulic cylinder 141 is provided with fixed block 143, fixed block 143 by flange is provided with stopper 144, passes through hydraulic pressure
Cylinder 141 drives fixed block 143 to move, and fixed block 143 drives the stretching of stopper 144 to stop and blocks bar 13, can cause reaction sphere 5
Quickly stop.
Frozen water or endothermic chemical reagent are contained with the interior ice chest 16, outer ice chest 19, the utility model utilizes frozen water
Or endothermic chemical reagent is used as coolant.
During utility model works, inlet valve 11 is in open mode in two feed cavities 10 of the top of reaction sphere 5 first,
Then the medicine intermediate of question response is put into from two feed cavities 10 of the top of reaction sphere 5, medicine intermediate is dropped into instead
Answer on the dividing plate 15 of ball 5, now rotary electric machine 6 is started working, rotary electric machine 6 drive two rotary shafts 4 in two support rings 3
Upper to rotate, two rotary shafts 4 drive the uniform rotation of reaction sphere 5, and medicine intermediate is rotarily driven in dividing plate 15 by reaction sphere 5
Wear in material hole and flow into and uniformly overturn up and down so that can fully be contacted between each composition of medicine intermediate, reaction
Cmpletely, rotary electric machine 6 is stopped after medicine intermediate reaction fully reaction, and two blocking mechanisms 14 start work
Make, drive fixed block 143 to move by hydraulic cylinder 141, fixed block 143 drives the stretching of stopper 144 to stop and blocks bar 13, energy
So that reaction sphere 5 is quickly stopped, the top discharge valve 9 of discharge nozzle 8 for being now placed in the lower section of reaction sphere 5 is in open mode, reaction
Medicine intermediate after finishing is flowed into collecting box 12 by discharge nozzle 8 to be collected, and in the utility model in four
The heat that coolant can be produced with the upper and lower ends medicine intermediate of absorbing reaction ball 5 during the course of the reaction in ice chest 16, and two
The heat that coolant can be produced with the left and right ends intermediate of absorbing reaction ball 5 during the course of the reaction in outer ice chest 19, so as to reach
Efficiently the effect of cooling heat absorption, realizes the rotation fast reaction of medicine intermediate and efficient cooling heat absorption function, solves existing
Have medicine intermediate reaction time length under pharmaceutical intermediate reactor inactive state, reaction not exclusively, reaction effect it is poor, work imitate
Influence that rate is low and going bad occurs in reaction temperature height such as uses at the problem, reaches purpose.
General principle of the present utility model, principal character and advantage has been shown and described above.The technical staff of the industry
It should be appreciated that the utility model is not restricted to the described embodiments, the simply explanation of the description in above-described embodiment and specification
Principle of the present utility model, on the premise of the utility model spirit and scope are not departed from, the utility model also has various changes
Change and improve, these changes and improvements are both fallen within the range of claimed the utility model.Model is claimed in the utility model
Enclose by appending claims and its equivalent thereof.
Claims (4)
1. a kind of sub-cooled formula pharmacy reaction kettle, it is characterised in that：Including base plate (1), the upper surface of the base plate (1) is symmetrical
It is provided with two pieces of supporting plates (2), every piece of supporting plate (2) and is welded with a support ring (3), it is logical in the middle part of each support ring (3)
Cross between two rotary shafts (4) that bearing is mounted on a rotary shaft (4), and two pieces of supporting plates (2) and be welded with reaction sphere
(5) rotary electric machine (6), is provided with by shaft coupling in the rotary shaft (4) on the left of reaction sphere (5), rotary electric machine (6) passes through
Motor cabinet is in L-type support (7), and L-type support (7) is welded in the supporting plate (2) on the left of reaction sphere (5)；It is described anti-
Answer ball (5) upper and lower ends to be symmetrically installed with two discharge nozzles (8), each discharge nozzle (8) and be mounted on an outlet valve (9)；
Reaction sphere (5) left and right sides, which is symmetrically arranged with, to be mounted on one on four feed cavities (10), each feed cavity (10) and enters
Expect valve (11)；Collecting box (12) is laid in the middle part of base plate (1) upper surface；Uniformly set from top to bottom in the reaction sphere (5)
It is equipped with dividing plate (15), dividing plate (15) to be evenly arranged with and wears material hole；
The upper and lower ends of reaction sphere (5) inwall are symmetrically installed with four interior ice chests (16), positioned at reaction sphere (5) upper end two
It is connected between interior ice chest (16) and between the interior ice chest (16) in reaction sphere (5) lower end two by conduit (17), and each
A feed tube (18) is respectively connected with interior ice chest (16)；The left and right sides of reaction sphere (5) outer wall is symmetrically installed with
Two No. two feed tubes (20) are symmetrically installed with two outer ice chests (19), and each outer ice chest (19).
2. a kind of sub-cooled formula pharmacy reaction kettle according to claim 1, it is characterised in that：The reaction sphere (5)
Lower end, which is symmetrically arranged with two, to block and be respectively symmetrically provided with two stops on bar (13), the inwall of two pieces of supporting plates (2)
Mechanism (14).
3. a kind of sub-cooled formula pharmacy reaction kettle according to claim 2, it is characterised in that：The blocking mechanism (14)
Including the hydraulic cylinder (141) in correspondence supporting plate (2), it is fixed in the middle part of hydraulic cylinder (141) in fixed board (142), it is fixed
Plate (142) is welded on correspondence supporting plate (2) side wall, and the top of hydraulic cylinder (141) is provided with fixed block (143) by flange,
Stopper (144) is provided with fixed block (143).
4. a kind of sub-cooled formula pharmacy reaction kettle according to claim 1, it is characterised in that：The interior ice chest (16),
Frozen water or endothermic chemical reagent are contained with outer ice chest (19).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621396178.3U CN206315796U (en) | 2016-12-19 | 2016-12-19 | A kind of sub-cooled formula pharmacy reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621396178.3U CN206315796U (en) | 2016-12-19 | 2016-12-19 | A kind of sub-cooled formula pharmacy reaction kettle |
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| Publication Number | Publication Date |
|---|---|
| CN206315796U true CN206315796U (en) | 2017-07-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621396178.3U Active CN206315796U (en) | 2016-12-19 | 2016-12-19 | A kind of sub-cooled formula pharmacy reaction kettle |
Country Status (1)
| Country | Link |
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| CN (1) | CN206315796U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114797741A (en) * | 2022-03-06 | 2022-07-29 | 谢磊磊 | Cryogenic cooling pharmaceutical reaction kettle |
-
2016
- 2016-12-19 CN CN201621396178.3U patent/CN206315796U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114797741A (en) * | 2022-03-06 | 2022-07-29 | 谢磊磊 | Cryogenic cooling pharmaceutical reaction kettle |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180409 Address after: 200120 201 rooms, No. 6999, Chuansha Road, Pudong New Area, Shanghai Patentee after: Shanghai Chelvon Biotechnology Co., Ltd. Address before: 246001 circular economy industrial park, Daguan Economic Development Zone, Anqing City, Anqing, Anhui Patentee before: ANHUI HAIKANG PHARMACEUTICAL CO., LTD. |