CN206298345U - Alembic overflow mechanism - Google Patents
Alembic overflow mechanism Download PDFInfo
- Publication number
- CN206298345U CN206298345U CN201621391822.8U CN201621391822U CN206298345U CN 206298345 U CN206298345 U CN 206298345U CN 201621391822 U CN201621391822 U CN 201621391822U CN 206298345 U CN206298345 U CN 206298345U
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- alembic
- crucible
- barrel
- cover
- heating furnace
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Abstract
The utility model discloses a kind of alembic overflow mechanism, belong to distillation equipment field, including heating furnace and alembic, alembic includes tank body and the cover covered on the upside of tank body, heating furnace includes furnace wall, insulating brick and heating furnace silk, the cover is located at outside heating furnace, cover connects vacuum lead, material storing box is set in tank body, crucible on the upside of material storing box and the barrel in crucible, crucible top is open, barrel top sets nozzle, the nozzle on barrel top is protruded upward outside crucible, in the side wall of barrel, discharging opening is set, via is set on the side wall of crucible, material storing box sets charging aperture, height of the height of via higher than discharging opening, a piece two-port through the overflow pipe of via connects discharging opening respectively, charging aperture, the utility model is a kind of alembic overflow mechanism that byproduct can be drained into material storing box automatically.
Description
Technical field
The utility model belongs to distillation equipment field, more particularly to a kind of alembic overflow mechanism.
Background technology
At present, the distillation equipment for being used in metallurgical distillation technique mainly has crucible type retort, flame-insulating type retort and tower
Disc type retort, the byproduct case of crucible type retort is often arranged on outside alembic, and the byproduct in barrel is needed by pump
Discharge.
Utility model content
The purpose of this utility model is to provide a kind of alembic overflow mechanism that byproduct can be drained into material storing box automatically.
To achieve the above object, the utility model is adopted the following technical scheme that：Alembic overflow mechanism, including heating furnace and
Alembic, alembic includes tank body and the cover covered on the upside of tank body, and heating furnace includes furnace wall, insulating brick and heating furnace silk, institute
Furnace wall, insulating brick, heating furnace silk and tank body are stated to set gradually from outside to inside, the cover is located at outside heating furnace, cover connection
Vacuum lead, sets material storing box, the crucible on the upside of material storing box and the barrel in crucible in tank body, crucible top opens
Mouthful, barrel top sets nozzle, and the nozzle on barrel top is protruded upward outside crucible, and discharging opening is set in the upper portion side wall of barrel,
Via is set on the side wall of crucible, and material storing box sets charging aperture, and the height of via is higher than the height of discharging opening, and one passes through via
The two-port of overflow pipe connect discharging opening, charging aperture respectively.
The longitudinal section of the cover takes the shape of the letter U shape, and vacuum lead is connected to the top of cover.
The tank body and cover are flange connection.
The tube wall of overflow pipe is provided with material charging port, and cover plate is provided with material charging port.
The discharging opening is on the lower sides of barrel.
Alembic overflow mechanism described in the utility model, during work, is equipped with material in barrel, heated when to alembic
When, the material in barrel is in molten state, is layered because density is different, and lower floor is product, and upper strata is byproduct, by siphon drainage
Principle so that upper strata byproduct is by overflow pipe overflow to material storing box.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Fig. 2 is the structural representation of overflow pipe；
In figure：Furnace wall 1, insulating brick 2, heating furnace silk 3, tank body 4, cover 5, barrel 6, crucible 7, cover plate 8, overflow pipe 9, storage
Hopper 10, vacuum lead 11, byproduct 12, discharging opening 13, product 14.
Specific embodiment
Alembic overflow mechanism as shown in Fig. 1 and Fig. 2, including heating furnace and alembic.
Alembic includes the tank body 4 of top end opening and covers the cover 5 in the upside of tank body 4, and the cover 5 arches upward upwards, tank
The longitudinal section of lid 5 takes the shape of the letter U shape, and downwards, the tank body 4 and cover 5 are flange connection to the U-shaped mouth of the longitudinal section of cover 5, cover 5
Bottom sets upper flange, and the top of tank body 4 sets lower flange, together with upper flange is bolted with lower flange, realizes tank
The docking up and down of lid 5 and tank body 4, the connection vacuum lead 11 of cover 5, vacuum lead 11 connects the upper portion side wall in cover 5
On, the inner chamber of cover 5 and the inner space of tank body 4, vacuum lead 11 are used to extract the gas in alembic, make in alembic
Vacuum is formed, material and air oxidation reaction is prevented.
Heating furnace includes furnace wall 1, insulating brick 2 and heating furnace silk 3, the furnace wall 1, insulating brick 2, heating furnace silk 3 and tank body 4
To set gradually from outside to inside, heating furnace silk 3 is electrical heating wire, and heating furnace silk 3 is coated on the periphery of tank body 4 and for being distillation
Tank is heated, to provide temperature needed for material distillation in barrel 6；Insulating brick 2 is coated on the periphery of heating furnace silk 3 and for being incubated,
The cover 5 is located at outside heating furnace, and cover 5 is located at the upside of heating furnace；Furnace wall 1 is coated on outside insulating brick 3.
Material storing box 10, crucible 7 and the barrel 6 in crucible 7 located at the upside of material storing box 10 are set in tank body 4, crucible 7 is pushed up
End is open, and the top of barrel 6 sets nozzle, and the nozzle on the top of barrel 6 is protruded upward outside crucible 7, is set in the lower sides of barrel 6
(the less lower floor's product 14 of output, is to occupy a large amount of skies in remaining space of barrel 6 to discharging opening 13 in the bottom space of barrel 6
Between upper strata byproduct 12, the position of discharging opening 13 is corresponding to upper strata byproduct 12), via, storing are set on the side wall of crucible 7
Case 10 sets charging aperture, the height of the height higher than discharging opening 13 of via, a two-port difference through the overflow pipe 9 of via
Connection discharging opening 13, charging aperture.
The tube wall of overflow pipe 9 is provided with material charging port, and being provided with material charging port can close the cover plate of material charging port
8.It is in inverted U-shape that overflow pipe 9 is overall, and at via and positioned at the peak of overflow pipe 9, material passes through material charging port
Material charging port is packed into overflow pipe 9, and material bonnet upper cover plate 8 is filled up in overflow pipe 9, material and overflow pipe 9 in barrel 6
Interior material is heated and becomes molten condition simultaneously, and overflow pipe 9 is connected and by siphon principle by upper strata pair in barrel 6 with barrel 6
Product is suctioned out to material storing box 10.
Alembic overflow mechanism described in the utility model, during work, material, material is respectively arranged with barrel 6 and overflow pipe 9
It is HfCl4And Mg, when heating furnace silk is heated to alembic 3, the material in barrel 6 and overflow pipe 9 is in molten state, barrel 6
Middle product is layered because density is different, and lower floor is product 14, and upper strata is byproduct 12, and byproduct 12 is more and occupies big in barrel
Segment space, product 14 is less only to occupy barrel bottom space, and overflow pipe 9 is by siphon principle so that upper strata byproduct passes through
In the overflow of overflow pipe 9 to material storing box 10, this alembic overflow mechanism is used to produce hydrofluoric acid (Hf) and magnesium chloride (MgCl2), change
Learning reaction equation is：
Wherein hydrofluoric acid (Hf) is major product, magnesium chloride (MgCl2) it is byproduct.
Claims (5)
1. alembic overflow mechanism, it is characterised in that：Including heating furnace and alembic, alembic includes tank body (4) and covers in tank
Cover (5) on the upside of body (4), heating furnace includes furnace wall (1), insulating brick (2) and heating furnace silk (3), the furnace wall (1), insulation
, to set gradually from outside to inside, outside heating furnace, cover is connected the cover (5) for brick (2), heating furnace silk (3) and tank body (4)
Material storing box (10), the crucible (7) on the upside of material storing box (10) are set in vacuum lead (11), tank body (4) and located at crucible (7)
Interior barrel (6), crucible (7) top is open, and barrel (6) top sets nozzle, and the nozzle on barrel (6) top protrudes upward crucible
(7) outward, discharging opening (13) is set on the side wall of barrel (6), via is set on the side wall of crucible (7), material storing box (10) is set
Charging aperture, the height of the height higher than discharging opening (13) of via a, two-port through the overflow pipe (9) of via is connected respectively
Discharging opening (13), charging aperture.
2. alembic overflow mechanism as claimed in claim 1, it is characterised in that：The longitudinal section of the cover (5) takes the shape of the letter U shape,
Vacuum lead (11) is connected to the top of cover (5).
3. alembic overflow mechanism as claimed in claim 1, it is characterised in that：The tank body (4) and cover (5) are flange company
Connect.
4. alembic overflow mechanism as claimed in claim 1, it is characterised in that：The tube wall of overflow pipe (9) is provided with material and fills out
Mouth is filled, cover plate (8) is provided with material charging port.
5. alembic overflow mechanism as claimed in claim 1, it is characterised in that：The discharging opening (13) is located at barrel (6)
On lower sides.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621391822.8U CN206298345U (en) | 2016-12-19 | 2016-12-19 | Alembic overflow mechanism |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621391822.8U CN206298345U (en) | 2016-12-19 | 2016-12-19 | Alembic overflow mechanism |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206298345U true CN206298345U (en) | 2017-07-04 |
Family
ID=59214383
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621391822.8U Active CN206298345U (en) | 2016-12-19 | 2016-12-19 | Alembic overflow mechanism |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206298345U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111004927A (en) * | 2019-12-31 | 2020-04-14 | 河钢股份有限公司承德分公司 | Reduction distillation furnace and device and method comprising same |
-
2016
- 2016-12-19 CN CN201621391822.8U patent/CN206298345U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111004927A (en) * | 2019-12-31 | 2020-04-14 | 河钢股份有限公司承德分公司 | Reduction distillation furnace and device and method comprising same |
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