CN206285867U - chemical reaction negative pressure feeding structure - Google Patents

chemical reaction negative pressure feeding structure Download PDF

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Publication number
CN206285867U
CN206285867U CN201621317568.7U CN201621317568U CN206285867U CN 206285867 U CN206285867 U CN 206285867U CN 201621317568 U CN201621317568 U CN 201621317568U CN 206285867 U CN206285867 U CN 206285867U
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CN
China
Prior art keywords
electrode slice
valve
reaction vessel
liquid feeding
pipe
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Expired - Fee Related
Application number
CN201621317568.7U
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Chinese (zh)
Inventor
张�浩
朱明�
洪亮
王娜
邓倩
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Henan Institute of Engineering
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Henan Institute of Engineering
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Priority to CN201621317568.7U priority Critical patent/CN206285867U/en
Application granted granted Critical
Publication of CN206285867U publication Critical patent/CN206285867U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of chemical reaction negative pressure feeding structure, including closed setting reaction vessel, reaction vessel top side is connected with vacuum-pumping pipeline and dog-house, and reaction vessel top is connected with feed pipe, and feed pipe top is connected with feed hopper;The exit of feed hopper is provided with the first valve, feed pipe is provided with quantitative liquid feeding case, feed pipe between quantitative liquid feeding case and reaction vessel is provided with the second valve, feed pipe between quantitative liquid feeding case and the first valve is connected with pressure-equalizing pipe, pressure-equalizing pipe is provided with the 3rd valve, quantitative liquid feeding case is connected with bleeder pipe, and bleeder pipe is provided with the 4th valve;Dog-house is provided with the 5th valve;Liquid-level switch is provided with quantitative liquid feeding case;Using the utility model, quantifying feed case is identical with the pressure in reaction vessel during charging, is not in the phenomenon that reaction solution pours at a high speed reaction vessel.Liquid level when again due to feeding every time in quantitative liquid feeding case is identical, therefore can realize quantitative liquid feeding.

Description

Chemical reaction negative pressure feeding structure
Technical field
The utility model is related to chemical technology field, more particularly to negative reaction feeding technique.
Background technology
Many chemical products productions are carried out under condition of negative pressure, and reaction vessel is in negative pressure state in production process. When reaction vessel is in negative pressure state, it is sometimes desirable to being slowly added solution in reaction vessel.In order to ensure the mistake of addition solution Cheng Gengjia is steady reliable, it is necessary to be added the operation of solution using technologies such as decompressions, does not occur balance also in the prior art The decompression feeding structure of pressure type.Directly feeding device is connected with reaction vessel, due to the effect of negative pressure, can make material or Liquid pours reaction vessel with speed higher, and one side feeding quantity is not easy precise control, and another aspect material high-speed is poured Reaction vessel, it is also possible to which what influence was reacted is normally carried out.
Utility model content
The purpose of this utility model is to provide a kind of chemical reaction negative pressure feeding structure, can realize stablizing liquid feeding, and And be easily controlled each liquid volume added, while can when liquid level reaches precalculated position automatic processing circuit.
To achieve the above object, chemical reaction negative pressure feeding structure of the present utility model includes that the reaction of closed setting is held Device, reaction vessel top side is connected with vacuum-pumping pipeline and dog-house, and reaction vessel top is connected with feed pipe, feed pipe top Portion is connected with the feed hopper for containing liquid;The exit of feed hopper is provided with the first valve, and feed pipe is provided with quantitative liquid feeding Case, the feed pipe between quantitative liquid feeding case and reaction vessel is provided with the second valve, between quantitative liquid feeding case and the first valve Feed pipe is connected with pressure-equalizing pipe, and the lower end of pressure-equalizing pipe is connected with reaction vessel, and pressure-equalizing pipe is provided with the 3rd Valve, quantitative liquid feeding box top is connected with bleeder pipe, and bleeder pipe is provided with the 4th valve;The 5th valve is provided with dog-house;It is fixed Liquid-level switch is provided with amount liquid feeding case;
Quantitative liquid feeding case lateral wall is provided with audible-visual annunciator, and audible-visual annunciator is connected with power supply, the power supply, sound and light alarm Device and liquid-level switch are connected by wired in series.
The top side wall of the reaction vessel is provided with vacuum meter and thermometer.
The liquid-level switch includes the open cylinder for setting of upper and lower ends, and cylinder top is symmetrical to be hinged with left electrode Piece and right electrode slice, left electrode slice and right electrode slice are in the curved surface that concave surface is downward, upper surface and the cylinder left end of left electrode slice Left spring is connected between top, right spring, left electrode slice are connected between the upper surface of right electrode slice and cylinder right-hand member top Up-narrow and down-wide toroidal construction of switch is constituted with right electrode slice;
Cylinder middle part is provided with annular backup pad, and endoporus is provided with the middle part of annular backup pad, and annular backup pad has been connected up The spacing slide cartridge that open at both ends is set, spacing slide cartridge is located at the surface of endoporus and is located at the underface of the construction of switch; The ball float being made up of ambroin is slidably connected in spacing slide cartridge, ball float is hollow setting, and the external diameter of ball float is interior more than described The diameter in hole;
The ball float left end is fixedly connected with left slider and its right-hand member is fixedly connected with right sliding block, the inner surface of spacing slide cartridge Left side offers the vertical chute in the left side being adapted with the left slider, and the inner surface right side of spacing slide cartridge offers and the right cunning The vertical chute in the right side that block is adapted;Left slider is slidably connected in left vertical chute, and right sliding block is slidably connected at right vertical chute It is interior;The metal foil for turning on left electrode slice and right electrode slice is covered with the top of the ball float;The ball float passes downwardly through company Wiring is connected with cone shell-shaped baffle plate, and cone shell-shaped baffle plate tip is upward and its bottom external diameter is more than the diameter of the endoporus.
The utility model has the following advantages:
Using the utility model, by operating first to fourth valve, quantifying feed case holds with reaction when can make charging Pressure in device is identical, therefore is not in the phenomenon that reaction solution pours at a high speed reaction vessel.It is quantitative when again due to feeding every time Liquid level in liquid feeding case is identical, therefore can realize quantitative liquid feeding.
The vacuum and temperature in reaction vessel can be easily monitored by vacuum meter and thermometer, it is corresponding so as to carry out Regulation, it is ensured that reaction is stably carried out in predetermined parameter area.
When liquid level reaches precalculated position, ball float can drive metal foil to rise and contacted with left electrode slice and right electrode slice, So as to turning circuit.Because ball float is made up of ambroin in itself, metal foil is not contacted with liquid, therefore will not make liquid band Electricity.
Cone shell-shaped baffle plate tip is upward and its bottom external diameter is more than the diameter of the endoporus, so as to ensure cone shell-shaped baffle plate energy Enough play a part of valve, the endoporus can be sealed.
Left electrode slice and right electrode slice in the curved surface that concave surface is downward, compared with planar structure, can have more with metal foil Big contact area, strengthens conductive capability.
Liquid-level switch can either easily be connected in circuit by left electrode slice and right electrode slice, and liquid is prevented from again It is powered, can liquid level reach precalculated position when automatic processing circuit.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model;
Fig. 2 is warning circuit schematic diagram of the present utility model;
Fig. 3 is the structural representation of liquid-level switch in the utility model.
Specific embodiment
As shown in Figure 1 to Figure 3, chemical reaction negative pressure feeding structure of the present utility model includes the reaction vessel of closed setting 31, the top side of reaction vessel 31 is connected with vacuum-pumping pipeline 32 and dog-house 33, and the top of reaction vessel 31 is connected with feed pipe 34, the top of feed pipe 34 is connected with the feed hopper 35 for containing liquid;The exit of feed hopper 35 is provided with the first valve 36, enters Expects pipe 34 is provided with quantitative liquid feeding case 37, and the feed pipe 34 between quantitative liquid feeding case 37 and reaction vessel 31 is provided with the second valve 38, the feed pipe 34 between the valve 36 of quantitative liquid feeding case 37 and first is connected with pressure-equalizing pipe 39, under pressure-equalizing pipe 39 End is connected with the top of reaction vessel 31, and pressure-equalizing pipe 39 is provided with the 3rd valve 40, the connection of the top of quantitative liquid feeding case 37 There is bleeder pipe 41, bleeder pipe 41 is provided with the 4th valve 42;The 5th valve 43 is provided with dog-house 33;Top in quantitative liquid feeding case 37 Liquid-level switch 44 is provided with portion position;
The lateral wall of quantitative liquid feeding case 37 is provided with audible-visual annunciator 45, and audible-visual annunciator 45 is connected with power supply 46, the power supply 46th, audible-visual annunciator 45 and liquid-level switch 44 are connected in series by wire 47.The top side wall of the reaction vessel 31 is provided with very Empty table 48 and thermometer 49.
Power supply 46, audible-visual annunciator 45, vacuum meter 48 and thermometer 49 are existing apparatus, and concrete structure is no longer described in detail.
The liquid-level switch 44 includes the open cylinder 1 for setting of upper and lower ends, and the top of cylinder 1 is symmetrical to be hinged with a left side Electrode slice 2 and right electrode slice 3, left electrode slice 2 and right electrode slice 3 in the downward curved surface in concave surface, the upper surface of left electrode slice 2 with Left spring 4 is connected between the left end of cylinder 1 top, right bullet is connected between the upper surface of right electrode slice 3 and the right-hand member of cylinder 1 top Spring 5, left electrode slice 2 and right electrode slice 3 constitute up-narrow and down-wide toroidal construction of switch;
The middle part of cylinder 1 is provided with annular backup pad 6, and the middle part of annular backup pad 6 is provided with endoporus 15, and annular backup pad 6 is upward The spacing slide cartridge 7 of open at both ends setting is connected with, spacing slide cartridge 7 is located at the surface of endoporus 15 and is located at the construction of switch Underface;The ball float 8 being made up of ambroin is slidably connected in spacing slide cartridge 7, ball float 8 is hollow setting, outside ball float 8 Footpath is more than the diameter of the endoporus 15, so as to ensure that ball float 8 will not fall down from annular backup pad 6.
The left end of the ball float 8 is fixedly connected with left slider 9 and its right-hand member is fixedly connected with right sliding block 10, spacing slide cartridge 7 Inner surface left side offers the vertical chute 11 in the left side being adapted with the left slider 9, and the inner surface right side of spacing slide cartridge 7 offers The vertical chute 12 in the right side being adapted with the right sliding block 10;Left slider 9 is slidably connected in left vertical chute 11, and right sliding block 10 is slided It is dynamic to be connected in right vertical chute 12;The top of the ball float 8 is covered with the gold for turning on left electrode slice 2 and right electrode slice 3 Category paper tinsel 13.
The ball float 8 passes downwardly through connecting line 16 and is connected with cone shell-shaped baffle plate 14, the tip of cone shell-shaped baffle plate 14 upward and its Bottom external diameter, so as to ensure that cone shell-shaped baffle plate 14 can play a part of valve, can be sealed more than the diameter of the endoporus 15 The endoporus 15.
When using, vacuum-pumping pipeline 32 is connected with external vavuum pump, opens the 5th valve 43, entered by dog-house 33 Row initially feeds intake, and when the existing liquid of reactant has solid again, the first to the 5th valve 43 can be opened, by the He of dog-house 33 Feed hopper 35 is respectively to addition solid-state reactants and reaction solution in reaction vessel 31.The first to the 5th valve 43 is then shut off, is opened Vavuum pump is opened, reaction vessel 31 is vacuumized, the vacuum in reaction vessel 31 is monitored by vacuum meter 48, when reaction is held Vacuum in device 31 is reached after the scope of setting, closes vavuum pump, is reacted.
In course of reaction, it is necessary to in the reaction vessel 31 in negative pressure state supplement reaction solution when, open the first valve 36 and the 4th valve 42, to reaction solution is added in quantitative liquid feeding case 37, the air in quantitative liquid feeding case 37 is by the 4th valve 42 Discharge.When the liquid level in quantitative liquid feeding case 37 rises to predetermined altitude, liquid-level switch 44 is closed, so that turning circuit, makes sound Light crossing-signal 45 sends acousto-optic prompting, and operating personnel in time close the first valve 36 and the 4th valve 42.Then the 3rd is opened Valve 40, makes pressure-equalizing pipe 39 connect quantitative liquid feeding case 37 and reaction vessel 31.Now the pressure in quantitative liquid feeding case 37 with Reaction vessel 31 is identical, is then shut off the 3rd valve 40, opens the second valve 38, enters the reaction solution in quantitative liquid feeding case 37 Reaction vessel 31.Because pressure is identical, therefore be not in that reaction solution pours at a high speed the phenomenon of reaction vessel 31.Again due to each Liquid level during charging in quantitative liquid feeding case 37 is identical, therefore can realize quantitative liquid feeding.The second valve is turned off after the completion of liquid feeding 38。
The course of work of liquid-level switch 44 is:Left electrode slice 2 and right electrode slice 3 are connected in series in circuit, by cylinder Body 1 is installed at predetermined monitoring liquid level.After liquid level is risen in spacing slide cartridge 7, ball float 8 rises in the presence of buoyancy, When liquid level is sufficiently high, ball float 8 is set to increase and when the left electrode slice 2 of top pressure and right electrode slice 3, metal foil 13 connects the He of left electrode slice 2 Right electrode slice 3, so that circuit is connected.When ball float 8 moves up and down in spacing slide cartridge 7, left slider 9, right sliding block 10 and a left side Vertical chute 11 and right vertical chute 12 define ball float 8, it is not rotated, so as to prevent metal foil 13 because ball float 8 is sent out Life rotates and leaves tip position.After liquid level declines, metal foil 13 leaves left electrode slice 2 and right electrode slice 3, so as to break again Open circuit.
When liquid level is too high, cone shell-shaped baffle plate 14 is driven by ball float 8 and rises and block the endoporus 15, so that liquid Body can not go successively to spacing slide cartridge 7, ball float 8 and left electrode slice 2 and the pressure on top surface mistake of right electrode slice 3 when preventing liquid level too high It is high.When the left electrode slice 2 of the top pressure of ball float 8 and right electrode slice 3, left spring 4 and right spring 5 are compressed, so as to play a part of buffering, And in the presence of spring force, also ensure that left electrode slice 2 and right electrode slice 3 are in close contact with metal foil 13.
Above example is only used to illustrative and not limiting the technical solution of the utility model, although with reference to above-described embodiment pair The utility model has been described in detail, it will be understood by those within the art that:The utility model can still be entered Row modification or equivalent, without deviating from any modification or partial replacement of spirit and scope of the present utility model, it all should Cover in the middle of right of the present utility model.

Claims (3)

1. chemical reaction negative pressure feeding structure, it is characterised in that:Reaction vessel including closed setting, reaction vessel top side Vacuum-pumping pipeline and dog-house are connected with, reaction vessel top is connected with feed pipe, and feed pipe top is connected with for containing liquid The feed hopper of body;The exit of feed hopper is provided with the first valve, and feed pipe is provided with quantitative liquid feeding case, quantitative liquid feeding case and reaction Feed pipe between container is provided with the second valve, and the feed pipe between quantitative liquid feeding case and the first valve is connected with pressure balance Pipe, the lower end of pressure-equalizing pipe is connected with reaction vessel, and pressure-equalizing pipe is provided with the 3rd valve, and quantitative liquid feeding box top connects Bleeder pipe is connected to, bleeder pipe is provided with the 4th valve;The 5th valve is provided with dog-house;Liquid level is provided with quantitative liquid feeding case to open Close;
Quantitative liquid feeding case lateral wall is provided with audible-visual annunciator, and audible-visual annunciator is connected with power supply, the power supply, audible-visual annunciator and Liquid-level switch is connected by wired in series.
2. chemical reaction negative pressure feeding structure according to claim 1, it is characterised in that:The side wall top of the reaction vessel Portion is provided with vacuum meter and thermometer.
3. chemical reaction negative pressure feeding structure according to claim 1 and 2, it is characterised in that:The liquid-level switch includes The open cylinder for setting of upper and lower ends, cylinder top is symmetrical to be hinged with left electrode slice and right electrode slice, left electrode slice and Right electrode slice in the curved surface that concave surface is downward, left spring is connected between the upper surface of left electrode slice and cylinder left end top, right Right spring is connected between the upper surface of electrode slice and cylinder right-hand member top, left electrode slice and right electrode slice composition are up-narrow and down-wide Toroidal construction of switch;
Cylinder middle part is provided with annular backup pad, and endoporus is provided with the middle part of annular backup pad, and annular backup pad has connected up two ends The open spacing slide cartridge for setting, spacing slide cartridge is located at the surface of endoporus and is located at the underface of the construction of switch;It is spacing The ball float being made up of ambroin is slidably connected in slide cartridge, ball float is hollow setting, and the external diameter of ball float is more than the endoporus Diameter;
The ball float left end is fixedly connected with left slider and its right-hand member is fixedly connected with right sliding block, the inner surface left side of spacing slide cartridge The vertical chute in the left side being adapted with the left slider is offered, the inner surface right side of spacing slide cartridge offers and the right sliding block phase The vertical chute in the right side of adaptation;Left slider is slidably connected in left vertical chute, and right sliding block is slidably connected in right vertical chute;Institute State the metal foil being covered with the top of ball float for turning on left electrode slice and right electrode slice;The ball float passes downwardly through connecting line company Cone shell-shaped baffle plate is connected to, cone shell-shaped baffle plate tip is upward and its bottom external diameter is more than the diameter of the endoporus.
CN201621317568.7U 2016-12-03 2016-12-03 chemical reaction negative pressure feeding structure Expired - Fee Related CN206285867U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621317568.7U CN206285867U (en) 2016-12-03 2016-12-03 chemical reaction negative pressure feeding structure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621317568.7U CN206285867U (en) 2016-12-03 2016-12-03 chemical reaction negative pressure feeding structure

Publications (1)

Publication Number Publication Date
CN206285867U true CN206285867U (en) 2017-06-30

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CN201621317568.7U Expired - Fee Related CN206285867U (en) 2016-12-03 2016-12-03 chemical reaction negative pressure feeding structure

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107314544A (en) * 2017-08-17 2017-11-03 重庆尚洁日化用品有限公司 Produce the heating tank of shampoo
CN111483105A (en) * 2020-04-23 2020-08-04 合肥荣丰包装制品有限公司 EPS foam material forming device and process

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107314544A (en) * 2017-08-17 2017-11-03 重庆尚洁日化用品有限公司 Produce the heating tank of shampoo
CN111483105A (en) * 2020-04-23 2020-08-04 合肥荣丰包装制品有限公司 EPS foam material forming device and process
CN111483105B (en) * 2020-04-23 2021-09-24 合肥荣丰包装制品有限公司 EPS foam material forming device and process

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170630

Termination date: 20171203