CN206240491U - A kind of macromolecular material solid phase reaction device - Google Patents

A kind of macromolecular material solid phase reaction device Download PDF

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Publication number
CN206240491U
CN206240491U CN201621361097.XU CN201621361097U CN206240491U CN 206240491 U CN206240491 U CN 206240491U CN 201621361097 U CN201621361097 U CN 201621361097U CN 206240491 U CN206240491 U CN 206240491U
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CN
China
Prior art keywords
solid phase
phase reaction
reaction device
tank body
macromolecular material
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621361097.XU
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Chinese (zh)
Inventor
郭俊峰
姚志光
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INNER MONGOLIA VOCATIONAL COLLEGE OF CHEMICAL ENGINEERING
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INNER MONGOLIA VOCATIONAL COLLEGE OF CHEMICAL ENGINEERING
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Application filed by INNER MONGOLIA VOCATIONAL COLLEGE OF CHEMICAL ENGINEERING filed Critical INNER MONGOLIA VOCATIONAL COLLEGE OF CHEMICAL ENGINEERING
Priority to CN201621361097.XU priority Critical patent/CN206240491U/en
Application granted granted Critical
Publication of CN206240491U publication Critical patent/CN206240491U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

A kind of macromolecular material solid phase reaction device, it is related to a kind of solid phase reaction device, and in particular to a kind of macromolecular material solid phase reaction device.The utility model causes solid phase reaction not exclusively to solve macromolecular material skewness, undercompounding in existing solid phase reaction device, influences the problem of product quality.The utility model includes tank body, closure, support, motor, shaft coupling, main shaft and the mixing component of upper end open, tank body is rack-mount, closure lid is at the opening of tank body upper end, motor is arranged on the upper surface of closure, main shaft is vertically arranged in tank body, the rotary shaft of motor is connected by shaft coupling with the upper end of main shaft, and the mixing component is connected with the lower end of main shaft.The utility model belongs to materialogy field.

Description

A kind of macromolecular material solid phase reaction device
Technical field
The utility model is related to a kind of solid phase reaction device, and in particular to a kind of macromolecular material solid phase reaction device, category In materialogy field.
Background technology
Solid phase reaction refer to it is all comprising solid matter participate in chemical reaction, including solid-solid reaction, solid-gas reaction, Solid-liquid reaction etc..Macromolecular material is also referred to as polymeric material, be with macromolecular compound as matrix, then equipped with other addition The material that agent is constituted.Macromolecular material by solid phase reaction can the various chemical industry commodity of production department, at present, macromolecular material The reaction unit that solid phase reaction is used is general chemistry reaction or medicinal reactor, and macromolecular material divides in reaction unit Cloth is uneven, undercompounding, causes solid phase reaction not exclusively, influences product quality.
The content of the invention
The utility model is to solve macromolecular material skewness in existing solid phase reaction device, undercompounding, Cause solid phase reaction not exclusively, influence the problem of product quality, and then propose a kind of macromolecular material solid phase reaction device.
The utility model is adopted the technical scheme that to solve the above problems:The utility model includes the tank of upper end open Body, closure, support, motor, shaft coupling, main shaft and mixing component, tank body are rack-mount, and closure lid is mounted in tank At the opening of body upper end, motor is arranged on the upper surface of closure, and main shaft is vertically arranged in tank body, motor Rotary shaft is connected by shaft coupling with the upper end of main shaft, and the mixing component is connected with the lower end of main shaft.
Further, the mixing component includes adapter sleeve, at least one cross bar and multiple puddlers, and adapter sleeve is sleeved on The lower end of main shaft, cross bar is horizontally set in tank body, and one end of cross bar is fixedly connected with the outer wall of adapter sleeve, and cross bar is along length The center line in direction is vertical with the axis of main shaft, and multiple puddlers are disposed side by side in tank body vertically, and each puddler is upper End is fixedly connected with cross bar, and center line of each puddler center line along its length with cross bar along its length hangs down Directly.
Further, the lower end of each puddler is the sphere of evagination.
Further, the utility model also includes auxiliary stand, auxiliary gas tank, conduit and auxiliary gas extension tube attached, auxiliary Gas tank is arranged on the side of support by auxiliary stand, and auxiliary gas extension tube attached is inserted on closure, aids in the outlet of gas tank Mouth is connected by conduit with auxiliary gas extension tube attached.
Further, conduit is provided with control valve.
Further, tank body is made up of shell body and inner housing, and shell body is sleeved on inner housing, the madial wall of shell body Left and the lateral wall of inner housing between and insulating foam is filled with cavity, cavity.
Further, the utility model also includes support set and at least one support bar, and support set is sleeved on main shaft, props up Strut is horizontally set in tank body, and one end of support bar is connected with the outer wall of support set, the other end and the tank body of support bar Madial wall is connected.
The beneficial effects of the utility model are:1st, stirring rod of the present utility model can make height under the drive of motor Molecular material is sufficiently mixed, and is evenly distributed, it is ensured that macromolecular material reaction is complete, it is to avoid product quality is impacted;2、 Tank body of the present utility model improves heat insulation effect, it is to avoid macromolecular material was reacting in the form of inner and outer shell suit Because tank body heat insulation effect is poor in journey, cause internal-response insufficient, product quality the problem of defect is occurred;3rd, this practicality is new Type is additionally provided with auxiliary gas tank, when course of reaction needs to import auxiliary gas, may be implemented in auxiliary gas tank filling auxiliary gas, instead Control valve is opened during answering to auxiliary gas is imported in tank body, reaction efficiency is improved;4th, mixing component of the present utility model Detachable connection is used with the lower end of main shaft, operating personnel can at any time change various sizes of stirring rod as needed.
Brief description of the drawings
Fig. 1 is overall structure diagram of the present utility model.
Specific embodiment
Specific embodiment one:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 Reaction unit includes tank body 1, closure 2, support 3, motor 4, shaft coupling 5, main shaft 6 and the mixing component of upper end open, Tank body 1 is arranged on support 3, and at the opening of the upper end of tank body 1, motor 4 is arranged on the upper of closure 2 to the lid of closure 2 On surface, main shaft 6 is vertically arranged in tank body 1, and the rotary shaft of motor 4 is connected by shaft coupling 5 with the upper end of main shaft 6, The mixing component is connected with the lower end of main shaft 6.
Specific embodiment two:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 The mixing component of reaction unit includes adapter sleeve 7, at least one cross bar 8 and multiple puddlers 9, and adapter sleeve 7 is sleeved on main shaft 6 Lower end, cross bar 8 is horizontally set in tank body 1, and one end of cross bar 8 is fixedly connected with the outer wall of adapter sleeve 7, and cross bar 8 is along length The center line in direction is vertical with the axis of main shaft 6, and multiple puddlers 9 are disposed side by side in tank body 1 vertically, and each puddler 9 Upper end be fixedly connected with cross bar 8, each center line along its length of puddler 9 with cross bar 8 along its length in Heart line is vertical.Other compositions and annexation are identical with specific embodiment one.
Specific embodiment three:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 The lower end of each puddler 9 of reaction unit is the sphere of evagination.It is arranged such, it is to avoid by high score in the rotation process of puddler 9 Sub- material is smashed, and influences reaction effect.Other compositions and annexation are identical with specific embodiment two.
Specific embodiment four:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 Reaction unit also includes auxiliary stand 10, auxiliary gas tank 11, conduit 12 and auxiliary gas extension tube attached 13, and auxiliary gas tank 11 is by auxiliary Support 10 is helped to be arranged on the side of support 3, auxiliary gas extension tube attached 13 is inserted on closure 2, aids in the gas outlet of gas tank 11 It is connected with auxiliary gas extension tube attached 13 by conduit 12.Other compositions and annexation are identical with specific embodiment one.
Specific embodiment five:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 The conduit 12 of reaction unit is provided with control valve 14.Other compositions and annexation are identical with specific embodiment four.
Specific embodiment six:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 The tank body 1 of reaction unit is made up of shell body 1-1 and inner housing 1-2, and shell body 1-1 is sleeved on inner housing 1-2, shell body 1- Left between 1 madial wall and the lateral wall of inner housing 1-2 and insulating foam is filled with cavity 1-3, cavity 1-3.Other compositions And annexation is identical with specific embodiment one.
Specific embodiment seven:Present embodiment, a kind of macromolecular material solid phase described in present embodiment are illustrated with reference to Fig. 1 Reaction unit also includes the support bar 16 of support set 15 and at least one, and support set 15 is sleeved on main shaft 6, and the level of support bar 16 sets Put in tank body 1, and one end of support bar 16 is connected with the outer wall of support set 15, the other end of support bar 16 is interior with tank body 1 Side wall connection.It is arranged such, makes to be shifted in the rotation process of main shaft 6, improve the stability that main shaft 6 is rotated, extends it Service life.Other compositions and annexation are identical with specific embodiment one.
The above, is only preferred embodiment of the present utility model, not makees any formal to the utility model Limitation, although the utility model is disclosed above with preferred embodiment, but is not limited to the utility model, any ripe Professional and technical personnel is known, is not being departed from the range of technical solutions of the utility model, when in the technology using the disclosure above Appearance makes a little change or is modified to the Equivalent embodiments of equivalent variations, as long as being without departing from technical solutions of the utility model Hold, according to technical spirit of the present utility model, within spirit of the present utility model and principle, what above example was made appoints What simple modification, equivalent and improvement etc., still falls within the protection domain of technical solutions of the utility model.

Claims (7)

1. a kind of macromolecular material solid phase reaction device, it is characterised in that:A kind of macromolecular material solid phase reaction device bag Include the tank body of upper end open(1), closure(2), support(3), motor(4), shaft coupling(5), main shaft(6)With stirring group Part, tank body(1)Installed in support(3)On, closure(2)Lid is mounted in tank body(1)At the opening of upper end, motor(4)Set In closure(2)Upper surface on, main shaft(6)It is vertically arranged in tank body(1)It is interior, motor(4)Rotary shaft pass through shaft coupling Device(5)With main shaft(6)Upper end connection, the mixing component and main shaft(6)Lower end connection.
2. a kind of macromolecular material solid phase reaction device according to claim 1, it is characterised in that:The mixing component includes Adapter sleeve(7), at least one cross bar(8)With multiple puddlers(9), adapter sleeve(7)It is sleeved on main shaft(6)Lower end, cross bar(8) It is horizontally set on tank body(1)It is interior, and cross bar(8)One end and adapter sleeve(7)Outer wall be fixedly connected, cross bar(8)Along length side To center line and main shaft(6)Axis it is vertical, multiple puddlers(9)It is disposed side by side on tank body vertically(1)It is interior, and each stirring Bar(9)Upper end and cross bar(8)It is fixedly connected, each puddler(9)Center line along its length is and cross bar(8)Along long Spend the central axis in direction.
3. a kind of macromolecular material solid phase reaction device according to claim 2, it is characterised in that:Each puddler(9)'s Lower end is the sphere of evagination.
4. a kind of macromolecular material solid phase reaction device according to claim 1, it is characterised in that:A kind of macromolecule material Material solid phase reaction device also includes auxiliary stand(10), auxiliary gas tank(11), conduit(12)With auxiliary gas extension tube attached(13), it is auxiliary Help gas tank(11)By auxiliary stand(10)Installed in support(3)Side, aid in gas extension tube attached(13)It is inserted into closure (2)On, aid in gas tank(11)Gas outlet pass through conduit(12)With auxiliary gas extension tube attached(13)Connection.
5. a kind of macromolecular material solid phase reaction device according to claim 4, it is characterised in that:Conduit(12)It is provided with control Valve processed(14).
6. a kind of macromolecular material solid phase reaction device according to claim 1, it is characterised in that:Tank body(1)By shell body (1-1)And inner housing(1-2)Composition, shell body(1-1)It is sleeved on inner housing(1-2)On, shell body(1-1)Madial wall with it is interior Housing(1-2)Lateral wall between leave cavity(1-3), cavity(1-3)It is interior filled with insulating foam.
7. a kind of macromolecular material solid phase reaction device according to claim 1, it is characterised in that:A kind of macromolecule material Material solid phase reaction device also includes support set(15)With at least one support bar(16), support set(15)It is sleeved on main shaft(6)On, Support bar(16)It is horizontally set on tank body(1)It is interior, and support bar(16)One end and support set(15)Outer wall connection, support bar (16)The other end and tank body(1)Madial wall connection.
CN201621361097.XU 2016-12-13 2016-12-13 A kind of macromolecular material solid phase reaction device Expired - Fee Related CN206240491U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621361097.XU CN206240491U (en) 2016-12-13 2016-12-13 A kind of macromolecular material solid phase reaction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621361097.XU CN206240491U (en) 2016-12-13 2016-12-13 A kind of macromolecular material solid phase reaction device

Publications (1)

Publication Number Publication Date
CN206240491U true CN206240491U (en) 2017-06-13

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Family Applications (1)

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CN201621361097.XU Expired - Fee Related CN206240491U (en) 2016-12-13 2016-12-13 A kind of macromolecular material solid phase reaction device

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Country Link
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108671803A (en) * 2018-07-08 2018-10-19 池巧明 A kind of paper pulp mixed stirring device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108671803A (en) * 2018-07-08 2018-10-19 池巧明 A kind of paper pulp mixed stirring device

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170613

Termination date: 20191213