CN206215204U - A kind of NVP polyplants - Google Patents

A kind of NVP polyplants Download PDF

Info

Publication number
CN206215204U
CN206215204U CN201621160214.6U CN201621160214U CN206215204U CN 206215204 U CN206215204 U CN 206215204U CN 201621160214 U CN201621160214 U CN 201621160214U CN 206215204 U CN206215204 U CN 206215204U
Authority
CN
China
Prior art keywords
kettle
solenoid valve
valve block
pipe
polymeric kettle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621160214.6U
Other languages
Chinese (zh)
Inventor
陈军
徐苏皖
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Qifuqing Material Technology Co Ltd
Original Assignee
Shanghai Qifuqing Material Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Qifuqing Material Technology Co Ltd filed Critical Shanghai Qifuqing Material Technology Co Ltd
Priority to CN201621160214.6U priority Critical patent/CN206215204U/en
Application granted granted Critical
Publication of CN206215204U publication Critical patent/CN206215204U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses a kind of NVP polyplants, including control device, polymeric kettle kettle and rabbling mechanism, the polymeric kettle kettle includes outer wall and inwall, and the outer wall and inner wall sealing constitute the interlayer connected with cooling water circulation pipe and water steam pipe;The second solenoid valve block is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe;The 3rd solenoid valve block is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe;The polymeric kettle kettle is internally provided with thermistor temperature sensor;The input of the controlling organization is connected with the output end of the thermistor temperature sensor, and the output end of the control device is connected with the input of the variable-frequency motor, the first solenoid valve block, the second solenoid valve block and the 3rd solenoid valve block.The utility model controls the high precision and convenience of temperature, simple structure, low cost and raising aggregate quality.

Description

A kind of NVP polyplants
Technical field
The utility model is related to a kind of field of chemical equipment, and in particular to a kind of NVP polyplants.
Background technology
Polyvinylpyrrolidone (polyvinyl pyrrolidone) abbreviation PVP, PVP are with monomer vinyl pyrrolidines Ketone (NVP) is raw material, is obtained by methods such as polymerisation in bulk, polymerisation in solutions, is a kind of non-ionic macromolecule compound, is It is most characteristic in N vinylamide polymer, and it is studied most deep, extensive fine chemicals kind.Have evolved into Nonionic, cation, the major class of anion 3, technical grade, pharmaceutical grade, 3 kinds of specifications of food-grade, relative molecular mass is from thousands of to one More than million homopolymers, copolymer and crosslinking series of polymers product, and extensive use is obtained with its excellent unique performance. In the production process of reaction generation PVP, NVP polymerisations are a most key rings in production process, therefore, polyplant It is also to generate the most key device in PVP productions.But existing polyplant complex structure and temperature are whard to control, High cost and quality is not ensured.
Utility model content
It is whard to control for existing polyplant complex structure and temperature based on this, high cost and quality is not ensured Problem, the utility model proposes a kind of NVP polyplants, can effectively solve the above problems.
The technical solution of the utility model is:
A kind of NVP polyplants, including control device, polymeric kettle kettle and rabbling mechanism, the rabbling mechanism include setting Variable-frequency motor, agitating shaft and multiple stirrer paddles at the top of polymeric kettle kettle, polymeric kettle kettle is stretched into one end of the agitating shaft Body, the other end is connected with the variable-frequency motor, and the polymeric kettle kettle top is provided with multiple feed pipes, and the feed pipe The first solenoid valve block is provided with, the polymeric kettle kettle includes outer wall and inwall, and the outer wall and inner wall sealing are constituted and cooling The interlayer that water-circulating pipe is connected with water steam pipe.Second is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe Solenoid valve block.The 3rd solenoid valve block is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe.Institute State polymeric kettle kettle and be internally provided with thermistor temperature sensor.The input of the controlling organization and the thermistor temperature Spend the output end connection of sensor, the output end of the control device and the variable-frequency motor, the first solenoid valve block, the second electromagnetism The input connection of valve group and the 3rd solenoid valve block.
Operation principle of the present utility model is:Starter, control device controls the first solenoid valve block by quantitative softening In water and NVP feeding polymeric kettle kettlies, the stirring motor of agitating device is opened, agitating device work is stirred mixing;Open 3rd solenoid valve block, rises to 70 DEG C, then control the first solenoid valve block by quantitative initiation by control device by steam by temperature Agent, ammoniacal liquor and hydrogen peroxide feeding polymeric kettle kettle in, will be warmed up to inside polymeric kettle kettle to 82 DEG C, at this moment reaction start and by Gradually acutely, the 3rd solenoid valve block is closed, when temperature rises to 92 DEG C, the first solenoid valve block is opened, is cooled down by cooling water, At this moment temperature may proceed to rise to 95 DEG C to 98 DEG C;When temperature is down to 88~90 DEG C, the first solenoid valve block is closed;Maintain temperature Steam heating can be opened to 90~95 DEG C, when temperature is low, and adds initiator, ammoniacal liquor, hydrogen peroxide drop residual several times, and detect residual It is single, until qualified, i.e. polymerization completion, after the completion of polymerization, bottom discharge mouthful blowing can be opened and ensured.Control the essence of temperature Degree is high and facilitates, simple structure, low cost and raising aggregate quality.
Further, multiple feed pipes are obliquely installed in the top of the polymeric kettle kettle.Being obliquely installed contributes to thing Material enters polymeric kettle.
The bottom of the interlayer is provided with condensate outlet pipe, and the 4th magnetic valve is provided with the condensate outlet pipe, The input of the 4th magnetic valve is connected with the output end of the control device.The water of steam condensation can be excluded, prevents from coagulating Bear water the efficiency of influence steam.
Multiple stirrer paddles are uniformly arranged on the agitating shaft from top to bottom.Can improve stirring uniformity and Stirring efficiency.
The polymeric kettle kettle is stainless steel polymeric kettle kettle.Stainless steel polymeric kettle kettle strengthens corrosion resistance and high temperature resistant Property, extend the life-span, reduces cost.
First solenoid valve block, the second solenoid valve block and the 3rd solenoid valve block are plating stainless steel solenoid valve block;Institute It is plating stainless steel magnetic valve to state the 4th magnetic valve.Strengthen the corrosion resistance of valve, extend the life-span, it is cost-effective.
The beneficial effects of the utility model are:
(1)Control the high precision and convenience of temperature, simple structure, low cost and raising aggregate quality;
(2)The feed pipe being obliquely installed contributes to material to enter polymeric kettle;
(3)Setting condensate outlet can exclude the water of steam condensation, prevent condensate from influenceing the efficiency of steam;
(4)Improve the uniformity and stirring efficiency of stirring;
(5)Polymeric kettle kettle and magnetic valve can strengthen its corrosion resistance using stainless steel, extend the life-span, save into This.
Brief description of the drawings
Fig. 1 is a kind of structure chart of NVP polyplants described in the utility model embodiment;
Description of reference numerals:
100th, polymeric kettle kettle;110th, inwall;120th, outer wall;200th, rabbling mechanism;210th, variable-frequency motor;220th, stir Axle;230th, stirrer paddle;300th, cooling water circulation pipe;310th, the second solenoid valve block;400th, water steam pipe;410th, the 3rd electricity Magnet valve group;420th, condensate outlet pipe;421st, the 4th magnetic valve;500th, feed pipe;510th, the first solenoid valve block;600th, temperature-sensitive electricity Resistance temperature sensor.
Specific embodiment
Embodiment of the present utility model is described in detail below in conjunction with the accompanying drawings.
Embodiment 1
As shown in figure 1, a kind of NVP polyplants, including control device, polymeric kettle kettle 100 and rabbling mechanism 200, institute Stating rabbling mechanism 200 includes being located at the variable-frequency motor 210 at the top of polymeric kettle kettle 100, agitating shaft 220 and multiple stirrer paddles 230, polymeric kettle kettle 100 is stretched into one end of the agitating shaft 220, and the other end is connected with the variable-frequency motor 210, the polymerization The top of kettle kettle 100 is provided with multiple feed pipes 500, and the feed pipe 500 and is provided with the first solenoid valve block 510, described Polymeric kettle kettle 100 includes outer wall 120 and inwall 110, and the outer wall 120 and the sealing of inwall 110 are constituted and cooling water circulation pipe 300 interlayers connected with water steam pipe 400.Is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe 300 Two solenoid valve blocks 310.The 3rd electromagnetism is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe 400 Valve group 410.The polymeric kettle kettle 100 is internally provided with thermistor temperature sensor 600.The input of the controlling organization Output end with the thermistor temperature sensor 600 is connected, the output end of the control device and the variable-frequency motor 210th, the input connection of the first solenoid valve block 510, the second solenoid valve block 310 and the 3rd solenoid valve block 410.
Embodiment 2
As shown in figure 1, a kind of NVP polyplants, including control device, polymeric kettle kettle 100 and rabbling mechanism 200, institute Stating rabbling mechanism 200 includes being located at the variable-frequency motor 210 at the top of polymeric kettle kettle 100, agitating shaft 220 and multiple stirrer paddles 230, polymeric kettle kettle 100 is stretched into one end of the agitating shaft 220, and the other end is connected with the variable-frequency motor 210, the polymerization The top of kettle kettle 100 is provided with multiple feed pipes 500, and the feed pipe 500 and is provided with the first solenoid valve block 510, described Polymeric kettle kettle 100 includes outer wall 120 and inwall 110, and the outer wall 120 and the sealing of inwall 110 are constituted and cooling water circulation pipe 300 interlayers connected with water steam pipe 400.Is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe 300 Two solenoid valve blocks 310.The 3rd electromagnetism is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe 400 Valve group 410.The polymeric kettle kettle 100 is internally provided with thermistor temperature sensor 600.The input of the controlling organization Output end with the thermistor temperature sensor 600 is connected, the output end of the control device and the variable-frequency motor 210th, the input connection of the first solenoid valve block 510, the second solenoid valve block 310 and the 3rd solenoid valve block 410.
Further, multiple feed pipes 500 are obliquely installed in the top of the polymeric kettle kettle 100.
Embodiment 3
As shown in figure 1, a kind of NVP polyplants, including control device, polymeric kettle kettle 100 and rabbling mechanism 200, institute Stating rabbling mechanism 200 includes being located at the variable-frequency motor 210 at the top of polymeric kettle kettle 100, agitating shaft 220 and multiple stirrer paddles 230, polymeric kettle kettle 100 is stretched into one end of the agitating shaft 220, and the other end is connected with the variable-frequency motor 210, the polymerization The top of kettle kettle 100 is provided with multiple feed pipes 500, and the feed pipe 500 and is provided with the first solenoid valve block 510, described Polymeric kettle kettle 100 includes outer wall 120 and inwall 110, and the outer wall 120 and the sealing of inwall 110 are constituted and cooling water circulation pipe 300 interlayers connected with water steam pipe 400.Is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe 300 Two solenoid valve blocks 310.The 3rd electromagnetism is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe 400 Valve group 410.The polymeric kettle kettle 100 is internally provided with thermistor temperature sensor 600.The input of the controlling organization Output end with the thermistor temperature sensor 600 is connected, the output end of the control device and the variable-frequency motor 210th, the input connection of the first solenoid valve block 510, the second solenoid valve block 310 and the 3rd solenoid valve block 410.
Further, multiple feed pipes 500 are obliquely installed in the top of the polymeric kettle kettle 100.
The bottom of the interlayer is provided with condensate outlet pipe 420, and the 4th electricity is provided with the condensate outlet pipe 420 Magnet valve 421, the input of the 4th magnetic valve 421 is connected with the output end of the control device.
Many embodiments 4
As shown in figure 1, a kind of NVP polyplants, including control device, polymeric kettle kettle 100 and rabbling mechanism 200, institute Stating rabbling mechanism 200 includes being located at the variable-frequency motor 210 at the top of polymeric kettle kettle 100, agitating shaft 220 and multiple stirrer paddles 230, polymeric kettle kettle 100 is stretched into one end of the agitating shaft 220, and the other end is connected with the variable-frequency motor 210, the polymerization The top of kettle kettle 100 is provided with multiple feed pipes 500, and the feed pipe 500 and is provided with the first solenoid valve block 510, described Polymeric kettle kettle 100 includes outer wall 120 and inwall 110, and the outer wall 120 and the sealing of inwall 110 are constituted and cooling water circulation pipe 300 interlayers connected with water steam pipe 400.Is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe 300 Two solenoid valve blocks 310.The 3rd electromagnetism is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe 400 Valve group 410.The polymeric kettle kettle 100 is internally provided with thermistor temperature sensor 600.The input of the controlling organization Output end with the thermistor temperature sensor 600 is connected, the output end of the control device and the variable-frequency motor 210th, the input connection of the first solenoid valve block 510, the second solenoid valve block 310 and the 3rd solenoid valve block 410.
Further, multiple feed pipes 500 are obliquely installed in the top of the polymeric kettle kettle 100.
The bottom of the interlayer is provided with condensate outlet pipe 420, and the 4th electricity is provided with the condensate outlet pipe 420 Magnet valve 421, the input of the 4th magnetic valve 421 is connected with the output end of the control device.
Multiple stirrer paddles 230 are uniformly arranged on the agitating shaft 220 from top to bottom.
Embodiment 5
As shown in figure 1, a kind of NVP polyplants, including control device, polymeric kettle kettle 100 and rabbling mechanism 200, institute Stating rabbling mechanism 200 includes being located at the variable-frequency motor 210 at the top of polymeric kettle kettle 100, agitating shaft 220 and multiple stirrer paddles 230, polymeric kettle kettle 100 is stretched into one end of the agitating shaft 220, and the other end is connected with the variable-frequency motor 210, the polymerization The top of kettle kettle 100 is provided with multiple feed pipes 500, and the feed pipe 500 and is provided with the first solenoid valve block 510, described Polymeric kettle kettle 100 includes outer wall 120 and inwall 110, and the outer wall 120 and the sealing of inwall 110 are constituted and cooling water circulation pipe 300 interlayers connected with water steam pipe 400.Is provided with the water inlet pipe and outlet pipe of the cooling water circulation pipe 300 Two solenoid valve blocks 310.The 3rd electromagnetism is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe 400 Valve group 410.The polymeric kettle kettle 100 is internally provided with thermistor temperature sensor 600.The input of the controlling organization Output end with the thermistor temperature sensor 600 is connected, the output end of the control device and the variable-frequency motor 210th, the input connection of the first solenoid valve block 510, the second solenoid valve block 310 and the 3rd solenoid valve block 410.
Further, multiple feed pipes 500 are obliquely installed in the top of the polymeric kettle kettle 100.
The bottom of the interlayer is provided with condensate outlet pipe 420, and the 4th electricity is provided with the condensate outlet pipe 420 Magnet valve 421, the input of the 4th magnetic valve 421 is connected with the output end of the control device.
Multiple stirrer paddles 230 are uniformly arranged on the agitating shaft 220 from top to bottom.
The polymeric kettle kettle 100 is stainless steel polymeric kettle kettle.
First solenoid valve block 510, the second solenoid valve block 310 and the 3rd solenoid valve block 410 are plating stainless steel electricity Magnet valve group;4th magnetic valve 421 is plating stainless steel magnetic valve.
Embodiment described above only expresses specific embodiment of the present utility model, and its description is more specific and detailed, But therefore can not be interpreted as the limitation to the utility model the scope of the claims.It should be pointed out that common for this area For technical staff, without departing from the concept of the premise utility, various modifications and improvements can be made, these all belong to In protection domain of the present utility model.

Claims (6)

1. a kind of NVP polyplants, including control device, polymeric kettle kettle and rabbling mechanism, the rabbling mechanism include being located at Polymeric kettle kettle is stretched into variable-frequency motor, agitating shaft and multiple stirrer paddles at the top of polymeric kettle kettle, one end of the agitating shaft, The other end is connected with the variable-frequency motor, and the polymeric kettle kettle top is provided with multiple feed pipes, and the feed pipe and sets It is equipped with the first solenoid valve block, it is characterised in that the polymeric kettle kettle includes outer wall and inwall, the outer wall and inner wall sealing structure Into the interlayer connected with cooling water circulation pipe and water steam pipe;Set on the water inlet pipe and outlet pipe of the cooling water circulation pipe It is equipped with the second solenoid valve block;The 3rd electromagnetism is provided with the vapor air inlet pipe and vapor escaping pipe of the water steam pipe Valve group;The polymeric kettle kettle is internally provided with thermistor temperature sensor;The input of the controlling organization and the heat The output end connection of quick RTD, the output end of the control device and the variable-frequency motor, the first solenoid valve block, The input connection of the second solenoid valve block and the 3rd solenoid valve block.
2. a kind of NVP polyplants according to claim 1, it is characterised in that multiple feed pipes be obliquely installed in The top of the polymeric kettle kettle.
3. a kind of NVP polyplants according to claim 1, it is characterised in that the bottom of the interlayer is provided with condensation Water outlet pipe, is provided with the 4th magnetic valve, the input of the 4th magnetic valve and the control on the condensate outlet pipe The output end connection of device.
4. a kind of NVP polyplants according to claim 1, it is characterised in that multiple stirrer paddles are from top to bottom It is uniformly arranged on the agitating shaft.
5. a kind of NVP polyplants according to claim 1, it is characterised in that the polymeric kettle kettle is poly- for stainless steel Close kettle kettle.
6. a kind of NVP polyplants according to claim 3, it is characterised in that the first solenoid valve block, the second solenoid valve block Plating stainless steel solenoid valve block is with the 3rd solenoid valve block;4th magnetic valve is plating stainless steel magnetic valve.
CN201621160214.6U 2016-11-01 2016-11-01 A kind of NVP polyplants Expired - Fee Related CN206215204U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621160214.6U CN206215204U (en) 2016-11-01 2016-11-01 A kind of NVP polyplants

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621160214.6U CN206215204U (en) 2016-11-01 2016-11-01 A kind of NVP polyplants

Publications (1)

Publication Number Publication Date
CN206215204U true CN206215204U (en) 2017-06-06

Family

ID=58789266

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621160214.6U Expired - Fee Related CN206215204U (en) 2016-11-01 2016-11-01 A kind of NVP polyplants

Country Status (1)

Country Link
CN (1) CN206215204U (en)

Similar Documents

Publication Publication Date Title
JP5231390B2 (en) Method and apparatus for processing high viscosity products
CN103936252B (en) A kind of continous way tower reactor for sludge hot hydrolysis treatment
CN206152804U (en) Reation kettle that energy -conserving self -loopa is preheated
WO2009107765A1 (en) Process for production of thermoplastic copolymer
CN204699671U (en) Chemical laboratory reactor
Lin et al. Highly efficient synthesis of polyvinyl butyral (PVB) using a membrane dispersion microreactor system and recycling reaction technology
JP4112255B2 (en) Method for producing impact-resistant monovinyl aromatic polymer
CN112661910A (en) Impact-resistant polystyrene with capacity of more than 5 ten thousand tons and equipment and production process thereof
CN206215204U (en) A kind of NVP polyplants
CN103421206A (en) Preparation method for acrylonitrile/methacrylic acid copolymer foamed plastic
CN206951192U (en) A kind of waste-heat recovery device of heat-conducting oil heating reactor
CN102101898B (en) Method for continuously preparing polymer and device thereof
CN206381984U (en) PVP polyplants
CN208302780U (en) A kind of temperature of reaction kettle regulating device
CN108607487A (en) A kind of New Polyacrylamide synthesizer
CN107617410A (en) Highly effective reaction device
CN105457580A (en) Reaction kettle
CN104650265B (en) A kind of solution polymerization process synthetic rubber polyreaction removes by the use of thermal means
CN206152797U (en) PVP polymeric kettle
CN106434293A (en) Rotary type biological fermentation container
JPH04218512A (en) Production of styrene-based resin
CN217431649U (en) Polymeric pan feeding device of polymeric kettle
CN105885041B (en) Production equipment, the method for a kind of device being used to prepare polyamide 5X, separation method and polyamide 5X
CN217511866U (en) Equipment for continuously producing styrene butadiene rubber
CN216367939U (en) Agitating unit is used in PVP production

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170606

Termination date: 20181101

CF01 Termination of patent right due to non-payment of annual fee