CN206184451U - Energy -concerving and environment -protective production calcium chloride device of reation kettle formula acid -proof fog - Google Patents
Energy -concerving and environment -protective production calcium chloride device of reation kettle formula acid -proof fog Download PDFInfo
- Publication number
- CN206184451U CN206184451U CN201621225321.2U CN201621225321U CN206184451U CN 206184451 U CN206184451 U CN 206184451U CN 201621225321 U CN201621225321 U CN 201621225321U CN 206184451 U CN206184451 U CN 206184451U
- Authority
- CN
- China
- Prior art keywords
- acid
- calcium chloride
- environment
- energy
- reation kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 title claims abstract description 23
- 239000001110 calcium chloride Substances 0.000 title claims abstract description 23
- 229910001628 calcium chloride Inorganic materials 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 239000002253 acid Substances 0.000 title abstract description 29
- 239000003595 mist Substances 0.000 claims abstract description 30
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 238000011084 recovery Methods 0.000 claims abstract description 19
- 229910001220 stainless steel Inorganic materials 0.000 claims abstract description 4
- 239000010935 stainless steel Substances 0.000 claims abstract description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract description 28
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 abstract description 12
- 229910000019 calcium carbonate Inorganic materials 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract description 3
- 238000005096 rolling process Methods 0.000 abstract description 2
- 238000005086 pumping Methods 0.000 abstract 2
- 239000000243 solution Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
The utility model discloses an energy -concerving and environment -protective production calcium chloride device of reation kettle formula acid -proof fog, it belongs to the energy -concerving and environment -protective production field of calcium chloride, the control unit comprises a reaction vessel, reation kettle upper portion is equipped with acid adding port and charge door, and acid adding port is used for adding hydrochloric acid, and the charge door is used for adding calcium carbonate, the reation kettle bottom is equipped with spiral shell sucker -rod pumping, and spiral shell sucker -rod pumping is used for carrying away reacted calcium chloride, the mouth is retrieved to last being equipped with of acid adding port, retrieve mouthful and to be connected through connecting pipe and the recovery pump of establishing the reation kettle bottom, the connecting pipe adopts the stainless steel flexible hose, it is equipped with the breather pipe to retrieve the pump other end, the breather pipe gos deep into reation kettle inner chamber bottom, through the recovery mouth structure on the acid adding port, and the acid mist of production when eo -acid process and violent reaction sequence are added in timely absorption to carry the reation kettle bottom through the breather pipe with the acid mist, not only can retrieve the acid mist, can also produce the effect of rolling to its inside, accelerate the reaction between calcium carbonate and the hydrochloric acid.
Description
Technical field
The utility model is related to calcium chloride energy-conserving and environment-protective production field, and in particular to one kind reaction autoclave acid-mist energy-saving ring
Protect production calcium chloride device.
Background technology
Hydrochloric acid is the aqueous solution of hydrogen chloride, is the unitary strong acid of water white transparency, and hydrochloric acid has extremely strong volatility, therefore beats
Open and can see above it after the container for filling concentrated hydrochloric acid white haze, it is actual to be combined with the vapor in air after volatile hydrogen chloride
The hydrochloric acid droplet of generation, hydrochloric acid clear, colorless or yellow, irritant smell and severe corrosive, if the unreasonable profit of acid mist
With it volatilizees away will cause the pollution in whole workshop and external environment condition, and calcium chloride can be used for drier, and refined calcium chloride can
Agent is converted for food, electronics industry and distillation oil, ether alcohol.
The production of calcium chloride can be acted on and obtained with calcium carbonate and hydrochloric acid, due to substantial amounts of heat can be distributed in production process,
Carbon dioxide and water are produced, for the enterprise that reactor produces calcium chloride, its hydrochloric acid will not produce acid fog outflow, improve substantially
The environment in whole workshop, but during eo-acid is added, because its violent reaction can cause to be arranged in this process acid mist
High-volume increase, cause acid mist to discharge reactor, influence the environment in workshop, secondly in order to ensure that reaction is fully mostly filled in reactor
There is stirring, although can accelerate to react but take up room.
The content of the invention
For the problems of in the prior art, a kind of reaction autoclave acid-mist energy-conserving and environment-protective that the utility model is provided
Production calcium chloride device, will can just add acid mist rationally secondary utilization during new hydrochloric acid, reduce the extraneous discharge of acid mist, accelerate
Reaction speed.
To achieve these goals, the technical solution adopted in the utility model is as follows：One kind reaction autoclave acid-mist energy-conservation
Environmental protection production calcium chloride device, including reactor, the reactor top is provided with acid-adding port and charge door, the reactor bottom
Screw pump is provided with, the acid-adding port is provided with recovery port, and the recovery port passes through connecting tube and the recovery for being located at reactor bottom
Pump is connected, and the recovery pump other end is provided with breather pipe, and the breather pipe gos deep into reactor intracavity bottom.
As preferred technical scheme, guide plate is provided with the acid-adding port, between the guide plate and acid-adding port shell
Cavity is provided with, the guide plate is provided with gap.
Used as preferred technical scheme, the acid-adding port top is provided with screw thread.
Used as preferred technical scheme, the part that the breather pipe gos deep into reactor intracavity bottom is evenly distributed with some leading to
Stomata.
Used as preferred technical scheme, the connecting tube uses stainless steel flexible hose.
The utility model is beneficial in that：
1., by the recovery mouth structure on acid-adding port, produced when timely drawing addition eo-acid process and vigorous reaction process
Acid mist, prevent from being diffused into workshop to personnel and environmental pollution.
2. the acid mist that recovery pump is drawn is passed through by breather pipe from reactor bottom, can not only reclaim acid mist, can be with
Accelerate the reaction between calcium carbonate and hydrochloric acid.
3. cavity is provided between guide plate and acid-adding port shell, it is ensured that be capable of the absorption acid mist of even circumferential in gap.
4. the passage on breather pipe produces the effect of stirring more preferable by internal solution, reacts more violent.
5. acid-adding port is provided with screw thread mouth, can according to circumstances facilitate and acid-adding port is blocked.
Brief description of the drawings
Fig. 1 is a kind of overall structure figure for reacting autoclave acid-mist energy-conserving and environment-protective production calcium chloride device；
Fig. 2 is a kind of acid-adding port structure chart for reacting autoclave acid-mist energy-conserving and environment-protective production calcium chloride device；
Fig. 3 is a kind of acid-adding port sectional view for reacting autoclave acid-mist energy-conserving and environment-protective production calcium chloride device.
In figure：1- reactors, 2- screw pumps, 3- breather pipes, 4- recovery pumps, 5- connecting tubes, 6- acid-adding ports, 7- charge doors,
8- recovery ports, 9- cavitys, 10- gaps, 11- guide plates, 12- screw threads.
Specific embodiment
For the ease of it will be appreciated by those skilled in the art that being further described to the utility model below in conjunction with the accompanying drawings.
As shown in figure 1, a kind of reaction autoclave acid-mist energy-conserving and environment-protective production calcium chloride device, including reactor 1, it is described anti-
The top of kettle 1 is answered to be provided with acid-adding port 6 and charge door 7, acid-adding port 6 is used for adding hydrochloric acid, and charge door 7 is used for adding calcium carbonate, described
The bottom of reactor 1 is provided with screw pump 2, and screw pump 2 is used for transferring out in reacted calcium chloride, and the acid-adding port 6 is provided with
Recovery port 8, the recovery port 8 is connected by connecting tube 5 with the recovery pump 4 for being located at the bottom of reactor 1, and the connecting tube 5 is used
Stainless steel flexible hose, the other end of the recovery pump 4 is provided with breather pipe 3, and the breather pipe 3 gos deep into the intracavity bottom of reactor 1, by adding
The structure of recovery port 8 on sour mouth 6, timely draws the acid mist produced during addition eo-acid process and vigorous reaction process, and lead to
Cross breather pipe 3 and acid mist is transported to the bottom of reactor 1, acid mist can not only be reclaimed, additionally it is possible to the effect of rolling is produced to its inside
Really, the reaction between calcium carbonate and hydrochloric acid is accelerated.
As shown in Figure 2 and Figure 3, guide plate 11 is provided with the acid-adding port 6, guide plate 11 can lead to acid mist flowing generation
To, cavity 9 is provided between the guide plate 11 and the shell of acid-adding port 6, the guide plate 11 is provided with gap 10, and cavity 9 can
Pressure when ensureing that its gap 10 is drawn, the absorption acid mist of the even circumferential of acid-adding port 6, the top of the acid-adding port 6 is provided with screw thread 12,
Can according to circumstances facilitate and acid-adding port 6 is blocked.
The part that the breather pipe 3 gos deep into the intracavity bottom of reactor 1 is evenly distributed with some passages, on breather pipe 3
Passage produces the effect of stirring more preferable by internal solution, reacts more violent.
It should be appreciated that the purposes of these embodiments is merely to illustrate the utility model and is not intended to limit of the present utility model
Protection domain.Additionally, it will also be appreciated that after technology contents of the present utility model have been read, those skilled in the art can be right
The utility model makes various changes, modification and/or modification, and all these equivalent form of value equally falls within right appended by the application will
Ask within the protection domain that book limited.
Claims (5)
1. a kind of reaction autoclave acid-mist energy-conserving and environment-protective production calcium chloride device, including reactor, the reactor top is provided with
Acid-adding port and charge door, the reactor bottom are provided with screw pump, it is characterised in that：The acid-adding port is provided with recovery port, institute
State recovery port to be connected with the recovery pump for being located at reactor bottom by connecting tube, the recovery pump other end is provided with breather pipe, institute
State breather pipe and go deep into reactor intracavity bottom.
2. a kind of reaction autoclave acid-mist according to claim 1 energy-conserving and environment-protective produce calcium chloride device, it is characterised in that：
Guide plate is provided with the acid-adding port, cavity is provided between the guide plate and acid-adding port shell, between the guide plate is provided with
Gap.
3. a kind of reaction autoclave acid-mist according to claim 1 energy-conserving and environment-protective produce calcium chloride device, it is characterised in that：
The acid-adding port top is provided with screw thread.
4. a kind of reaction autoclave acid-mist according to claim 1 energy-conserving and environment-protective produce calcium chloride device, it is characterised in that：
The part that the breather pipe gos deep into reactor intracavity bottom is evenly distributed with some passages.
5. a kind of reaction autoclave acid-mist according to claim 1 energy-conserving and environment-protective produce calcium chloride device, it is characterised in that：
The connecting tube uses stainless steel flexible hose.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621225321.2U CN206184451U (en) | 2016-11-14 | 2016-11-14 | Energy -concerving and environment -protective production calcium chloride device of reation kettle formula acid -proof fog |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621225321.2U CN206184451U (en) | 2016-11-14 | 2016-11-14 | Energy -concerving and environment -protective production calcium chloride device of reation kettle formula acid -proof fog |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206184451U true CN206184451U (en) | 2017-05-24 |
Family
ID=58725704
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621225321.2U Expired - Fee Related CN206184451U (en) | 2016-11-14 | 2016-11-14 | Energy -concerving and environment -protective production calcium chloride device of reation kettle formula acid -proof fog |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206184451U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107117992A (en) * | 2017-06-12 | 2017-09-01 | 贵州诺威施生物工程有限公司 | Calcium chloride preparation system and calcium chloride preparation method |
-
2016
- 2016-11-14 CN CN201621225321.2U patent/CN206184451U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107117992A (en) * | 2017-06-12 | 2017-09-01 | 贵州诺威施生物工程有限公司 | Calcium chloride preparation system and calcium chloride preparation method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 262725 Shandong city of Weifang province Shouguang Hou Town Industrial Park Dongxin Road No. 28 Patentee after: SHANDONG DONGXIN NEW MATERIALS TECHNOLOGY CO.,LTD. Address before: 262725 Shandong city of Weifang province Shouguang Hou Town Industrial Park Dongxin Road No. 28 Patentee before: SHANDONG DONGXIN CHEMICAL Co.,Ltd. |
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| CP01 | Change in the name or title of a patent holder | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170524 |
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| CF01 | Termination of patent right due to non-payment of annual fee |