CN206184019U - Take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator - Google Patents

Take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator Download PDF

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Publication number
CN206184019U
CN206184019U CN201621234757.8U CN201621234757U CN206184019U CN 206184019 U CN206184019 U CN 206184019U CN 201621234757 U CN201621234757 U CN 201621234757U CN 206184019 U CN206184019 U CN 206184019U
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China
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rectifying
tower
dividing wall
column
gas
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CN201621234757.8U
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Chinese (zh)
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李绍通
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Luoyang Hemeng Technology Co Ltd
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Luoyang Hemeng Technology Co Ltd
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Abstract

The utility model discloses a take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator, include: by the division board rectifying columns such as non - that division board rectification tower segment such as multistage non -, a section or multiple ends gas -liquid modulator, the supporting body flange of rectifying column constitute, the raw materials trades heat treatment unit, top of the tower material processing unit, material processing unit at the bottom of the tower. The utility model discloses the difficult problem that operating flexibility is little, the adjustment of production technical scheme is difficult and three above multicomponent material separation device investment is big, the energy consumption is high that take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator had solved the rectifying column device.

Description

The combined non-decile dividing wall column device of multistage with gas-liquid modulator
Technical field
The utility model is related to the device of spiral-screen column of fractional distillation process in petrochemical industry production, belongs to petrochemical technology neck Domain.
Background technology
In chemical separation process, rectifying column is most widely used fractionation separation equipment, but defect is to invest big, energy consumption Higher, in the industries such as oil refining, petrochemical industry, the ratio that its energy consumption accounts for overall process is even as high as 70%, and equipment investment is more than 50%.
Partitioned column has low energy consumption and inexpensive huge advantage as novel distillation tower for multicomponent rectification.At present Ternary mixture separation is mainly used in, partitioned column is the longitudinally disposed one piece of dividing plate along tower in common rectifying column, every Tower body middle part is divided into the subregions such as left and right two by plate, and compared to common rectifying column, the uprising gas of dividing plate tower bottom will It is allocated in dividing plate both sides, product purity and energy consumption in the gas apportioning cost influence distillation process of dividing plate both sides are appropriate The energy consumption that gas apportioning cost can not only reduce partitioned column can also be significantly increased the purity of rectifying product.
Iris type rectifying column generates more operation frees degree due to its structure and the complexity of technique, energy-conservation and obtains The product not a duck soup of high-purity is taken, it is necessary to the controllability of internal system variable is stronger, cause iris type rectifying column every control Problem becomes a principal element for hindering its commercial Application, will particularly enter the uprising gas of dividing plate tower bottom in dividing plate Both sides are allocated, and product purity and energy consumption in this apportioning cost influence distillation process, appropriate gas apportioning cost not only may be used To reduce the energy consumption of partitioned column, the purity of rectifying product can also be significantly increased, the air flow rate of both sides how to distribute and Effective control problem turns into industry focus of attention.Relative to common rectifying column, iris type rectifying column need regulation simultaneously every The liquid and bottom of towe that plate upper end drops to dividing plate both sides rise to the gas of dividing plate both sides.Adjusted because gas is distributed in dividing plate both sides Section is related to the series of computation processes such as elevation computation, the dynamic analog of operating parameter, the analysis in gas-liquid two-phase flow field of complexity, Thus, there is difficulty very high in the distribution regulation and control of dividing plate both sides gas.
At present, generally using gas by the way of dividing plate both sides are freely distributed, the ratio for freely distributing is by partitioned column Portion's component(Such as packed height, the column plate number of plies, flow channel area)With the operation operating mode decision in tower, the rising gas of bottom of towe Body will comply with the equal rule of left and right sides pressure drop and be automatically assigned to dividing plate both sides.
The weight of influence gas distribution can all be turned into due to the change of feed composition and state and the allocation proportion etc. of liquid Factor is wanted, thus the optimal operating conditions of partitioned column can not be usually reached in the gas flow ratio that dividing plate both sides are distributed automatically.
Gas distribution regulation and control are that the special inner member of design adjusts gas phase distribution to change dividing plate both sides pressure drop composition Purpose, for example, dividing plate bottom install one piece can with the baffle plate of shift position, changed by the change in location of the baffle plate every The circulation area of plate both sides, so as to change gas phase distribution ratio, dividing plate both sides is changed using inner member or by the eccentric placement in next door Pressure drop, not only its operating flexibility is smaller, sensitivity is low, and due to mechanical wear caused by baffle plate movement so that equipment can not Long-period stable operation.
A kind of dividing plate fractionating column and its gas-liquid flow control methods are disclosed in PCT/US2011/056079 patent documents, The dividing plate fractionating column includes that tower body, gas phase are collected and distribution structure and liquid phase collection and distribution structure, wherein, gas phase is collected and divided With mainly by the bypass gas phase pipeline with regulating valve and flowmeter outside tower, with reference to automatically control the distribution of realizing gas with Control.The technical scheme major defect is:Firstly, since gas phase is drawn and gas phase is again introduced into being required to be set in Ta Nei in tower Gas phase apparatus for redistributing is put, so increased the complexity of tower height and internals;Secondly, for production disposal ability it is larger every Plate tower, the diameter for bypassing gas phase pipeline can be very big, and associated components are installed and maintenance is inconvenient;Again, for regulating valve and The bypass gas phase pipeline of flowmeter, not only increases tower height, and the characteristic of gas flow pressure drop will also become sufficiently complex, pressure drop Conference causes the downspout liquid flooding below dividing plate, and system is by cisco unity malfunction;Finally, the size of regulating valve is with unit scale And change, investment will become sufficiently expensive, and can not sensitively and accurately regulate and control gas phase flow rate in the range of lower drag drop.
Chinese patent 201320829355.2 discloses a kind of gas allocation device in partitioned column, is examined using flow Survey device, controller, cylinder, dividing plate, square separate slot, downspout, inlet channel, square valve block governor motion, sleeve, rotating shaft, Motor and gas distribution mechanism.The design defect that the device is primarily present is:There is performance of control curve not in adjusting gas flow Rule, it is not easy to realize fine setting, regulation control law is poor, the defect such as tolerance is non-linear;The resistance drop of dividing plate both sides gas is anti- Should be delayed, square valve block does not possess fine setting characteristic, causes the sane regulation difficult to realize of square valve block governor motion;Due in tower There is drive disk assembly, lubrication and wear problem are relatively difficult to resolve and can certainly influence the long period of equipment to run well.
Aforementioned barriers formula rectifying column thermal coupling technological operation variable is more, and many parameters intercouple, dividing plate both sides Gas flow and its dependent variable physical relation it is complicated, gas is to ensure to produce in effective distribution of dividing plate both sides and robust control The important means of product index and reducing energy consumption, urgent need has advanced technological means to solve this industrial problem.
Utility model content
Technical problem to be solved in the utility model is:
The operating flexibility of existing device of spiral-screen column is small, production technology project setting is difficult and more than three multi-component masses point From plant investment is big, high energy consumption problem.
The utility model solves the technical scheme that the technical problem used:
The combined non-decile dividing wall column device of multistage with gas-liquid modulator, including:Demarcation strip essence is waited by multistage is non- Evaporate tower section, one section or multiterminal gas-liquid modulator(10), the supporting body flange of rectifying column(33)The non-decile dividing wall column for constituting, Raw material heat exchange processing unit, tower top material processing unit, materials at bottom of tower processing unit;It is characterized in that:It is non-to wait demarcation strip rectifying Non- decile dividing wall column stage casing (9) charging aperture of tower is managed with the feed(raw material)inlet of raw material heat exchange processing unit(7)Connection;Non- decile The rectifying tower top of dividing wall column(13)By rectifying column top duct(15)With rectifying column top feed back pipeline(18)With Tower top material processing unit is connected;The rectifying tower reactor of non-decile dividing wall column(1)By bottom of towe thermal material circulation pipe(32)With Materials at bottom of tower outlet(3)It is connected with materials at bottom of tower processing unit.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Tower top Material processing unit is by rectifying column top duct(15), rectifying tower top cooler(16), rectifying tower top cooler recirculated water turnover Mouth pipe(17), rectifying column top feed back pipeline(18), rectifying tower top return tank(19), thermometer(14), pressure gauge(29)、 Rectifying column top material outlet pipe(20), rectifying column top feed back pump(21)And supporting valve, pipeline, pipe fitting, electric instrument Control device is constituted;Rectifying column top duct(15)Connection rectifying tower top cooler(16), rectifying tower top cooler(16)Connection Rectifying tower top return tank(19), rectifying column top feed back pump(21)Entrance connects rectifying tower top return tank(19)Bottom, essence Evaporate top of tower feed back pump(21)Outlet connection rectifying column top feed back pipeline(18)With rectifying column top material outlet Pipe(20).
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Raw material Heat exchange processing unit is by materials at bottom of tower delivery pump(2), materials at bottom of tower outlet(3), stage casing material-handling pump(4), stage casing material Outlet(5), raw material materials at bottom of tower heat exchanger(6), feed(raw material)inlet pipe(7), raw material stage casing material heat exchanger(8)And supporting valve Door, pipeline, pipe fitting, electric instrument control control equipment are constituted;Manage feed(raw material)inlet(7)With raw material stage casing material heat exchanger(8)With raw material tower bottom Material heat exchanger(6)Tube side be sequentially connected after, with non-decile dividing wall column stage casing(9)Feed pipe connection;Materials at bottom of tower Outlet(3)With materials at bottom of tower delivery pump(2)Afterwards, with raw material materials at bottom of tower heat exchanger(6)Shell side connection, then with rectifying tower reactor (1)Discharge nozzle is connected;Stage casing material outlet pipe(5)With stage casing material-handling pump(4)Afterwards, with raw material stage casing material heat exchanger (8)Shell side connection, then with non-decile dividing wall column stage casing(9)Outlet connection.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Bottom of towe Material processing unit is managed by non-decile dividing wall column bottom reboiler heating agent gateway(30), non-decile dividing wall column bottom reboiling Device (31), bottom of towe thermal material circulation pipe (32) and supporting valve, pipeline, pipe fitting, electric instrument control control equipment are constituted;The hot thing of bottom of towe After material circulation pipe (32) is connected with non-decile dividing wall column bottom reboiler (31) tube side, with rectifying tower reactor(1)Upper pipe connects Connect.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:It is non-etc. Demarcation strip rectifying column is by rectifying tower top(13), multistage non-decile dividing wall column section, one or more snippets gas-liquid modulator(10), essence Evaporate tower reactor(1), the supporting body flange of rectifying column and connecting bolt(33)Composition;The non-of non-decile dividing wall column waits demarcation strip essence Evaporate tower section and gas-liquid modulator(10)By the supporting body flange of rectifying column and connecting bolt(33)Connection;One section of non-grade demarcation strip Rectifying tower section and one section of gas-liquid modulator(10)After connection, then it is connected with another section of non-decile dividing wall column section;Rectifying tower top (13)With non-decile dividing wall column section epimere(11)Connection, non-decile dividing wall column hypomere(26)With rectifying tower reactor(1)Even Connect.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:It is non-etc. Demarcation strip rectifying tower section is main by rectifying tower section, rectifying column internal partition, the supporting body flange of rectifying column and connecting bolt(33), essence Evaporate inner-tower filling material and match mechanism or tower tray and match mechanism, feed pipe, discharge nozzle and supporting valve, pipeline, pipe fitting, electric instrument Control device is constituted;Rectifying column inner chamber is separated into two parts that volume is not waited by rectifying column internal partition, and two partial volume ratios are 1:0.95~1:0.60.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Gas-liquid Modulator(10)Mainly by rectifying tower section, heat exchanger and inlet/outlet pipe(23), the supporting body flange of rectifying column and connecting bolt (33)And supporting valve, pipeline, pipe fitting, electric instrument equipment control composition;Heat exchanger is coiled, or shell and tube, in pipe Logical recirculated water or raw material.
The beneficial effects of the utility model are:
1st, the rectifying column of device of spiral-screen column is mainly using the combined non-decile dividing wall column section of multistage and gas-liquid regulation and control Device is constituted, and when production processing parameter adjustment amplitude is larger, can rapidly increase by one section or two sections combined non-decile Dividing wall column section and gas-liquid modulator, improve device disposal ability, produce high quality of products.
2nd, the combined non-decile dividing wall column section of the multistage of device of spiral-screen column is spaced with gas-liquid modulator and installs, Ke Yitong The recirculated water or mass flow of gas-liquid modulator inside heat exchanger are overregulated, gas-liquid allocation proportion is adjusted, meeting production technology will Ask.
3rd, rectifying column inner chamber is separated into volume two parts not etc. by the dividing plate in non-decile rectifying tower section, can be according to every Material component distribution in section rectifying column is adjusted, and the key component of content is discharged from capacious rectifying tower section compartment Mouth extraction, further improves equipment efficiency of usage.
4th, for multi-component masses, the particularly 4 disposable cuttings of component above material are separated, band of the present utility model The combined non-decile dividing wall column device of multistage of gas-liquid modulator can make the reserved outlet input of every section of rectifying column With separation more multicomponent.
5th, the heat of high-temperature product and raw material is carried out heat exchange by raw material heat exchange processing unit, substantially increase device Heating efficiency, reduces plant energy consumption.
Brief description of the drawings
The utility model is further illustrated with reference to the accompanying drawings and examples.
Fig. 1 is that the combined non-decile dividing wall column apparatus structure of the multistage with gas-liquid modulator of the present utility model is illustrated Figure.
In figure, 1, rectifying tower reactor;2nd, materials at bottom of tower delivery pump;3rd, materials at bottom of tower outlet;4th, stage casing material-handling pump;5、 Stage casing material outlet pipe;6th, raw material materials at bottom of tower heat exchanger;7th, feed(raw material)inlet pipe;8th, raw material stage casing material heat exchanger;9th, it is non-etc. Demarcation strip rectifying midsection;10th, gas-liquid modulator;11st, non-decile dividing wall column epimere;12nd, on non-decile dividing wall column Section dividing plate;13rd, rectifying tower top;14th, thermometer;15th, rectifying column top duct;16th, rectifying tower top cooler;17th, rectifying tower top Cooler recirculated water inlet/outlet pipe;18th, rectifying column top feed back pipeline;19th, rectifying tower top return tank;20th, rectifying tower top Portion's material outlet pipe;21st, rectifying column top feed back pump;22nd, the reserved outlet of non-decile dividing wall column epimere material; 23rd, gas-liquid modulator heat exchanger and gateway are managed;24th, non-decile dividing wall column stage casing material outlet pipe;25th, it is non-etc. to separate Plate rectifying midsection dividing plate;26th, non-decile dividing wall column hypomere;27th, non-decile dividing wall column hypomere dividing plate;28th, it is non-etc. Demarcation strip rectifying column hypomere material reserves outlet;29th, pressure gauge;30th, non-decile dividing wall column bottom reboiler heating agent comes in and goes out Mouth pipe;31st, non-decile dividing wall column bottom reboiler;32nd, bottom of towe thermal material circulation pipe;33rd, the supporting body flange of rectifying column and Connecting bolt.
Specific embodiment
The utility model is further illustrated below by embodiment, but and be not so limited claims guarantor Shield content.
Embodiment
The combined non-decile dividing wall column apparatus structure of multistage with gas-liquid modulator of the present utility model is as follows:
The combined non-decile dividing wall column device of multistage with gas-liquid modulator, including:Demarcation strip essence is waited by multistage is non- Evaporate tower section, one section or multiterminal gas-liquid modulator(10), the supporting body flange of rectifying column(33)The non-decile dividing wall column for constituting, Raw material heat exchange processing unit, tower top material processing unit, materials at bottom of tower processing unit;It is characterized in that:It is non-to wait demarcation strip rectifying Non- decile dividing wall column stage casing (9) charging aperture of tower is managed with the feed(raw material)inlet of raw material heat exchange processing unit(7)Connection;Non- decile The rectifying tower top of dividing wall column(13)By rectifying column top duct(15)With rectifying column top feed back pipeline(18)With Tower top material processing unit is connected;The rectifying tower reactor of non-decile dividing wall column(1)By bottom of towe thermal material circulation pipe(32)With Materials at bottom of tower outlet(3)It is connected with materials at bottom of tower processing unit.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Tower top Material processing unit is by rectifying column top duct(15), rectifying tower top cooler(16), rectifying tower top cooler recirculated water turnover Mouth pipe(17), rectifying column top feed back pipeline(18), rectifying tower top return tank(19), thermometer(14), pressure gauge(29)、 Rectifying column top material outlet pipe(20), rectifying column top feed back pump(21)And supporting valve, pipeline, pipe fitting, electric instrument Control device is constituted;Rectifying column top duct(15)Connection rectifying tower top cooler(16), rectifying tower top cooler(16)Connection Rectifying tower top return tank(19), rectifying column top feed back pump(21)Entrance connects rectifying tower top return tank(19)Bottom, essence Evaporate top of tower feed back pump(21)Outlet connection rectifying column top feed back pipeline(18)With rectifying column top material outlet Pipe(20).
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Raw material Heat exchange processing unit is by materials at bottom of tower delivery pump(2), materials at bottom of tower outlet(3), stage casing material-handling pump(4), stage casing material Outlet(5), raw material materials at bottom of tower heat exchanger(6), feed(raw material)inlet pipe(7), raw material stage casing material heat exchanger(8)And supporting valve Door, pipeline, pipe fitting, electric instrument control control equipment are constituted;Manage feed(raw material)inlet(7)With raw material stage casing material heat exchanger(8)With raw material tower bottom Material heat exchanger(6)Tube side be sequentially connected after, with non-decile dividing wall column stage casing(9)Feed pipe connection;Materials at bottom of tower Outlet(3)With materials at bottom of tower delivery pump(2)Afterwards, with raw material materials at bottom of tower heat exchanger(6)Shell side connection, then with rectifying tower reactor (1)Discharge nozzle is connected;Stage casing material outlet pipe(5)With stage casing material-handling pump(4)Afterwards, with raw material stage casing material heat exchanger (8)Shell side connection, then with non-decile dividing wall column stage casing(9)Outlet connection.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Bottom of towe Material processing unit is managed by non-decile dividing wall column bottom reboiler heating agent gateway(30), non-decile dividing wall column bottom reboiling Device (31), bottom of towe thermal material circulation pipe (32) and supporting valve, pipeline, pipe fitting, electric instrument control control equipment are constituted;The hot thing of bottom of towe After material circulation pipe (32) is connected with non-decile dividing wall column bottom reboiler (31) tube side, with rectifying tower reactor(1)Upper pipe connects Connect.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:It is non-etc. Demarcation strip rectifying column is by rectifying tower top(13), multistage non-decile dividing wall column section, one or more snippets gas-liquid modulator(10), essence Evaporate tower reactor(1), the supporting body flange of rectifying column and connecting bolt(33)Composition;The non-of non-decile dividing wall column waits demarcation strip essence Evaporate tower section and gas-liquid modulator(10)By the supporting body flange of rectifying column and connecting bolt(33)Connection;One section of non-grade demarcation strip Rectifying tower section and one section of gas-liquid modulator(10)After connection, then it is connected with another section of non-decile dividing wall column section;Rectifying tower top (13)With non-decile dividing wall column section epimere(11)Connection, non-decile dividing wall column hypomere(26)With rectifying tower reactor(1)Even Connect.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:It is non-etc. Demarcation strip rectifying tower section is main by rectifying tower section, rectifying column internal partition, the supporting body flange of rectifying column and connecting bolt(33), essence Evaporate inner-tower filling material and match mechanism or tower tray and match mechanism, feed pipe, discharge nozzle and supporting valve, pipeline, pipe fitting, electric instrument Control device is constituted;Rectifying column inner chamber is separated into two parts that volume is not waited by rectifying column internal partition, and two partial volume ratios are 1:0.95~1:0.60.
According to the combined non-decile dividing wall column device of the above-mentioned multistage with gas-liquid modulator, it is characterised in that:Gas-liquid Modulator(10)Mainly by rectifying tower section, heat exchanger and inlet/outlet pipe(23), the supporting body flange of rectifying column and connecting bolt (33)And supporting valve, pipeline, pipe fitting, electric instrument equipment control composition;Heat exchanger is coiled, or shell and tube, in pipe Logical recirculated water or raw material.

Claims (7)

1. the combined non-decile dividing wall column device of multistage with gas-liquid modulator, including:Demarcation strip rectifying is waited by multistage is non- Tower section, one section or multiterminal gas-liquid modulator(10), the supporting body flange of rectifying column(33)The non-decile dividing wall column for constituting, it is former Material heat exchange processing unit, tower top material processing unit, materials at bottom of tower processing unit;It is characterized in that:Non- decile dividing wall column Non- decile dividing wall column stage casing (9) charging aperture and raw material heat exchange processing unit feed(raw material)inlet pipe(7)Connection;Non- grade separates The rectifying tower top of plate rectifying column(13)By rectifying column top duct(15)With rectifying column top feed back pipeline(18)With tower Top material processing unit connection;The rectifying tower reactor of non-decile dividing wall column(1)By bottom of towe thermal material circulation pipe(32)And tower Bottom material outlet pipe(3)It is connected with materials at bottom of tower processing unit.
2. the combined non-decile dividing wall column device of the multistage with gas-liquid modulator according to claim 1, its feature It is:Tower top material processing unit is by rectifying column top duct(15), rectifying tower top cooler(16), rectifying tower top cooler follows Ring water entrance pipe(17), rectifying column top feed back pipeline(18), rectifying tower top return tank(19), thermometer(14), pressure Power table(29), rectifying column top material outlet pipe(20), rectifying column top feed back pump(21)And supporting valve, pipeline, Pipe fitting, electric instrument control control equipment are constituted;Rectifying column top duct(15)Connection rectifying tower top cooler(16), rectifying tower top cooler (16)Connection rectifying tower top return tank(19), rectifying column top feed back pump(21)Entrance connects rectifying tower top return tank(19) Bottom, rectifying column top feed back pump(21)Outlet connection rectifying column top feed back pipeline(18)With rectifying column headpiece Material outlet(20).
3. the combined non-decile dividing wall column device of the multistage with gas-liquid modulator according to claim 1, its feature It is:Raw material exchanges heat processing unit by materials at bottom of tower delivery pump(2), materials at bottom of tower outlet(3), stage casing material-handling pump(4)、 Stage casing material outlet pipe(5), raw material materials at bottom of tower heat exchanger(6), feed(raw material)inlet pipe(7), raw material stage casing material heat exchanger(8)And Supporting valve, pipeline, pipe fitting, electric instrument control control equipment composition;Manage feed(raw material)inlet(7)With raw material stage casing material heat exchanger(8)With Raw material materials at bottom of tower heat exchanger(6)Tube side be sequentially connected after, with non-decile dividing wall column stage casing(9)Feed pipe connection; Materials at bottom of tower outlet(3)With materials at bottom of tower delivery pump(2)Afterwards, with raw material materials at bottom of tower heat exchanger(6)Shell side connection, then with Rectifying tower reactor(1)Discharge nozzle is connected;Stage casing material outlet pipe(5)With stage casing material-handling pump(4)Afterwards, changed with raw material stage casing material Hot device(8)Shell side connection, then with non-decile dividing wall column stage casing(9)Outlet connection.
4. the combined non-decile dividing wall column device of the multistage with gas-liquid modulator according to claim 1, its feature It is:Materials at bottom of tower processing unit is managed by non-decile dividing wall column bottom reboiler heating agent gateway(30), the demarcation strip essence such as non- Evaporate bottom reboiler (31), bottom of towe thermal material circulation pipe (32) and supporting valve, pipeline, pipe fitting, electric instrument control control equipment structure Into;After bottom of towe thermal material circulation pipe (32) is connected with non-decile dividing wall column bottom reboiler (31) tube side, with rectifying tower reactor(1) Upper pipe is connected.
5. the combined non-decile dividing wall column device of the multistage with gas-liquid modulator according to claim 1, its feature It is:Non- decile dividing wall column is by rectifying tower top(13), multistage non-decile dividing wall column section, the regulation and control of one or more snippets gas-liquid Device(10), rectifying tower reactor(1), the supporting body flange of rectifying column(33)And connecting bolt composition;Non- decile dividing wall column it is non- Decile dividing wall column section and gas-liquid modulator(10)By the supporting body flange of rectifying column(33)And connecting bolt connection;One section Duan Yuyi sections of gas-liquid modulator of non-decile dividing wall column(10)After connection, then with another section of non-decile dividing wall column Duan Lian Connect;Rectifying tower top(13)With non-decile dividing wall column section epimere(11)Connection, non-decile dividing wall column hypomere(26)With essence Evaporate tower reactor(1)Connection.
6. the combined non-decile dividing wall column device of the multistage with gas-liquid modulator according to claim 1, its feature It is:Non- decile dividing wall column section is main by rectifying tower section, rectifying column internal partition, the supporting body flange of rectifying column(33)And even Connecting bolt, rectifying inner-tower filling material and match mechanism or tower tray and match mechanism, feed pipe, discharge nozzle and supporting valve, pipeline, Pipe fitting, electric instrument control control equipment are constituted;Rectifying column inner chamber is separated into two parts that volume is not waited, two by the dividing plate in rectifying tower section Partial volume ratio is 1:0.95~1:0.60.
7. the combined non-decile dividing wall column device of the multistage with gas-liquid modulator according to claim 1, its feature It is:Gas-liquid modulator(10)Mainly by rectifying tower section, heat exchanger and inlet/outlet pipe(23), the supporting body flange of rectifying column (33)And connecting bolt and supporting valve, pipeline, pipe fitting, electric instrument equipment control composition;Heat exchanger is coiled, or row Tubular type;Logical recirculated water or raw material in pipe.
CN201621234757.8U 2016-11-17 2016-11-17 Take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator Expired - Fee Related CN206184019U (en)

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CN201621234757.8U CN206184019U (en) 2016-11-17 2016-11-17 Take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator

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Application Number Priority Date Filing Date Title
CN201621234757.8U CN206184019U (en) 2016-11-17 2016-11-17 Take division board rectifying column devices such as combined non - of multistage of gas -liquid modulator

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CN206184019U true CN206184019U (en) 2017-05-24

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