CN206089548U - Low temperature resistant epoxy gluing agent apparatus for producing - Google Patents
Low temperature resistant epoxy gluing agent apparatus for producing Download PDFInfo
- Publication number
- CN206089548U CN206089548U CN201621039802.4U CN201621039802U CN206089548U CN 206089548 U CN206089548 U CN 206089548U CN 201621039802 U CN201621039802 U CN 201621039802U CN 206089548 U CN206089548 U CN 206089548U
- Authority
- CN
- China
- Prior art keywords
- storage tank
- epoxy
- low temperature
- temperature resistant
- pump
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Epoxy Resins (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The utility model provides a low temperature resistant epoxy gluing agent apparatus for producing mainly includes: epoxy chloropropyl alcohol storage tank, triethylamine storage tank, feedstock pump, reation kettle, delivery pump, curing agent storage tank, relation of connection between each component parts of apparatus for producing does: the triethylamine storage tank is connected with feedstock pump, and epoxy chloropropyl alcohol storage tank is connected with feedstock pump, and reation kettle is connected with feedstock pump and delivery pump respectively, and feedstock pump is connected with the curing agent storage tank, wherein, epoxy chloropropyl alcohol storage tank full volume 5.5 - 6.5L, 3600 - 3800mm of total length, 710 - 730mm of pot diameter in the reation kettle, 820 - 860mm of outer pot diameter, 6.5 - 7.5mm of epoxy chloropropyl alcohol storage tank barrel wall thickness, reation kettle nominal volume 350 - 380L.
Description
Technical field
The present invention relates to a kind of low temperature resistant epoxy adhesive process units.
Background technology
Low temperature resistant epoxy adhesive contains various polarity group and the very big epoxy radicals of activity, thus with metal, glass, water
The various polarity material such as mud, timber, plastics, the especially high material of surface-active have very strong bonding force, while epoxy is solid
The cohesive strength of compound is also very big, so its glue-joint strength is very high.Produce substantially free of low molecular weight volatile thing during solidification.Glue-line
Cubical contraction is little, and about 1% one 2%, it is one of minimum kind of cure shrinkage in thermosetting resin.Adding can drop after filler
To less than 0.2%.The linear expansion coefficient of epoxy curing compound also very little.Therefore internal stress is little, affects little to glue-joint strength.In addition epoxy
The creep of solidfied material is little, so the good stability of the dimension of glue-line.Therefore, low temperature resistant epoxy adhesive process units is good and bad for carrying
High yield quality, reduces by-products content and has Important Economic meaning.
The content of the invention
It is an object of the invention to provide a kind of low temperature resistant epoxy adhesive process units, mainly includes：Epoxy chloropropionate alcohol
Storage tank (F101), triethylamine storage tank (F102), raw material pump (J101, J102, J103), reactor (D101), delivery pump (J104),
Curing agent storage tank (F103)；Annexation between process units each part is：Triethylamine storage tank (F102) and raw material
Pump (J102) is connected, and epoxy chloropropionate alcohol storage tank (F101) is connected with raw material pump (J101), reactor (D101) respectively with original
Material pump (J101, J102, J103) is connected with delivery pump (J104), and raw material pump (J103) is connected with curing agent storage tank (F103)
Connect；Wherein, epoxy chloropropionate alcohol storage tank (F101) 5.5-6.5L of total volume, 3600-3800mm of total length；In reactor (D101)
Pot 710-730mm of diameter, outer pot 820-860mm of diameter；Wherein, described epoxy chloropropionate alcohol storage tank (F101) cylinder wall thickness
6.5—7.5mm；Described reactor (D101) 350-380L of nominal volume.
A kind of low temperature resistant epoxy adhesive process units, production procedure is：Equal benzene triamide and F101 epoxy prapanols are added
Enter reactor D101, under the effect of F102 catalyst of triethylamine carry out that the shrink of trimesic acid three is synthesized out at 8-10 DEG C
Glyceride, 70-75 DEG C of product fusing point, epoxide number 0.76-0.79 is the major ingredient of adhesive, sequentially adds butyronitrile-40, curing agent
With α-ethyl -4-methylimidazole, calcium carbonate, it is mixed uniform, you can make low temperature adhesive product.
The invention has the advantages that：Reaction intermediate link is reduced, reaction temperature and reaction time is reduced, reaction is improve
Yield.
Description of the drawings
Fig. 1 is a kind of low temperature resistant epoxy adhesive process units,
Mainly include：Epoxy chloropropionate alcohol storage tank (F101), triethylamine storage tank (F102), raw material pump (J101, J102,
J103), reactor (D101), delivery pump (J104), curing agent storage tank (F103)；
Specific embodiment
With reference to example is embodied as, the invention will be further described：
A kind of low temperature resistant epoxy adhesive process units,
Example 1：
Raw materials for production and consumption
Equal benzene triamide and F101 epoxy prapanols are added into reactor D101,8 under the effect of F102 catalyst of triethylamine
Carry out that trimesic acid three-glycidyl ester, 70 DEG C of product fusing point is synthesized out at DEG C, epoxide number 0.76 is the major ingredient of adhesive,
Butyronitrile -40, curing agent and α-ethyl -4-methylimidazole, calcium carbonate are sequentially added, is mixed uniform, you can make low temperature resistant
Adhesive product 1.
The property of product 1
| Outward appearance | The thick colloid of Dark grey | Adhesion strength (steel-steel shearing) | >19MPa |
| Solid content | >93.5% |
Example 2：
Raw materials for production and consumption
| 1,3,5- benzene trimethamides | Technical grade | 150 | Butyronitrile -40 | Technical grade | 22 |
| Epoxy chloropropionate alcohol | Technical grade | 350 | α-ethyl -4-methylimidazole | Reagent | 23 |
| Triethylamine | Technical grade | In right amount | Calcium carbonate | Technical grade | 39 |
Equal benzene triamide and F101 epoxy prapanols are added into reactor D101,9 under the effect of F102 catalyst of triethylamine
Carry out that trimesic acid three-glycidyl ester, 72 DEG C of product fusing point is synthesized out at DEG C, epoxide number 0.77 is the major ingredient of adhesive,
Butyronitrile -40, curing agent and α-ethyl -4-methylimidazole, calcium carbonate are sequentially added, is mixed uniform, you can make low temperature resistant
Adhesive product 2.
The property of product 2
| Outward appearance | The thick colloid of Dark grey | Adhesion strength (steel-steel shearing) | >23MPa |
| Solid content | >95.7% |
Example 3：
Raw materials for production and consumption
Equal benzene triamide and F101 epoxy prapanols are added into reactor D101,10 under the effect of F102 catalyst of triethylamine
Carry out that trimesic acid three-glycidyl ester, 75 DEG C of product fusing point is synthesized out at DEG C, epoxide number 0.79 is the major ingredient of adhesive,
Butyronitrile -40, curing agent and α-ethyl -4-methylimidazole, calcium carbonate are sequentially added, is mixed uniform, you can make low temperature resistant
Adhesive product 3.
The property of product 3
| Outward appearance | The thick colloid of Dark grey | Adhesion strength (steel-steel shearing) | >26MPa |
| Solid content | >97.8% |
Claims (3)
1. a kind of low temperature resistant epoxy adhesive process units, it is characterised in that mainly include：Epoxy chloropropionate alcohol storage tank (F101),
Triethylamine storage tank (F102), raw material pump (J101, J102, J103), reactor (D101), delivery pump (J104), curing agent storage tank
(F103)；Annexation between process units each part is：Triethylamine storage tank (F102) and raw material pump (J102) phase
Connection, epoxy chloropropionate alcohol storage tank (F101) is connected with raw material pump (J101), reactor (D101) respectively with raw material pump (J101,
J102, J103) it is connected with delivery pump (J104), raw material pump (J103) is connected with curing agent storage tank (F103)；Wherein, epoxy
Chloropropyl alcohol storage tank (F101) 5.5-6.5L of total volume, 3600-3800mm of total length；The interior pot diameter 710 of reactor (D101)-
730mm, outer pot 820-860mm of diameter.
2. a kind of low temperature resistant epoxy adhesive process units according to claim 1, it is characterised in that described epoxy chloropropionate
Alcohol storage tank (F101) 6.5-7.5mm of cylinder wall thickness.
3. a kind of low temperature resistant epoxy adhesive process units according to claim 1, it is characterised in that described reactor
(D101) 350-380L of nominal volume.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621039802.4U CN206089548U (en) | 2016-09-06 | 2016-09-06 | Low temperature resistant epoxy gluing agent apparatus for producing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621039802.4U CN206089548U (en) | 2016-09-06 | 2016-09-06 | Low temperature resistant epoxy gluing agent apparatus for producing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206089548U true CN206089548U (en) | 2017-04-12 |
Family
ID=58475930
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621039802.4U Expired - Fee Related CN206089548U (en) | 2016-09-06 | 2016-09-06 | Low temperature resistant epoxy gluing agent apparatus for producing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206089548U (en) |
-
2016
- 2016-09-06 CN CN201621039802.4U patent/CN206089548U/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102358717B (en) | Alicyclic epoxy acrylate prepolymer and preparation method thereof | |
| CN104312508B (en) | A kind of epoxy resin adhesive and preparation method thereof | |
| JP2011089071A5 (en) | ||
| CN105001591B (en) | Ionic liquid toughening type pentaerythritol acrolein resin and curing method thereof | |
| CN105837797A (en) | A water-based epoxy resin curing agent | |
| CN110194942A (en) | A kind of low-temperature rapid thermal cured one-component epoxy adhesive and preparation method thereof | |
| CN206089548U (en) | Low temperature resistant epoxy gluing agent apparatus for producing | |
| CN107778774B (en) | Epoxy resin adhesive film and preparation method thereof | |
| CN107603431B (en) | A kind of amino-stoving varnish multi-functional promotor and preparation method thereof | |
| WO2013101531A3 (en) | Curable water soluble epoxy acrylate resin compositions | |
| CN108822695A (en) | A kind of modified resin oil paint | |
| CN108865033A (en) | A kind of high removing toughness folding adhesive and preparation method thereof | |
| CN104388026A (en) | Dual-component solvent-free epoxy damping adhesive for marine use and preparation method thereof | |
| CN107793977A (en) | A kind of low temperature resistant epoxy adhesive process units | |
| CN106318233A (en) | Binding agent for attaching trim layer to glass fiber reinforced plastic digestion tank | |
| CN108239258B (en) | Modified epoxy resin, preparation method thereof and LED lamp bead packaging material | |
| CN109957234A (en) | A kind of corrosion-resisting resin and preparation method | |
| CN107903847A (en) | A kind of compound wooden case adhesive and preparation method thereof | |
| CN104356358B (en) | The preparation method of dimer acid modified itaconic acid epoxide resin | |
| CN205969956U (en) | Tubular product mould | |
| CN206089547U (en) | Glutinous agent apparatus for producing of monocomponent epoxy glue | |
| CN106459380A (en) | Fast curing resin compositions, manufacture and use thereof | |
| CN105856545A (en) | Pipe mold | |
| CN103524685A (en) | Unsaturated polyester resin dedicated to manufacturing mining anchor rods and preparation method thereof | |
| CN103289627A (en) | Weather-proof injection-type bar-planting adhesive tube based on acrylic epoxy resin as well as preparation method and use method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170412 Termination date: 20170906 |