CN206082522U - Accurate preparation glass reactor for silver powder - Google Patents

Accurate preparation glass reactor for silver powder Download PDF

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Publication number
CN206082522U
CN206082522U CN201621089275.8U CN201621089275U CN206082522U CN 206082522 U CN206082522 U CN 206082522U CN 201621089275 U CN201621089275 U CN 201621089275U CN 206082522 U CN206082522 U CN 206082522U
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CN
China
Prior art keywords
reactor
kettle
argentum powder
accurately
electric heating
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Active
Application number
CN201621089275.8U
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Chinese (zh)
Inventor
张树利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Inreal Optoelectronic Material Technology Co., Ltd.
China Pingmei Shenma Energy and Chemical Group Co Ltd
Original Assignee
Suzhou Inreal Optoelectronic Material Technology Co Ltd
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Priority to CN201621089275.8U priority Critical patent/CN206082522U/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/60Glass recycling

Abstract

The utility model relates to a machining device especially relates to an accurate preparation glass reactor for silver powder, including having the reation kettle that can dismantle the kettle cover, reation kettle electricity thermal clip cover, agitating unit and at least one high pressure nozzle, agitating unit includes puddler and stirring head, still include the grinding head, the outside at reation kettle is established to reation kettle electricity thermal clip ways, reation kettle electricity thermal clip cover bottom be equipped with pass reation kettle electricity thermal clip cover bottom and with the communicating discharge gate of reation kettle, be equipped with at least one feed inlet on the kettle cover, still be equipped with the high pressure nozzle who is linked together with the feed inlet in the reation kettle, the puddler passes reation kettle's kettle cover and fixes continuously with the stirring head in the reation kettle, the bottom of stirring head is equipped with the grinding head, the utility model provides an accurate preparation glass reactor for silver powder can the accurate silver powder of preparing certain particle diameter.

Description

One kind accurately prepares argentum powder glass reaction kettle
Technical field
This utility model is related to chemical field, more particularly to one kind accurately prepares argentum powder glass reaction kettle.
Background technology
Argentum powder preparing device is to carry out most widely used argentum powder by additive methods such as liquid phase reductions or electrolysis The preparation facilitiess of volume production, are mainly used in chemical industry manufacture field;The simple process that argentum powder is prepared in prior art is typically adopted The preparation method of quick stirring is carried out in clear glass instrument, in order to prepare the silver powder particles in certain particle size range, can be adjusted The speed stirred in course of reaction prepared by argentum powder generally prepares the accuracy rate of different-grain diameter argentum powder not controlling reaction condition Good control, also easily increased production cost.
Utility model content
To solve above-mentioned technical problem, the purpose of this utility model is to provide a kind of argentum powder that can accurately prepare certain particle diameter Accurately prepare argentum powder glass reaction kettle.
It is of the present utility model accurately to prepare argentum powder glass reaction kettle, including the reactor with detachable kettle cover, reaction Kettle electric heating chuck, agitating device and at least one high-pressure nozzle, the agitating device includes puddler and stirring-head, also including grinding Bistrique, the reactor electric heating chuck is set in the outside of the reactor, and the reactor electric heating chuck bottom is provided through The reactor electric heating chuck bottom and the discharging opening communicated with the reactor, the kettle cover is provided with least one charging Mouthful, the high-pressure nozzle being connected with the charging aperture is additionally provided with the reactor, the puddler passes through the reaction The kettle cover of kettle is fixedly linked with the stirring-head in the reactor, and the bottom of the stirring-head is provided with the grinding head.
Further, the grinding head detachable type is fixed on the bottom of the stirring-head, and the grinding head is set to spherical Grinding head.
Further, also including heat-insulation layer, between the reactor electric heating chuck and reactor the heat-insulation layer is provided with.
Further, also including the acidometer being plugged on the kettle cover.
Further, also including automatic discharging valve, the bottom of the reactor electric heating chuck is provided with by the discharging opening The automatic discharging valve being connected with the reactor.
Specifically, the automatic discharging valve is set to polytetrafluoro valve.
Further, also include the thermal electric generator being connected with the reactor electric heating chuck and be driven with the puddler Connected stirring motor.
By such scheme, this utility model at least has advantages below:It is uncontrollable due to reaction condition in order to prevent And the ineligible argentum powder for producing, it is to avoid unnecessary loss, one kind that this utility model is provided accurately prepares argentum powder use Glass reaction kettle can accurately prepare the argentum powder of certain particle diameter.
Described above is only the general introduction of technical solutions of the utility model, in order to better understand skill of the present utility model Art means, and being practiced according to the content of description, with preferred embodiment of the present utility model and coordinate accompanying drawing detailed below Describe in detail bright as after.
Description of the drawings
Fig. 1 is the front view for accurately preparing argentum powder glass reaction kettle that this utility model is provided.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiment of the present utility model is described in further detail.Below Embodiment is used to illustrate this utility model, but is not limited to scope of the present utility model.
Referring to Fig. 1, one kind of the preferred embodiment of this utility model one accurately prepares argentum powder glass reaction kettle, including carrying The reactor 2 of detachable kettle cover 1, reactor electric heating chuck 3, agitating device and at least one high-pressure nozzle 4, agitating device includes Puddler 5 and stirring-head 6, also including grinding head 7, reactor electric heating chuck 3 is set in the outside of reactor 2, reactor electric heating The discharging opening 8 that the bottom of chuck 3 is provided through the bottom of reactor electric heating chuck 3 and communicates with reactor 2, kettle cover 1 is provided with least The high-pressure nozzle 4 being connected with charging aperture 9, kettle of the puddler 5 through reactor 2 are additionally provided with one charging aperture 9, reactor 2 Lid 1 is fixedly linked with the stirring-head 6 in reactor 2, and the bottom of stirring-head 6 is provided with grinding head 7.
This utility model accurately prepares the operation principle of argentum powder glass reaction kettle:
This utility model provide accurately prepare argentum powder glass reaction kettle include with detachable kettle cover 1 reactor 2, Reactor electric heating chuck 3, agitating device and at least one high-pressure nozzle 4, agitating device includes puddler 5 and stirring-head 6, also wraps Grinding head 7 is included, reactor electric heating chuck 3 is set in the outside of reactor 2, and the bottom of reactor electric heating chuck 3 is provided through reaction The bottom of kettle electric heating chuck 3 and the discharging opening 8 communicated with reactor 2, kettle cover 1 is provided with least one charging aperture 9, in reactor 2 The high-pressure nozzle 4 being connected with charging aperture 9 is additionally provided with, puddler 5 is through the stirring-head in the kettle cover 1 and reactor 2 of reactor 2 6 are fixedly linked, and the bottom of stirring-head 6 is provided with grinding head 7;Before argentum powder preparation reaction starts, can pass through can folding in reactor 2 Kettle cover 1 on charging aperture 9 add reactant liquor in reactor 2, the reactor electric heating chuck 3 being arranged outside reactor 2 can be with The reaction temperature being accurately controlled in reactor 2, in reactor 2 agitating device is provided with, and silver-colored reduction reaction can be promoted more fast Speed, in addition, the bottom of stirring-head 6 is provided with grinding head 7, can be prepared in course of reaction, by regulating and controlling stirring with thoroughly in argentum powder And the argentum powder particle diameter that the speed Effective Regulation of grinding is prepared;Argentum powder is prepared after the completion of reaction, can pass through charging aperture 9, After the completion of can be to react in the preparation of argentum powder, wash solution be added, and through high-pressure nozzle 4 to spraying in reactor 2 And cleaning, wash solution include hot nitric acid, 10% NaOH solution and distilled water.
In order to precise control argentum powder reacts the particle size range of the argentum powder for generating, grinding head 7 is detachable to be fixed on stirring-head 6 Bottom, grinding head 7 is set to spherical grinding head;As such, it is possible to pass through different types of grinding head be ground to argentum powder, obtain The argentum powder of different-grain diameter.
For the reaction temperature when colder season maintaining high-volume argentum powder to prepare reaction, also including heat-insulation layer 10, it is provided with heat-insulation layer 10 between reactor electric heating chuck 3 and reactor 2.
Sufficiently grasp to prepare stage for carrying out of reaction to argentum powder in reactor 2, also including being plugged on kettle cover 1 Acidometer 11;As such, it is possible to passing through argentum powder in the solution reaction kettle of acidometer 11 2 prepares the soda acid degree of reaction or to reaction Cleanliness factor detection is carried out after the completion of the process that kettle 2 is rinsed.
The discharging from reactor 2, also including automatic discharging valve 12, the bottom of reactor electric heating chuck 3 are carried out for convenience The automatic discharging valve 12 being connected with reactor 2 by discharging opening 8 is provided with, automatic discharging valve 12 is set to polytetrafluoro valve.
For the reaction temperature and stir speed (S.S.) of the silver mirror reaction in monitor in real time reactor 2, also include and reactor The connected thermal electric generator 13 of electric heating chuck 3 and the stirring motor 14 being connected with the transmission of puddler 5.
The above is only preferred implementation of the present utility model, be not limited to this utility model, it is noted that for For those skilled in the art, on the premise of without departing from this utility model know-why, if can also make Dry to improve and modification, these are improved and modification also should be regarded as protection domain of the present utility model.

Claims (8)

1. one kind accurately prepares argentum powder glass reaction kettle, including with the reactor of detachable kettle cover, reactor electric heating chuck, Agitating device and at least one high-pressure nozzle, the agitating device includes puddler and stirring-head, it is characterised in that:Also include grinding Bistrique, the reactor electric heating chuck is set in the outside of the reactor, and the reactor electric heating chuck bottom is provided through The reactor electric heating chuck bottom and the discharging opening communicated with the reactor, the kettle cover is provided with least one charging Mouthful, the high-pressure nozzle being connected with the charging aperture is additionally provided with the reactor, the puddler passes through the reaction The kettle cover of kettle is fixedly linked with the stirring-head in the reactor, and the bottom of the stirring-head is provided with the grinding head.
It is 2. according to claim 1 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:The grinding head is detachable Formula is fixed on the bottom of the stirring-head.
It is 3. according to claim 2 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:The grinding head is set to ball Shape grinding head.
It is 4. according to claim 1 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:Also include heat-insulation layer, institute State and the heat-insulation layer is provided between reactor electric heating chuck and reactor.
It is 5. according to claim 1 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:It is also described including being plugged in Acidometer on kettle cover.
It is 6. according to claim 1 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:Also include automatic discharging Valve, the bottom of the reactor electric heating chuck is provided with the automatic discharging being connected with the reactor by the discharging opening Valve.
It is 7. according to claim 6 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:The automatic discharging valve sets For polytetrafluoro valve.
It is 8. according to claim 1 accurately to prepare argentum powder glass reaction kettle, it is characterised in that:Also include and the reaction The connected thermal electric generator of kettle electric heating chuck and the stirring motor being connected with puddler transmission.
CN201621089275.8U 2016-09-29 2016-09-29 Accurate preparation glass reactor for silver powder Active CN206082522U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621089275.8U CN206082522U (en) 2016-09-29 2016-09-29 Accurate preparation glass reactor for silver powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621089275.8U CN206082522U (en) 2016-09-29 2016-09-29 Accurate preparation glass reactor for silver powder

Publications (1)

Publication Number Publication Date
CN206082522U true CN206082522U (en) 2017-04-12

Family

ID=58481153

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621089275.8U Active CN206082522U (en) 2016-09-29 2016-09-29 Accurate preparation glass reactor for silver powder

Country Status (1)

Country Link
CN (1) CN206082522U (en)

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Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Zhang Jianguo

Inventor after: Zhang Shuli

Inventor after: Zhou Wensheng

Inventor after: Wang Xufeng

Inventor after: Li Fei

Inventor after: Zhang Jing

Inventor before: Zhang Shuli

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20180123

Address after: 21 Pingdingshan City, Jiangsu Province, the middle of the miners Road, No. 467000

Co-patentee after: Suzhou Inreal Optoelectronic Material Technology Co., Ltd.

Patentee after: China Pingmei Shenma Energy Chemical Group Co., Ltd.

Address before: 215000 Suzhou Industrial Park, Jiangsu, China Road, No. 1

Patentee before: Suzhou Inreal Optoelectronic Material Technology Co., Ltd.

CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Zhang Jianguo

Inventor after: Lv Youchang

Inventor after: Zhang Shuli

Inventor after: Zhou Wensheng

Inventor after: Wang Xufeng

Inventor after: Gu Xiaohu

Inventor after: Zhang Jing

Inventor before: Zhang Jianguo

Inventor before: Zhang Shuli

Inventor before: Zhou Wensheng

Inventor before: Wang Xufeng

Inventor before: Li Fei

Inventor before: Zhang Jing