CN206082473U - Generate simple and easy device of hydrogen sulfide - Google Patents

Generate simple and easy device of hydrogen sulfide Download PDF

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Publication number
CN206082473U
CN206082473U CN201621053414.1U CN201621053414U CN206082473U CN 206082473 U CN206082473 U CN 206082473U CN 201621053414 U CN201621053414 U CN 201621053414U CN 206082473 U CN206082473 U CN 206082473U
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CN
China
Prior art keywords
valve
main body
sodium sulfide
pump
discharge pipe
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Application number
CN201621053414.1U
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Chinese (zh)
Inventor
吴乐谋
陈深培
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Kelixin (Zhuhai) new energy Co.,Ltd.
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ZHUHAI KELIXIN METAL MATERIALS CO Ltd
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Abstract

The utility model discloses a generate simple and easy device of hydrogen sulfide. It includes vulcanized sodium makeup tank, vulcanized sodium storage tank, check valve, filter equipment, main part reation kettle and barometer. The utility model discloses a generate simple and easy device of hydrogen sulfide is the totally -enclosed configuration, can reduce hydrogen sulfide gas and personally experience sth. Part of the body to the pollution of environment, the utility model discloses a generate simple and easy device of hydrogen sulfide simple structure, easy to operate, the security is high, can effectual reduction working strength.

Description

A kind of easy device for generating hydrogen sulfide
Technical field
This utility model is related to a kind of reaction unit, and in particular to a kind of easy device of generation hydrogen sulfide.
Background technology
Traditional cobalt metallurgy industry, be related to removing heavy metals need to using sulfide removal when, more using sodium sulfide or sulfuration Ammonia is processed, but some as high-purity cobalt liquid need to use sulfide removal when, using sodium sulfide or sulfuration ammonia treatment when, will Bring sodium ion and these impurity of ammonium ion, or the device closed system imperfection for making hydrogen sulfide into, it is impossible to meet normal raw The demand of product.
Utility model content
The purpose of this utility model is to provide a kind of easy device for generating hydrogen sulfide, and the device can produce offer and not bring into The high-pure hydrogen sulfide of impurity, and its airtight performance is good, can reduce environmental pollution.
This utility model is practiced by the following technical programs:
The easy device for generating hydrogen sulfide of the present utility model, it is characterised in that including sodium sulfide make-up tank, sodium sulfide storage Groove, one way stop peturn valve, defecator, main body reactor and air gauge, the described discharge pipe of sodium sulfide make-up tank and entering for pump A Liquid mouth is connected, and the leakage fluid dram of pump A is connected with the first pipeline, and the other end of the first pipeline is stretched in sodium sulfide storage tank, sodium sulfide The discharge pipe of storage tank is connected with the inlet of pump B, and the leakage fluid dram of pump B is connected with the first return duct and second pipe simultaneously, and first The other end of return duct is stretched in sodium sulfide storage tank, and the other end of second pipe is connected with the liquid inlet of main body reactor, Defecator, one way stop peturn valve, stream are sequentially provided with toward main body reactor direction on described second pipe, from sodium sulfide storage tank Gauge, is also connected with sulphuric acid feed tube on the liquid inlet of main body reactor, on described sulphuric acid feed tube, anti-toward main body from free end Kettle direction is answered to be sequentially provided with one way stop peturn valve and effusion meter, the leakage fluid dram of main body reactor is connected with the 3rd pipeline, the 3rd pipeline Other end be connected with the liquid inlet of pump C, the leakage fluid dram of pump C is connected with the second return duct and waste liquid discharge pipe simultaneously, described The other end of the second return duct be connected with the reclaimed materials entrance for being provided with main body reactor top, the row on main body reactor top QI KOU is connected with hydrogen sulfide discharge pipe, on hydrogen sulfide discharge pipe is provided with air gauge, on waste liquid discharge pipe is provided with effusion meter, Agitator is additionally provided with sodium sulfide make-up tank.
It is preferred that, observation window is additionally provided with main body reactor, to observe the response situation in main body reactor.
It is preferred that, valve A is provided with the discharge pipe of sodium sulfide make-up tank, valve is provided with the discharge pipe of sodium sulfide storage tank B, is provided with valve C on the first return duct, and on second pipe, the leading portion and back segment of defecator is respectively equipped with valve D and valve E, on sulphuric acid feed tube, the leading portion of one way stop peturn valve is provided with valve F, on the 3rd pipeline is provided with valve G, in effusion meter and pump C Between waste liquid discharge pipe be provided with valve I, valve H is provided with the second return duct, in the recovery of valve H and main body reactor The second return duct between material entrance is provided with evacuated tube, and evacuated tube is provided with valve J.
This utility model is so operation:
Sodium sulfide and water form sodium sulfide solution in being added to sodium sulfide make-up tank, Jing pump A pumps to sodium sulfide storage tank are stored, Sodium sulfide solution Jing pump B pumps Jing in sodium sulfide storage tank filters device and filters, and one way stop peturn valve and effusion meter are reacted into main body In kettle, unnecessary the first return ducts of sodium sulfide solution Jing blowback sodium sulfide storage tank, dilute sulfuric acid Jing sulphuric acid feed tubes flow through one-way non-return Valve, effusion meter are entered in main body reactor, in main body reactor, and sulphuric acid and sodium sulfide reaction generate hydrogen sulfide, stink damp The air vent on body Jing main body reactors top, hydrogen sulfide discharge pipe are discharged for using, and reacted waste liquid solid Jing pump C pumps are extremely Waste liquid discharge pipe is discharged, and if some waste liquid solids can be recycled, it is anti-that Jing pump C pumps to the second return duct are back to main body In answering kettle.
As can be seen here, the easy device for generating hydrogen sulfide of the present utility model is total enclosing configuration, it is possible to reduce hydrogen sulfide Pollution of the gas to environment, the easy device simple structure of generation hydrogen sulfide of the present utility model are easily operated, safe, Working strength can be effectively reduced.
Description of the drawings:
Fig. 1 is the structural representation of the easy device for generating hydrogen sulfide of the present utility model;
Wherein 1, sodium sulfide make-up tank;2nd, agitator;3rd, pump A;4th, the first pipeline;5th, sodium sulfide storage tank;6th, the first backflow Pipe;7th, pump B;8th, second pipe;9th, effusion meter;10th, one way stop peturn valve;11st, defecator;12nd, sulphuric acid feed tube;13rd, air pressure Table;14th, one way stop peturn valve;15th, effusion meter;16th, observation window;17th, the 3rd pipeline;18th, pump C;19th, effusion meter;20th, waste liquid is discharged Pipe;21st, evacuated tube;22nd, hydrogen sulfide discharge pipe;23rd, main body reactor;24th, the second return duct;A, B, C, D, E, F, G, H, I and J Valve A, B, C, D, E, F, G, H, I and J are represented respectively.
Specific embodiment:
Following examples are further illustrated to of the present utility model, rather than to restriction of the present utility model.
Embodiment 1:
As shown in figure 1, the easy device of the generation hydrogen sulfide of the present embodiment, including sodium sulfide make-up tank 1, sodium sulfide storage tank 5th, one way stop peturn valve, defecator 11, main body reactor 23 and air gauge 13, the discharge pipe of described sodium sulfide make-up tank 1 with The inlet of pump A 3 is connected, and the leakage fluid dram of pump A is connected with the first pipeline 4, and the other end of the first pipeline stretches into sodium sulfide storage tank In 5, the discharge pipe of sodium sulfide storage tank is connected with the inlet of pump B 7, the leakage fluid dram of pump B simultaneously with the first return duct 6 and second Pipeline 8 is connected, and the other end of the first return duct is stretched in sodium sulfide storage tank, other end and the main body reactor of second pipe 23 liquid inlet is connected, and on described second pipe, from sodium sulfide storage tank is sequentially provided with filtration dress toward main body reactor direction 11, one way stop peturn valve 10, effusion meter 9 are put, sulphuric acid feed tube 12 on the liquid inlet of main body reactor, is also connected with, described sulphuric acid enters One way stop peturn valve 14 and effusion meter 15, the row of main body reactor are sequentially provided with toward main body reactor direction in liquid pipe, from free end Liquid mouth is connected with the 3rd pipeline 17, and the other end of the 3rd pipeline is connected with the liquid inlet of pump C 18, the leakage fluid dram of pump C simultaneously with Second return duct 24 is connected with waste liquid discharge pipe 20, the other end of described the second return duct be provided with main body reactor top Reclaimed materials entrance be connected, the air vent on main body reactor top is connected with hydrogen sulfide discharge pipe 22, on hydrogen sulfide discharge pipe Air gauge 13 is provided with, effusion meter 19 is provided with waste liquid discharge pipe, agitator 2 is additionally provided with sodium sulfide make-up tank.
Observation window 16 is additionally provided with main body reactor, to observe the response situation in main body reactor.
Valve A A are provided with the discharge pipe of sodium sulfide make-up tank, valve B is provided with the discharge pipe of sodium sulfide storage tank B, is provided with valve C C on the first return duct, on second pipe the leading portion and back segment of defecator be respectively equipped with valve D D and Valve E E, on sulphuric acid feed tube, the leading portion of one way stop peturn valve is provided with valve F F, and valve G G are provided with the 3rd pipeline, Waste liquid discharge pipe between effusion meter and pump C 18 is provided with valve I I, is provided with valve H H, in valve H on the second return duct The second return duct and the reclaimed materials entrance of main body reactor between is provided with evacuated tube 21, and evacuated tube is provided with valve J.

Claims (3)

1. a kind of easy device for generating hydrogen sulfide, it is characterised in that including sodium sulfide make-up tank, sodium sulfide storage tank, it is unidirectional only Valve, defecator, main body reactor and air gauge are returned, the discharge pipe of described sodium sulfide make-up tank is connected with the inlet of pump A, The leakage fluid dram of pump A is connected with the first pipeline, and the other end of the first pipeline is stretched in sodium sulfide storage tank, the discharge of sodium sulfide storage tank Pipe is connected with the inlet of pump B, and the leakage fluid dram of pump B is connected with the first return duct and second pipe simultaneously, the first return duct it is another Outer one end is stretched in sodium sulfide storage tank, and the other end of second pipe is connected with the liquid inlet of main body reactor, described Defecator, one way stop peturn valve, effusion meter, main body are sequentially provided with toward main body reactor direction on two pipelines, from sodium sulfide storage tank Sulphuric acid feed tube is connected with the liquid inlet of reactor also, on described sulphuric acid feed tube, from free end toward main body reactor direction One way stop peturn valve and effusion meter are sequentially provided with, the leakage fluid dram of main body reactor is connected with the 3rd pipeline, other the one of the 3rd pipeline End is connected with the liquid inlet of pump C, and the leakage fluid dram of pump C is connected with the second return duct and waste liquid discharge pipe simultaneously, described second time The other end of flow tube is connected with the reclaimed materials entrance for being provided with main body reactor top, the air vent and sulfur on main body reactor top Change hydrogen discharge pipe to be connected, air gauge is provided with hydrogen sulfide discharge pipe, is provided with effusion meter, matches somebody with somebody in sodium sulfide on waste liquid discharge pipe Agitator is additionally provided with groove processed.
2. it is according to claim 1 generate hydrogen sulfide easy device, it is characterised in that be additionally provided with main body reactor Observation window.
3. it is according to claim 1 generate hydrogen sulfide easy device, it is characterised in that in the discharge of sodium sulfide make-up tank Pipe is provided with valve A, and valve B is provided with the discharge pipe of sodium sulfide storage tank, and valve C is provided with the first return duct, second On pipeline, the leading portion and back segment of defecator is respectively equipped with valve D and valve E, the leading portion of one way stop peturn valve on sulphuric acid feed tube Valve F is provided with, valve G is provided with the 3rd pipeline, be provided with valve I on the waste liquid discharge pipe between effusion meter and pump C, Two return ducts are provided with valve H, are provided with emptying on the second return duct between the reclaimed materials entrance of valve H and main body reactor Pipe, evacuated tube are provided with valve J.
CN201621053414.1U 2016-09-13 2016-09-13 Generate simple and easy device of hydrogen sulfide Active CN206082473U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621053414.1U CN206082473U (en) 2016-09-13 2016-09-13 Generate simple and easy device of hydrogen sulfide

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Application Number Priority Date Filing Date Title
CN201621053414.1U CN206082473U (en) 2016-09-13 2016-09-13 Generate simple and easy device of hydrogen sulfide

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108883935A (en) * 2015-12-27 2018-11-23 梅多克斯私人投资有限公司 For generating H in alkaline medium2The system and its application method of S

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108883935A (en) * 2015-12-27 2018-11-23 梅多克斯私人投资有限公司 For generating H in alkaline medium2The system and its application method of S

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CP03 Change of name, title or address

Address after: 519000 No. 6, surge Road, nanshaui Town, Gaolan Port Economic Zone, Zhuhai, Guangdong

Patentee after: Kelixin (Zhuhai) new energy Co.,Ltd.

Address before: 519050 comprehensive building, Langshan Road, fine chemical industry zone, Gaolan Port Economic Zone, Zhuhai City, Guangdong Province

Patentee before: ZHUHAI KELIXIN METAL MATERIALS Co.,Ltd.

CP03 Change of name, title or address