CN206081759U - Organosilicon diformazan sour oil separating device that hydrolysises - Google Patents

Abstract

The utility model discloses an organosilicon diformazan sour oil separating device that hydrolysises, it includes horizontal cylinder, the supporting legs top at parallel arrangement is installed to the cylinder cylinder, the left end of cylinder intercommunication has a digest inlet pipe, is provided with the overflow cylinder at the top of cylinder, the top of overflow cylinder is provided with the top spout hole, install the overflow pipe on the lateral wall of overflow cylinder, sour back flow is installed to the bottom of cylinder, is provided with the sight glass hole at the right -hand member of cylinder. Hydrochloric acid and oily hydrolyzate that this separator formed after can effectually hydrolysising to the organosilicon diformazan carry out effectual separation, improve separation efficiency, and automatic formation of being convenient for is moreover reduced equipment cost and is dropped into.

Description

A kind of organosilicon diformazan hydrolysis acid oil separating device

Technical field

This novel practical is related to chemical production technical production field, particularly a kind of organosilicon diformazan monomer hydrolysis acid oil From.

Background technology

The hydrochloric acid formed after the hydrolysis of diformazan monomer and oily hydrolysate, the two needs longer time of repose to divide completely From most manufacturer is processed by the following two kinds mode：One is to adopt big volume oleic acid separator, but due to separating As lower diameter, oil is larger in separator interior interference effect with acid, causes interface not obvious enough, separates effect on device top Fruit is still poor；Two is that the hydrolysate is sent into into special storage tank storage, is separated again after standing fully, although separating effect Preferably, but equipment investment is higher.

Utility model content

The utility model discloses a kind of sour oil separating device of organosilicon diformazan hydrolysis, this point according to the deficiencies in the prior art Hydrochloric acid and oily hydrolysate that can be effectively to being formed after the hydrolysis of organosilicon diformazan from device be efficiently separated, and are improved Separative efficiency, and it is easy to automation to generate, reduce equipment cost input.

In order to solve above-mentioned technical problem, the utility model proposes technical scheme below：A kind of organosilicon diformazan hydrolysis acid Oil separating device, it includes horizontal cylinder cylinder, and the cylinder cylinder is arranged on the support feet top being arranged in parallel Portion, the left end of the cylinder cylinder is communicated with hydrolyzate feed pipe, and at the top of cylinder cylinder overflow cylinder is provided with, Top spout hole is provided with the top of the overflow cylinder, overflow pipe, the cylinder point are installed on the side wall of the overflow cylinder Sour return duct is installed from the bottom of cylinder, the right-hand member of cylinder cylinder is provided with peephole hole.

Liquid level display column is installed on the side wall of the overflow cylinder.

Charging electromagnetic valve is installed on the hydrolyzate feed pipe.

Overflow discharging electromagnetic valve is installed on the overflow pipe, after the overflow discharging electromagnetic valve discharging is connected with Tail pipe, the end of the discharging tail pipe is arranged on inside fluid surge tank.

Acid solution discharging electromagnetic valve is installed on the sour return duct, after the acid solution discharging electromagnetic valve acid is connected with Liquid discharging tail pipe, the end of the acid solution discharging tail pipe is arranged on inside acid liquor storage tank.

The utility model has the advantages that：

1st, the sour oil mixture that Concentrated acid hydrolysis are formed is entered after cylinder cylinder by hydrolyzate feed pipe and is layered, lower floor Hydrochloric acid is back to closed circuit by sour return duct, and upper strata oily hydrolysate, to hydrolysate surge tank, is made by overflow pipe overflow Production operation serialization, automation.

2nd, separator adopts horizontal cylinder cylinder, vertical type cylinder device top, provide not only larger separated space, and And the upper oil phase extraction time is extended, and separating interface is become apparent from, separating effect is more preferable.

3rd, using the sour oil interface of separation visor observation at peephole hole, it is thick that liquid level display column constantly monitors oil reservoir Degree, the two fit through regulation mend acid amount come controlling interface stablize.

Description of the drawings

With reference to the accompanying drawings and examples the utility model is described in further detail.

Fig. 1 is the utility model overall structure diagram.

Fig. 2 is the utility model stereogram.

Fig. 3 is utility model works theory structure schematic diagram.

In figure：Hydrolyzate feed pipe 1, charging electromagnetic valve 2, cylinder cylinder 3, support feet 4, sour return duct 5, acid solution Discharging electromagnetic valve 6, acid solution discharging tail pipe 7, acid liquor storage tank 8, fluid surge tank 9, discharging tail pipe 10, peephole hole 11, overflow Flow out material electromagnetic valve 12, overflow pipe 13, top spout hole 14, overflow cylinder 15, liquid level display column 16.

Specific embodiment

Embodiment of the present utility model is described further below in conjunction with the accompanying drawings.

Such as Fig. 1-3, a kind of organosilicon diformazan hydrolysis acid oil separating device, it includes horizontal cylinder cylinder 3, described Cylinder cylinder 3 is arranged on the top of support feet 4 being arranged in parallel, and the left end of the cylinder cylinder 3 is communicated with hydrolyzate Feed pipe 1, at the top of cylinder cylinder 3 overflow cylinder 15 is provided with, and the top of the overflow cylinder 15 is provided with top overflow Hole 14, is provided with overflow pipe 13 on the side wall of the overflow cylinder 15, the bottom of the cylinder cylinder 3 is provided with sour return duct 5, the right-hand member of cylinder cylinder 3 is provided with peephole hole 11.

Further, liquid level display column 16 is installed on the side wall of the overflow cylinder 15.Shown by liquid level Post 16 constantly shows the height of the inside fluid of overflow cylinder 15 according to law of connected vessels.

Further, charging electromagnetic valve 2 is installed on the hydrolyzate feed pipe 1.Can by feeding electromagnetic valve 2 Control dosing for hydrolyzate.

Further, overflow discharging electromagnetic valve 12, the overflow discharging electromagnetic valve are installed on the overflow pipe 13 Discharging tail pipe 10 is connected with after 12, the end of the discharging tail pipe 10 is arranged on inside fluid surge tank 9.Buffered by fluid Fluid after 9 pairs, tank is separated is collected.

Further, acid solution discharging electromagnetic valve 6, the acid solution discharging electromagnetic valve 6 are installed on the sour return duct 5 Acid solution discharging tail pipe 7 is connected with afterwards, and the end of the acid solution discharging tail pipe 7 is arranged on inside acid liquor storage tank 8.By acid solution Acid solution after holding vessel 8 pairs is separated is reclaimed, and is utilized next time with facilitating.

The course of work of the present utility model and operation principle are：

As shown in figure 3, first, the sour oil mixture that Concentrated acid hydrolysis are formed is by hydrolyzate feed pipe 1 into cylinder point It is layered after cylinder 3, lower floor's hydrochloric acid is back to closed circuit by sour return duct 5, upper strata oily hydrolysate is overflow by overflow pipe 13 Fluid surge tank 9 is flow to, production operation serialization, automation is made.

In separation process, control charging electromagnetic valve 2 can be passed through and then the flow of entrance is controlled, by controlling acid solution The back-flow velocity of discharging electromagnetic valve 6 and then control acid solution, by controlling overflow discharging electromagnetic valve 12 upper strata oil can be controlled The tapping flowrate of shape hydrolysate.

By the sour oil interface of separation visor at peephole hole 11 observation, when detached fluid be not enough can automatically to Tank interior supplements fluid.

By above-mentioned description, those skilled in the art completely can be without departing from this utility model technological thought In the range of, carry out various change and modification all within protection domain of the present utility model.It is of the present utility model most Matters, belong to the common knowledge of those skilled in the art.

Claims (6)

1. a kind of organosilicon diformazan hydrolyzes sour oil separating device, it is characterised in that：It includes horizontal cylinder cylinder（3）, The cylinder cylinder（3）Installed in the support feet being arranged in parallel（4）Top, the cylinder cylinder（3）Left end connect It is connected with hydrolyzate feed pipe（1）, in cylinder cylinder（3）Top be provided with overflow cylinder（15）, the overflow cylinder（15）'s Top is provided with top spout hole（14）, the overflow cylinder（15）Side wall on overflow pipe is installed（13）, the cylinder point From cylinder（3）Bottom sour return duct is installed（5）, in cylinder cylinder（3）Right-hand member be provided with peephole hole（11）.

2. a kind of organosilicon diformazan according to claim 1 hydrolyzes sour oil separating device, it is characterised in that：The overflow cylinder （15）Side wall on liquid level display column is installed（16）.

3. a kind of organosilicon diformazan according to claim 1 hydrolyzes sour oil separating device, it is characterised in that：The hydrolyzate Feed pipe（1）On charging electromagnetic valve is installed（2）.

4. a kind of organosilicon diformazan according to claim 1 hydrolyzes sour oil separating device, it is characterised in that：The overflow pipe （13）On be provided with overflow discharging electromagnetic valve（12）, the overflow discharging electromagnetic valve（12）Discharging tail pipe is connected with afterwards （10）, the discharging tail pipe（10）End be arranged on fluid surge tank（9）It is internal.

5. a kind of organosilicon diformazan according to claim 1 hydrolyzes sour oil separating device, it is characterised in that：The acid backflow Pipe（5）On be provided with acid solution discharging electromagnetic valve（6）, the acid solution discharging electromagnetic valve（6）Acid solution discharging tail is connected with afterwards Pipe（7）, the acid solution discharging tail pipe（7）End be arranged on acid liquor storage tank（8）It is internal.

6. a kind of organosilicon diformazan according to claim 2 hydrolyzes sour oil separating device, it is characterised in that：The liquid level is high Degree display column（16）Made using transparent material.